• Journal of the Korean Chemical Society
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• v.51 no.2
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• pp.165-170
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• 2007

In this work, caffeine and some catechin compounds such as +C, EGC and EGCG were extracted from green tea using quercetin molecular imprinted polymers in solid-phase extraction. For synthesis of MIP, quercetin as the templates, MAA as the monomer, EGDMA as the crosslinker and AIBN as the initiator were used. For extraction of caffeine and catechin compounds from green tea, the solid-phase extractions of a load followed by wash and elution procedures were done with water, methanol and methanol:acetic acid=90:10 (vol.%) as the solvents, respectively. HPLC analysis (C18 column, 5 μm, 250×4.6 mm) with the mobile phase of methanol:water=40:60 (vol.%) at a flow rate of 0.5 ml/min was adopted for the quantitative determination. By solid-phase extraction, the resolutions of caffeine and some catechin compounds from green tea were increased. The quercetin-MIP had higher selectivity to +C compounds.

• Journal of the Korean Arthroscopy Society
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• v.9 no.1
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• pp.51-55
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• 2005

Purpose: To compare the stability and clinical result after anterior cruciate ligament reconstructed knee after graft fixation using Intrafix in tibial tunnel with or without additional tibial post fixation. Materials and Methods: We analyzed 37 cases which were treated with four-strand hamstring tendon autograft during the period from May 2002 to January 2003. The grafts were fixed with Rigidfix system (Mitek Product, Johnson and Johnson, USA) in femur tunnel and Intrafix system (Mitek Product, Johnson and Johnson, USA) in tibial tunnel. After tibial fixation, additional tibial post fixation was done, which was determined by the serial case number prospectively. Patients were followed for average of fourteen months(range, thirteen to twenty-five months) At the time of final follow-up, patients were evaluated in terms of Lachman test, pivot shift test, Lysholm scores, IKDC (International Knee Documentation Committee) assessment, side-to-side KT-1000 maximum-manual arthrometer differences. Results: At last follow-up, Lysholm score was average 93.1(range: 65 to 98), IKDC assessment revealed that 26 cases had score of A, 10 cases had score of B and 1 case had score of C. The average maximum-manual KT-1000 arthrometer side ?to-side difference was 2.5 mm$(0{\sim}6mm)$. There was one case in which the Lachman test was graded as 2+ and four cases in which the Lachman test was graded as 1+ and the remaining thirty-two cases were normal by Lachman test. One case had a 2+ pivot-shift, and 2 cases had a 11 pivot-shift. The remaining 34 knees were normal on pivot -shift testing. The average maximum-manual KT-1000 arthrometer side-to-side difference was average 2.8 mm$(0{\sim}6mm)$ in Intrafix only group and average 2.2 mm$(0{\sim}4mm)$ in additional fixation group (P>0.05). Conclusion: Without additional tibial fixation, the stability of the anterior cruciate reconstructed knee with hamstring graft which was fixed with Intrafix was restored.

• KSBB Journal
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• v.25 no.3
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• pp.205-214
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• 2010

Many successive liquid-liquid extractions occur enabling purification of the crude material to occur. In high performance counter-current chromatography (HPCCC), crude material is partitioned between two immiscible layers of solvent phases. The stationary phase (SP) is retained by hydrodynamic force field effect and the mobile phase (MP) is pumped through the column. Purification occurs because of the different solubility of the components in the liquid mobile and stationary phases. There are many key benefits of liquid stationary phases such as high mass and volume injection loadings, total sample recovery, and easy scale-up. Many researchers showed that predictable scale-up from simple test is feasible with knowledge of the stationary phase retention for the planned process scale run. In this review we review the recent advances in HPCCC research and also describe the key applications such as natural products and synthetics (small or large molecules).

• KSBB Journal
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• v.24 no.4
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• pp.353-360
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• 2009

This study was accomplished using Anaerobic/Anoxic/Oxic upflow packed-bed column reactors with fixed media and Loop Reactor with fluidized media instead of Oxic reactor. The objectives of this study was to investigate the characteristics of organics, nitrogen and phosphorus removal from sewage with the HRT. The average removal efficiencies of $BOD_5$ and SS increase as increasing the hydraulic retention time (HRT) until 16 h of the HRT, and they were constant over 16 h of the HRT. The removal efficiency of $BOD_5$ in case of packed-bed reactor and Loop Reactor was about 86.6% and 90.9% respectively at 16 h of the HRT. The removal efficiency of SS in packed-bed reactor and Loop Reactor was about 78.0% and 88.2% respectively at 16 h of the HRT. The average removal efficiencies of $COD_{Cr}$ and $COD_{Mn}$ showed similar trends as those of $BOD_5$ and SS. At the HRT of 16 h, the removal efficiency of $COD_{Cr}$ in case of packed-bed reactor and Loop Reactor was 63.5%, 75.2% and that of $COD_{Mn}$ was 60.7%, 73.6% respectively. The average removal efficiencies of T-N and T-P increase as increasing the HRT. The removal efficiencies of T-N and T-P in Loop Reactor were 33.6% and 54.5% respectively at 16 h of the HRT and T-N and T-P were better removed in Loop Reactor. From this result, it was found that the performance of Loop Reactor was much higher than the performance of packed-bed reactor and the optimum HRT was 16 h.

• Proceedings of the KIEE Conference
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• 2003.07d
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• pp.2070-2072
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• 2003

본 연구는 3상 소형 유도전동기의 고정자 권선 고장의 효과적인 진단을 위하여 고정자 전류에 대하여 Park's Vector를 이용한 기법을 적용하였다. 본 기법은 고정자 3상 전류를 측정하여 Park's vector 변환을 통하여 직축, 횡축 전류로 변환하고 이를 이용하여 고장 진단을 위한 Park's Vector Pattern을 통하여 고장진단을 수행하였다. 제안한 방법의 유용성을 확인하기 위하여 고정자 권선 한 상에 2턴, 10턴, 그리고 20턴의 단락고장을 발생시켜 정격부하의 25%, 50%, 100%에 대하여 부하변동에 따른 각각의 단락고장의 경우와 정상 전동기의 Park's Vector Pattern 비교하였으며 그 유용성을 확인하였다.

• KSBB Journal
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• v.9 no.2
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• pp.200-210
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• 1994

In batch bioreactor fermentations for cyclosporin A (CyA) production, good potential for bioprocess improvement was demonstrated in the immobilized cell system, providing appreciably better utilization of the catalytic activity of the biomass than the freely suspended cells, especially during the exponential phase. When concentrated nutrient medium was added pulsely during the exponential phase of cell growth(at hour 139 of fermentation), reactivation and regermination in both immobilized and suspended cell cultures were observed to contribute to the longevity of CyA production, maintaining maximum CyA titre until 250 hours of fermentation. Contrarily, simple batch fermentations without any supplement of medium in both systems showed repid decrease in CyA concentrations during the late stationary phase. Notably, the CyA yield coefficient $(Y_p/x)$ for the immobilized cell system was maintained quite high even after the pulse addition of the concentrated full medium, reaching almost 80% of the level attained during the exponential phase. This is in sharp contrast when compared with the corresponding value of 58% in the case of parallel-suspended cells. This pattern of CyA production resulted in considerably enhanced CyA production in the immobilized cell system, reaching almost 2 time higher maximum CyA production in comparison with the free cell system.

• Proceedings of the KIEE Conference
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• 2008.07a
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• pp.968-969
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• 2008

본 논문에서는 유도전동기에서 발생되는 고장들 중에서 고정자 권선 단락 고장 특성 해석과 고장 판별에 대한 방법을 제시한다. 고정자 권선 단락을 판별하기 위해서 단락상태의 고정자를 모델링하여 3상 전류 불평형과 공극자속밀도에 대한 유한요소해석을 수행하였다. 유한요소해석으로 얻어진 결과의 타당성을 입증하기 위해 실험을 통하여 전류와 공극자속에 대한 유기기전력 측정값을 비교하였다. 공극자속의 유기기전력을 측정하기 위해 고정자 슬롯에 자속센서를 취부하였다. 고정자 권선 단락 시 3상 전류는 불평형을 이루고 공극자속밀도가 감소되어 유도전동기의 고정자 고장을 판별하는 기초자료가 된다.

• Nuclear Engineering and Technology
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• v.27 no.6
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• pp.898-910
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• 1995

기존경수로 핵연료의 연소도를 크게 증가시키는 고연소도 핵연료 및 미래형 핵연료에서는 연료봉의 축방향 조사성장이 증가하게 되고 이와 같이 증가된 축방향 연료봉 성장을 수용하기 위해서는 상.하단 고정체 사이의 간격이 더 필요하게 된다. 이 요구되는 상.하단고정체 사이의 축방향 공간을 얻기 위하여 기존 국산핵연료 하단고정체 유로판 및 이물질여과 하단고정체에 대하여 응력강도를 기준으로 두께최적화 계산을 수행하였다. 계산은 범용 유한요소 코드인 ANSYS 코드를 이용하였다. 이 두께 최적화에 의해 기존의 국산 17$\times$17 경수로 핵연료의 하단고정체에서는 지지 Leg의 폭과 길이를 증가시킴으로써 유로판의 두께 감소를 약 5.1mm 줄일 수 있음을 알 수 있고, DRBEP용 하단고정체에서는 약 4.6mm의 두께 감소가 가능한 것으로 해석되었다.

• Proceedings of the KIPE Conference
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• 2008.10a
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• pp.88-90
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• 2008

본 논문에서는 유도전동기에서 발생되는 고장들 중에서 고정자 권선 단락 고장 특성 해석과 고장 판별에 대한 방법을 제시한다. 고정자 권선 단락을 판별하기 위해서 단락상태의 고정자를 모델링하여 3상 전류 불평형과 공극자속밀도에 대한 유한요소해석을 수행하였다. 유한요소해석으로 얻어진 결과의 타당성을 입증하기 위해 실험을 통하여 전류와 공극자속에 대한 유기기전력 측정값을 비교하였다. 공극자속의 유기기전력을 측정하기 위해 고정자 슬롯에 자속센서를 취부하였다. 고정자 권선 단락 시 3상 전류는 불평형을 이루고 공극자속밀도가 감소되어 유도전동기의 고정자 고장을 판별하는 기초자료가 된다.

• Environmental engineer
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• s.18
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• pp.35-37
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• 1988