• Proceedings of the Optical Society of Korea Conference
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• 2000.02a
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• pp.236-237
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• 2000

용액인상법에 의하여 Cr$^{3+}$ 이온이 0.1-0.2% 주입된 Alexandrite (Cr$^{3+}$ :BeAl$_2$O$_4$) 단결정을 성장하고, 성장한 단결정을 이용하여 레이저 소자를 제조하였다. 고품질의 단결정을 성장할 수 있는 결정성장조건을 규명하고, Cr$^{3+}$ 이온의 유효편석 계수를 계산하였으며, 결정 결함 및 분광 물성을 조사하였다. 결정성장 실험 결과, 유속 3 1/min의 질소분위기, 이리듐 도가니 및 <001>방위의 Alexandrite 단결정을 종자결정으로 사용하여 결정을 성장하는 경우 최적의 결정성장 조건은 인상속도 0.5-1.0 mm/hr와 회전속도 20-25 rpm이었다. 육성된 결정은 (100)면이 넓게 발달되었으며, (120)과 (010)면이 측면에 발달되는 판상의 직팔각기둥의 형태로 성장되었다. 결정결함으로써 parasite crystal의 형성과 경계면의 균열, striation, inclusion 등이 검출되었다. Alexandrite 단결정 내에 분포하는 Cr$^{3+}$ 이온의 유효편석계수 k$_{eff}$는 2.8로 계산되었다. 분광물성으로써 실온에서의 $^4$A$_2$$\longrightarrow$$^4$T$_2$(689.6-489.3 nm), $^4$A$_2$$\longrightarrow$$^4$T$_1$(489.3-311.33m) 천이에 의한 흡수를 확인하고, $^4$T$_2$$\longrightarrow$$^4$A$_2$(650-800 nm), $^2$E$\longrightarrow$$^4$A$_2$에 의한 nophonon line R$_1$, R$_2$(680.4, 678.5 nm) 및 $^2$T$_1$$\longrightarrow$$^4$A$_2$(655.7, 649.3, 645.2 nm)의 형광방출 스펙트럼을 얻었으며, 형광수명은 0.264 ms로 조사되었다. 제조된 레이저 발진봉은 직경 6.3 m, 길이 45 nm이었다.

• The Journal of Engineering Geology
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• v.27 no.3
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• pp.233-244
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• 2017

We conducted hydraulic fracturing experiments on cement samples to investigate the dependency of fracture propagation on the viscosity of injection fluid and the in situ stress state. Ten cubic samples (20 cm side length) were produced using cement that was cured in water for more than one month. Samples were placed in a tri-axial compression apparatus with three independent principal stresses. An injection hole was drilled and the sample was hydraulically fractured under a constant injection rate. We measured injection pressures and acoustic emissions (AE) during the experiments, and investigated the fracture patterns produced by hydraulic fracturing. Breakdown pressures increased exponentially with increasing viscosity of the injection fluid. Fracture patterns were dependent on differential stress (i.e., the difference between the major and minor principal stresses). At low differential stress, multiple fractures oriented sub-parallel to the major principal stress axis propagated from the injection hole, and in some samples the fracture orientation changed during propagation. However, at high differential stress, a single fracture propagated parallel to the major principal stress axis. AE results show similar patterns. At low differential stress, AE source locations were more widespread than at high differential stress, consistent with the fracture pattern results. Our study suggests that hydraulic fracturing during shale gas extraction should be performed parallel to the orientation of minimum differential stress.

• Journal of Korean Society of Steel Construction
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• v.12 no.3 s.46
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• pp.239-250
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• 2000

This study investigates the mechanical behavior on trough rib to crossbeam joint in orthotropic steel plate decks, specially emphasizing on the effect of diaphragm inside trough rib on the fatigue behavior of slit by static and fatigue tests. In particular, the effects of diaphragm on in-plane stress and out-of-plane stress, stress concentration, propagation of fatigue cracks at the silt are studied. With the result of experiment and numerical analysis, we have estimated the fatigue strength using the nominal stress and hot-sport stress. The details with diaphragm have occurred about 50% stress reduction at trough rib part of trough rib to crossbeam joint than the detail without diaphragm, however, the lower parts of crossbeam have occurred much more stress. Initial crack size or slit have an considerable influence on the propagation of fatigue cracks due to V-notch. The fatigue strength category of the details without diaphragm has higher value than fatigue limit, whereas that of the details with diaphragm is estimated lower than fatigue limit.

• Journal of the Computational Structural Engineering Institute of Korea
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• v.28 no.1
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• pp.1-8
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• 2015

In this paper, computational evaluation method for fatigue crack growth rate(FCGR) based on material viscoplastic-damage model is proposed. Viscoplastic-damage model expressing material constitutive behavior of 7% nickel steel is introduced and is implemented into commercial finite element analysis(FEA) code, ABAQUS, as a user defined material subroutine(UMAT) for application in the FEA environments. Verification of developed UMAT and material parameters of material model are carried out by uniaxial tensile test simulations of 7% nickel steel. Moreover, jump-in-cycles procedure and rearrangement of critical damage are employed and also implemented to the ABAQUS UMAT for fatigue damage analysis. Typical FCGR test results such as relationship between crack length and number of cycles and relationship between da/dN and ${\Delta}K$ could be obtained from FCGR test simulation using developed UMAT and these results are compared with experimental results in order to verify of proposed computational method.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.8 no.4
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• pp.645-650
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• 1998

Alumina- and yttria-coated SiC powder was prepared by the surface-induced precipitation method, and sintered properties of silicon carbide prepared from this powder were investigated. After a well dispersion of SiC powders in the aqueous solution of $Al_2(SO_4)_3$ and $Y_2(SO_4)_3$, the mixed precursors of aluminum hydroxide, aluminum carbonate, yttrium hydroxide, and yttrium carbonate were precipitated on the surfaces of SiC particles through the hydrolysis reaction of urea. SiC specimens with alumina and yttria exhibit, 97.8% of theoretical density after the sintering at $1900^{\circ}C$ for 2 hrs. During annealing at $2000^{\circ}C$, $\beta$longrightarrow$\alpha$ phase transformation of SiC had taken place and resulted with a rodlike microstructure. Toughness of sintered SiC was enhanced by crack deflection around the rodlike grains. In case of annealing less than that of 3 hr, the fracture toughness of SiC was slightly improved with increasing the amount of sintering aid. However, annealed specimens for a long time showed constant fracture toughness even though the amount of sintering aid increased. It is resulted that the main factor for toughening in annealed SiC for a long time is the pullout effect of rodlike grains during the propagation of cracks, and the amount of sintering aids is less effective on the fracture toughness of SiC.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.6 no.1
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• pp.73-87
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• 1996

The mechanical properties of 2D ceramic composites fabricated bythe newly developed powder infiltration and subsequent multiple impregnation process were characterised by both 3-point flexure and tensile tests. These tests were performed with strain gauge and acoustic emission instrument. The woven fabric composites used for the test have the basic combinations of $Al_{2}$$O_{3}$ fabric/$Al_{2}$$O_{3}$ and SiC fabric (Tyranno)/SiC. Uniaxially aligned SiC fibre(Textron SCS-6)/SiC composites were also tested for comparison, The ultimate flexural strength and first-matrix cracking stress of SiC fabric/SiC composite with 73% of theoretical density were about 300 MPa and 77 MPa respectively. However, the ultimate tensile strengths of composite were generally one third of flexural strengths, and first-matrix cracking stress in a tension test was also much lower than the value obtained from flexure test. The lower mechanical properties measured by tension test were analysed quantitatively bythe differences in stressed volume using Weibull statistics. This showed that the ultimate strength and the firs-tmatrix cracking stress of woven laminate composites were mainly determined bythe gauge length of fibres and the stressed volume of matrix respectively. Incorporation of SiC whiskers into the matrix increased first-matrix cracking stress by increasing the matrix failure strain of composites.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.19 no.1
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• pp.25-32
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• 2009

The glass-ceramics composed of coal bottom ash produced from a thermal power plant, $Na_{2}O$ and $Li_{2}O$ as a flux agent and $TiO_2$ as a nucleation agent were fabricated and its microstructures were analyzed. The nepheline was a major crystal phase in the glass-ceramics fabricated and its amount increased with $TiO_2$ addition. The glass-ceramics without $TiO_2$ addition had the thick surface crystals induced by a surface-crystallization mechanism and no crystal in the interior matrix. The surface crystallization, however, was restrained and the interior matrix was completely crystallized showing dendrite shape spread with fine particles < $1{\mu}m$ when added with $TiO_2$ above 4 wt%. For the glass-ceramics containing 6 wt% $TiO_2$, the $5{\mu}m$-long dendrite crystal; were interlocked each other which could suppress the crack propagation effectively at the external loading applied.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.28 no.1
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• pp.55-62
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• 2004

Although the previous researches evaluated the fatigue behavior of glass fiber/epoxy laminates using the traditional fracture mechanism, their researches were not sufficient to do it: the damage zone of glass fiber/epoxy laminates was occurred at the delamination zone instead of the crack-metallic damages. Thus, previous researches were not applicable to the fatigue behavior of glass fiber/epoxy laminates. The major purpose of this study was to evaluate delamination behavior using the relationship between crack length and delamination width in hybrid composite material such as Al/GFRP laminate. The details of investigation were as follows : 1) Relationship between crack length and delamination width, 2) Relationship between delamination aspect ratio and delamination area rate, 3) Variation of delamination growth rate is attendant on delamination shape factors. The test results indicated that the delamination growth rate depends on delamination width delamination aspect ratio and delamination shape factors.

• Journal of the Korean GEO-environmental Society
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• v.15 no.12
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• pp.43-51
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• 2014

Organic matter in dredged soil has a lot of engineering problem in ground including a large settlement, crack propagation, low bearing capacity and low friction angle. From an agricultural point of view, however, organic matter contributes greatly soil quality and plant health. This paper investigated the relationship between engineering and germination characteristics of stabilized mixture consisting of different ratios of organic content (0 %, 10 %, 20 %, 30 %) for recycling dredged soil including organic matter. Several series of laboratory tests such as flow test, unconfined compressive test and consolidation test were performed to find out engineering characteristics. pH, percent of germination and growth of plants were also measured to investigate the germination characteristics. The experimental results indicated that, as organic content increased, unconfined compressive stress decreased and compression and swelling indices increased. However, percent of germination and plant growth increases as organic content increases.

• Journal of the Korean Ceramic Society
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• v.36 no.1
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• pp.43-49
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• 1999

Gas pressure sintered silicon nitride based composites with 0~5wt% $\beta$-Si3N4 whiskers were prepared. The whiskers were unidirectionally oriented by a modified tape casting technqiue and green bodies with various microstructure were formed by changing stacking sequences of sheets cut from the tape. Orientations of the large elongated grains of the sample after gas pressure sintering were the same as the those of the whiskers of green body, and the sintering shrinkage and mechanical properties of sintered sample were consistent with the microstructural characteristics. In case of unidirectional samples, the sintering shrinkage normal to whisker alignment direction was larger than that parallel to the direction. The shrinkage difference inceaed as the whiskercontent increaed. As whisker content increaed, the crack length normal to and parallel to tape casting direction became shorter and larger, respectively. Although the grain size increased by th whisker addition, the flexural strength of unidirectional samples was not lower than that of smaple without the whisker. In case of crossplied and 45$^{\circ}$rotated samples, the anisotropy of mechanical preoperties disappeared.