• Title/Summary/Keyword: 금속시편

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Lap Shear Strength Test of Space Adhesives (우주용 접착제의 중첩 전단 강도 시험)

  • 서유덕;박상훈;윤성기;이상률;이덕규;장홍술;이승훈;김현중;김지연;엄태경;이응식;정대준
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.34 no.10
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    • pp.40-47
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    • 2006
  • Optical performance of the mirror for satellite camera is highly dependent on the adhesive properties of its support. Therefore, in this paper, the adhesive properties of three kinds of space adhesives are investigated. For this purpose, the lap shear test is performed with Zerodur-to-metal lap shear specimen as well as metal-to-metal one. And it is also investigated whether reliable adhesive strength can be secured after the specific thermal cycle. Finally, the properties of three adhesives are compared with each other.

Interfacial Fracture Toughness Measurement of Composite/metal Bonding (복합재료/금속 접착 계면의 파괴인성치 측정)

  • Kim, Won-Seock;Lee, Jung-Ju
    • Composites Research
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    • v.21 no.4
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    • pp.7-14
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    • 2008
  • Prediction of the load-bearing capacity of an adhesive-bonded Joint is of practical importance for engineers. This paper introduces interface fracture mechanics approach to predict the load-bearing capacity of composite metal bonded joints. The adhesion strength of composite/steel bonding is evaluated in terms of the energy release rate of an interfacial crack and the fracture toughness of the interface. Virtual track closure technique (VCCT) is used to calculate energy release rates, and hi-material end-notched flexure (ENF) specimens are devised to measure the interfacial fracture toughness. Bi-material ENF specimens gave consistent mode II fracture toughness $(G_{IIc})$ values of the composite/steel interface regardless of the thickness of specimens. The critical energy release rates of double-lap joints showed a good agreement with the measured fracture toughness. Therefore. the energy-based interfacial fracture characterization can be a practical engineering tool for predicting the load-bearing capacity of bonded joints.

A STUDY ON METAL RELEASE OF TIN ION-PLATED STAINLESS STEEL ORTHODONTIC APPLIANCES (TiN 피막 처리된 스테인레스강 교정용 장치물의 금속 유리에 대한 연구)

  • KIM, Myung-Sook;Sung, Jae-Hyun;Kwon, Oh-Won
    • The korean journal of orthodontics
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    • v.25 no.1 s.48
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    • pp.43-54
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    • 1995
  • This study was conducted to examine the metal release of TiN-plated stainless steel orthodontic appliances by constructing the simulated orthodontic appliances equivalent to maxillary half arch, by dividing into TiN-plated and TiN-nonplated Bloops and by dividing again these groups into welded and nonwelded groups. And then, the total quantity of metal release was obtained by measuring the amounts of both soluble and precipitated nickel and chromium after immersing in artificial saliva for 15 days. And then, the corrosion appearance of surface structure was observed by using SEM. The results of this study were summarized as follows. 1. The total amounts of released nickel and chromium showed that the TiN-plated group after welding(Group 1) was 25.46 ${\mu}g$, respectively, and 17.4 ${\mu}g$, while the TiN-nonplated group after welding(Group III) was 54.69 ${\mu}g$, respectively, and 85.27 ${\mu}g$. Then, the TiN-Plated group indicated less amounts of metal release(p<0.05). 2. The total amounts of the TiN-plated group without welding(Group II) was 0.05${\mu}g$ and 0.34${\mu}g$, respectively. Then, it was shown that the TiN-plated group without welding(Group II) indicated less metal release than that of the TiN-Plated group after welding(Group I)(p<0.01, p<0.05). 3. When observing their surface structure, there were a lot of precipitate and pitting corrosion in the groups with welding(Group I & III), when the TiN-plated group(Group I) showed lower level than the TiN-nonplated group(Group IIII). On the other hand, the groups without welding(Group II & IV) indicated a little of pitting corrosion. 4. In case of observation with the naked eyes, it was shown that there were significant disco1oration and corrosion in the groups with welding(Group I & III), while there was no any remarkable change in the groups without welding(Group II & IV).

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Effect of engineered barriers on the leach rate of cesium from spent PWR fuel (가압경수로 사용후핵연료 중 세슘의 침출에 미치는 공학적 방벽 영향)

  • Chun Kwan Sik;Kim Seung-Soo;Choi Jong-Won
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.3 no.4
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    • pp.329-333
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    • 2005
  • To identify the effect of engineered barriers on the leach rate of cesium from spent PWR fuel under a synthetic granitic groundwater, the related leach tests with and without bentonite or metals have been performed up to about 6 years. The leach rates were decreased as a function of leaching time and then became a constant after a certain period. The period in a bare spent fuel was much longer than that with bentonite or metal sheets. The cumulative fraction of cesium released from the spent fuel with bentonite or with copper and stainless steel sheets was steadily increased, but the fraction from bare fuel was rapidly and then sluggishly increased. However, the values deducted its gap inventory from the cumulative fraction of cesium released from the bare fuel was almost very close to the others. These suggest that the initial release of cesium from bare fuel might be dependant on its gap inventory and the effect of engineered barriers on the long-term leach rate of cesium would be insignificant but the rate with engineered barriers could be reduced in the initial transient period due to their retardation effect. And the long-term leach rate of cesium from spent fuel in a repository would be approached to a constant rate of $2\times10^{-2}g/m^2-day$.

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Applicability of Volatile Corrosion Inhibitor and VCI Films for Conservation of Artworks (미술작품의 보존을 위한 기화성 방청제 및 방청필름의 적용성 연구)

  • Beom, Dae Geon;Han, Ye Bin
    • Journal of Conservation Science
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    • v.36 no.2
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    • pp.82-92
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    • 2020
  • Modern artworks are constructed using a variety of materials and techniques. Sculptures, which predominantly consist of metals, usually have different shapes and consist of different material mixtures. The structural and material properties of these sculptures are often controlled by conservation treatment methods. However, the application of existing treatment methods is challenging at times, indicating that more diverse treatment materials and techniques are necessary. Therefore, in this study, a treatment method that employs volatile corrosion inhibitor(VCI) powder, rather than an anti-corrosion solution, for the conservation and management of metal artworks was used. VCI powder and VCI films containing VCI powder were used, and the results obtained confirmed that both of them showed anti-corrosion effect. Only a slight change in the chromaticity of metal samples was observed, and compared to the untreated samples, the application of the VCI powder resulted in a decrease in the rate of corrosion by half. Moreover, VCI film tests revealed that comparing to the untreated or polyethylene film-treated samples, VCI film treatment resulted in a decrease in the occurrence of corrosion compounds. The contact angle, surface energy, and surface electrical resistance were measured, and the evaluation of these surface properties established the anti-corrosion effect of VCI. Additionally, direct application of VCI and VCI films on actual sculptures further confirmed the anti-corrosion effect of VCI.

The hardening effect by ice-quenching after oxidation of a Pd-Ag-Sn-Au metal-ceramic alloy during porcelain firing simulation (금속-세라믹용 Pd-Ag-Sn-Au계 합금의 모의소성 시 산화처리 후 급랭에 의한 경화 효과)

  • Shin, Hye-Jeong;Kim, Min-Jung;Kwon, Yong-Hoon;Kim, Hyung-Il;Seol, Hyo-Joung
    • Korean Journal of Dental Materials
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    • v.44 no.3
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    • pp.197-206
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    • 2017
  • The hardening effect by ice-quenching after oxidation of a Pd-Ag-Sn-Au metal-ceramic alloy during porcelain firing simulation was investigated by means of hardness test, field emission scanning electron microscopic observations, and X-ray diffraction analysis. The hardness decreased by ice-quenching after oxidation, which was induced by the homogenization of the ice-quenched specimen. The decreased hardness by ice-quenching after oxidation was recovered from the wash stage which was the first stage of the remaining firing process for bonding porcelain. After wash stage, the hardness of the ice-quenched specimens decreased during the subsequent porcelain firing process. But the final hardness of the ice-quenched specimens after oxidation was higher than that of the specimens cooled at stage 0 after oxidation. The increase in hardness of the specimens during the first firing process was caused by the lattice strains generated at the interface between the face-centered cubic Pd-Ag-rich matrix and the face-centered tetragonal Pd3(Sn, Ga, In) precipitate. The decrease in hardness of the specimens during the remaining firing process was caused by the microstructural coarsening.

Feasibility Study of Flexible Phased Array Ultrasonic Technology Using Irregular Surface Specimen (불규칙 표면 시편을 이용한 Flexible 위상배열초음파기술 적용 연구)

  • Lee, Seung-Pyo;Moon, Yong-Sig;Jung, Nam-Du
    • Journal of the Korean Society for Nondestructive Testing
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    • v.35 no.1
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    • pp.52-60
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    • 2015
  • Nuclear power plant contain many dissimilar metal welds that connect carbon steel components with stainless steel pipes using alloy600 welding materials. Primary water stress corrosion cracks at dissimilar metal welds have been continuously reported around the world. In periodic integrity evaluations, dissimilar metal welds are examined using a generic ultrasonic testing procedure, KPD-UT-10. In this procedure, the gap between the probe and examination surface is limited to 1/32 inch (0.8mm). It is not easy to test some dissimilar metal welds in Korean plants applying ordinary technology because of their tapered shapes and irregular surface conditions. This paper introduces a method for applying a flexible phased array technology to improve the reliability of ultrasonic testing results for various shapes and surface conditions. The artificial flaws in specimens with irregular surfaces were completely detected using the flexible phased array ultrasonic technology. Therefore, it can be said that the technology is applicable to field examination.

Development of a Functional Mortar for Algae Growth Restraining by Using Soluble Glass (수용성 유리를 이용한 조류 생장 억제형 기능성 모르타르의 개발)

  • Kim, Jun Hwan;Kang, Hojeong;Choi, Se Young;Lim, Yun Mook
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.35 no.4
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    • pp.791-799
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    • 2015
  • This study focuses on the algae growth restraining. Many researches on a critical damage from algae growth are published, but it is hard to find how th restrain. Abnormal algae increasing is a problem, because it makes red tides, biodeterioration, etc. Therefore this study aims to decrease the damage from algae growth. Some metal ions have been used microorganism killing materials from old times. Especially, Cu ions are highly effective. Based on these uses of the metal ions, a functional mortar which restrains algae growth is developed. The mortar contains soluble glass which dissolve in water. The soluble glass was made of Cu ions and phosphates. When the soluble glass is dissolved, Cu ions are soaked out stably from the soluble glass. Culture mediums which incubate algae were made to evaluate the developed mortar specimens. Culture mediums were filled with fresh water and sea water. Algae were incubated for fourteen days in culture mediums. The evaluating methods are measuring volume of the dissolved organic carbon and the chlorophyll. Using these two measurements, the mortar specimens are judged that can restrain algae or not. According to the result, the functional mortars of culture medium filled with fresh and sea water shows similar trend. The functional mortar for restraining algae growth performs that's role well.

Matrix Effects on X-Ray Fluorescence Intensities in Fe-Ni-Cr System (철-니켈-크롬 三成分系에서 X-線 螢光의 매트릭스 效果에 관한 硏究)

  • Yang Che-Hyon;Yeh Jin-Hae
    • Journal of the Korean Chemical Society
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    • v.37 no.10
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    • pp.861-866
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    • 1993
  • In general, the concentration of constituents can be more accurately measured in x-ray fluorescence analysis of Fe-Ni-Cr alloy by reducing and correcting the matrix effect with standard ingot samples. Because of the difficult the treatment at a high temperature in preparing the ingot samples of various concentrations, several standard specimens were prepared by mixing the powders of the metallic oxides in certain proportions and pressing them with a costant pressure. With the metallic oxide specimens thus obtained, different matrix coefficients were calculate from the intensities of the strength of the x-ray fluorescence and the concentration of the substances. It is found that effects of Fe and Cr on Ni are absorption rich and effects of Fe and Ni on Cr are enhancement rich, whereas Ni enhances Fe Fluorescence but Cr absorves Fe K${\alpha}$ line. And the x-ray fluorescence intensities were compared and analyzed between the metallic oxides and the ingot samples.

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Shearing Phase Lock-in Infrared Thermography for Defects Evaluation of Metallic Materials Specimen (금속재료 시편의 결함평가에 대한 전단위상 Lock-in 적외선열화상 연구)

  • Park, Jeong-Hak;Choi, Man-Yong;Kim, Won-Tae
    • Journal of the Korean Society for Nondestructive Testing
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    • v.30 no.2
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    • pp.91-97
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    • 2010
  • This paper proposes method to evaluate the location and size of the internal defects of metallic specimens by the shearing phase lock-in infrared thermography. Until now, infrared thermography test for metal specimen of STS304 and Cu-Zn were conducted to find the best test conditions. However, In unspecified situation of the form and existence of defects, there was a disadvantage to takes a long time for finding the optimal experimental conditions. The defect detection and evaluation was performed at 60 MHz signal using lock-in and shearing-phase method under limited heating conditions. By shearing-phase distribution method, Defects for the maximum, minimum and zero points were quantitatively detected at the size and location of the subsurface. As results, application of the proposed technique was verified for STS304 and Cu7-Zn3 with artificial defect and factors affected defect evaluation were searched and analyzed.