• Journal of Sericultural and Entomological Science
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• v.48 no.1
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• pp.11-15
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• 2006

Antheraea yamamai silk fibroin powder was prepared by treatment with HCl. The prepared A. yamamai fibroin hydrolysate was characterized by gel filtration chromatography, amino acid analysis, X-ray diffractometry, circular dichroism analysis, differential thermal analysis, and thermogravimetry. The average molecular weight of A. yamamai powder was about 430 and the major amino acids composed of the powder were Ala and Ser. According to XRD analysis, A. yamamai silk powder showed sharp diffraction peaks at $2{\theta}=20.34^{\circ}\;and\;31.5^{\circ}$. CD spectrum showed a peak around 220 nm and a should 215 nm, assigned to ${\alpha}-helix\;and\;{\beta}-sheet$ structure, respectively. DSC and TGA showed that the maximum degradation temperature of powder was around $250{\sim}270^{\circ}C$. Moreover, no harmful heavy metal was contained in the A. yamamai silk fibroin hydrolysate.

• Proceedings of the Korea Information Processing Society Conference
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• 2014.11a
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• pp.703-706
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• 2014

AUOTSAR(Automotive Open system Architecture)는 자동차 ECU(Electronic Control Unit) 에 내장되는 소프트웨어에 대한 표준 구조로서, ECU 소프트웨어의 품질 향상은 물론, 개발 및 관리 비용의 절감에 기여하는 등 많은 장점을 갖는다. AUTOSAR 의 이런 장점 때문에 많은 자동차 회사들이 ECU 소프트웨어에 AUTOSAR 적용을 추진하고 있다. 이에 따라 기존 레거시 ECU 소프트웨어 시스템을 AUTOSAR 표준에 맞는 ECU 소프트웨어 시스템으로 변환하는 방법에 대한 관심도 높아지고 있다. 그 이유는 이미 많은 ECU 레거시 소프트웨어 시스템들이 개발되어 사용되고 있으며, 이들에게는 이미 기능 및 안정성 검증을 위하여 많은 시간과 비용이 투자하여 되어 있다. 따라서 ECU 소프트웨어 시스템에 AUTOSAR 를 적용하는 경우 기존의 레거시 소프트웨어 시스템을 재사용할 수 있으면 생산성 및 품질 면에서 많은 장점을 갖는다. 본 연구에서는 C 언어로 작성된 기존의 ECU 소프트웨어 시스템을 AUTOSAR 플랫폼에서 재사용할 수 있도록 하기 위하여, 기존의 레거시 ECU 소프트웨어 시스템을 AUTOSAR 플랫폼으로 마이그레이션하는 방법에 대하여 연구하였다. 마이그레이션 과정은 크게 두 단계로 나누어 지는데, 이는 레거시 소프트웨어 시스템을 분석하여 마이그레이션이 가능하도록 기능별로 분해하는 것과, 분해된 구성 요소들을 AUTOSAR 플랫폼에 맞는 구조로 재구성하는 과정이다. 본 논문에서는 이중 첫 번째 과정인 레거시 소프트웨어 시스템의 분석 및 기능별 분해 방법을 제시하고자 한다.

• Journal of the Korean Wood Science and Technology
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• v.39 no.1
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• pp.86-94
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• 2011

Pyrolytic lignin was obtained from biooil produced with yellow poplar wood. Fast pyrolysis was performed under various temperature ranges and residence times using fluidized bed type reactor. Several analytical methods were adopted to characterize the structure of pyrolytic lignin as well as the effect of pyrolysis temperature and residence time on the modification of the lignin. The yield of pyrolytic lignin increased as increasing pyrolysis temperature and decreasing residence time of pyrolysis products. The molecular weight of pyrolytic lignin determined by gel permeation chromatography (GPC) was approximately 1,200 mol/g, which was approximately a tenth of milled wood lignin (MWL) purified from the same woody biomass. Based on analytical data, demethoxylation and side chain cleavage reaction were dominantly occurred during fast pyrolysis.

• Proceedings of the Korean Vacuum Society Conference
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• 2012.08a
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• pp.183-183
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• 2012

최근 환경오염과 천연자원의 고갈로 태양광을 이용한 수소와 산소를 제조하는 광전기화학적 물분해 반응이 많은 관심을 받고 있다. 본 연구에서는 란타늄 알루미네이트 단결정 기판 위에 니오븀을 도핑한 이산화 티타늄을 증착 시킨 후 two-step sol-gel법을 이용하여 아나타제 이산화티탄늄 나노막대를 성장시켰다. 성장시킨 아나타제 티타늄산화 막대는 구조적인 특징과 모양, 크기를 전구체 용액의 수소이온화지수(pH)를 조절함으로써 변화 시킬 수 있다. 니오븀을 도핑한 이산화 티타늄 기판 위에 높은 수소이온화지수(pH 10 이상)을 이용하여 우선 배향된 아나타제 나노 막대를 성장 시킬 수 있으며, 주사전자현고해상도 투과전자현미경, x선 회절 분석기를 통해 구조적 특성을 평가하였다. 또한 수소이온화지수를 조절(pH 9)하여 만든 다결정질 아나타제 나노구형과 우선배향된 나노막대의 전하이동특성을 분석하기 위하여 기체 색층분석법(GC), 광전기화학법(PEC), 임피던스를 측정하였다.

• Environmental and Resource Economics Review
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• v.20 no.2
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• pp.255-289
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• 2011

This study made linked Energy IO Table 00-05-08 of 76 sectors in intermediate sectors and analyzed structural decomposition analysis in energy consumption change in industrial sector with both by aggregate data and micro data. Structural decomposition analysis focused value added level change, value added share change of each industry, output structural change of each industry and energy intensity change of each industry as factors. Supply side model based on Ghosh inverse matrix was applied as empirical model because Korea has export driven industrial structure. Empirical results with aggregate data showed that value added change increased energy consumption and output structural change of each industry decreased energy consumption in both 2000~2005 and 2005~2008. However value added share change and energy intensity change caused opposite direction in energy consumption change with time. Policy based on aggregate data can not evaluate effort of each industry in energy efficiency and make effective results because aggregate data delete character of each industry.

• Journal of the Korean Wood Science and Technology
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• v.42 no.3
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• pp.266-274
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• 2014

To extend the understanding of the pyrolysis mechanism of wood, we have investigated wood dust charcoal and condensate of volatile organic compounds (VOC) obtained during the pyrolysis of red pine (Pinus densiflora Sieb. et Zucc.) at $180{\sim}450^{\circ}C$ using elemental analysis, IR and GC/Mass. The effect of activation process on the charcoal structure also has been studied by comparing elemental analysis and IR data of charcoal carbonated at $600^{\circ}C$ and charcoals activated at $750^{\circ}C$. The results show that pyrolysis of wood has mainly started near at $240^{\circ}C$ and its chemical components did not changed much up to $270^{\circ}C$. However, the element contents and IR spectra drastically changed at $300^{\circ}C$. The fact that IR peaks related to the aromatic ring of lignin are observed in the charcoal pyrolized at $450^{\circ}C$ indicates that a small part of lignin still remains at this temperature. The chemical structure of the activated charcoal seems almost unaffected by the activation time.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.30 no.6
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• pp.244-250
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• 2020

β-Tricalcium phosphate (β-TCP, Ca3(PO4)2) is a kind of biodegradable calcium phosphate ceramics with chemical and mineral compositions similar to those of bone. It is a potential candidate for bone repair surgery. To improve the bioactivity and osteoinductivity of β-TCP, various ions doped calcium phosphate have been studied. Among them, Iron is a trace element and its deficiency in the human body causes various problems. In this study, we investigated the effect of Fe ions on the structural variation, degradation behavior of β-TCP. Fe-doped β-TCP powders were synthesized by the coprecipitation method, and the heat treatment temperature was set at 925 and 1100℃. The structural analysis was carried out by Rietveld refinement using the X-ray diffraction results. Fe ions existed in a different state (Fe2+ or Fe3+) with different heat treatment temperatures, and the substitution sites (Ca-(4) and Ca-(5)) also changed with temperature. The degradation rate was fastest at Fe-doped β-TCP with heated at 1100℃. The cell viability behavior was also enhanced with the substitution of Fe ions. Therefore, the substitution of Fe ion has accelerated the degradation of β-TCP and improved the biocompatibility. It could be more utilized in biomedical devices.

• Journal of Labour Economics
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• v.33 no.1
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• pp.85-107
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• 2010

In this article, since the financial crisis, Korean employment movement to service market, productivity gap between manufacturing and service industry was significant compared with other countries. The results from productivity decomposition show that negative structural changes, which employment increase is contrary to the productivity, have been intensified since the financial crisis. It is caused from a different developing pattern. While the proportion of employment was reduced, productivity has improved in manufacturing industry. While the developing was due to the high increase of the employment proportion in service industry, productivity was not improved significantly. This tendency is clearly revealed in international comparisons. In Korea the negative trend of structural changes in service industry are intensified compared to manufacturing industry after the financial crisis.

• Journal of the Korea institute for structural maintenance and inspection
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• v.17 no.2
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• pp.94-100
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• 2013

In this paper, Machinery analysis was conducted, in order to predict highest exposure temperatures and the analyze fire damage in the case of fire on reinforced concrete structure. After analyzing differential thermal of reference materials in accordance with temperature of concrete reference core specimen, it turned out that powerful endothermic peak came resulting from evaporation of capillary water and get water untill $200^{\circ}C$, another endothermic peak came resulting from decomposition of calcium hydroxide at $520^{\circ}C$, and then mass of reference materials remarkably decreased due to endothermic reaction. Another powerful endothermic reaction came after decomposition of calcite at $720^{\circ}C$. After analyzing X-ray diffraction of reference materials in accordance with temperature of concrete reference core specimen, it turned out that calcium hydroxide existed until the temperature of $400^{\circ}C$, but CH almost disappeared and CaO appeared from $600^{\circ}C$. The production increased in proportion to the temperature. This is because that calcium hydroxide and calcite are decomposed and CaO is produced when the temperature of concrete increases with fire. It is estimated that calcium hydroxide and calcite are utterly decomposed and peak disappears, and peak of CaO is remarkably formed instead, at the temperature of $700-800^{\circ}C$.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2009.05a
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• pp.235-236
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• 2009

금속 아세테이프가 금속으로 열분해하는 반응을 이용하여 템플레이트 안에 잘 정렬된 금속 나노 구조물을 얻는 것은 센서 (sensor), 분리 막(separation), 저장 장치(storage), 에너지 전환 장치 (energy conversion)에 응용이 가능하다. 실버 아세테이트와 팔라듐 아세테이트에서 순수 실버와 팔라듐 나노 구조의 제조 및 형태의 차이를 밝히는 것을 목적으로 나노 입자의 크기와 활성화 에너지가 이에 영향을 주는 것으로 확인할 수 있었다. 금속 나노 구조의 확인 및 나노입자의 크기와 활성화 에너지를 분석 관찰하기 위해 DSC, TG, XRD, FE-SEM 등을 이용하였다.