• Title/Summary/Keyword: 고온자전합성법

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Preparation and thermodynamics consideration of MgO-Al spinel by self-propagation high- temperature synthesis (자전고온연소합성법에 의한 MgO-Al 스피넬 제조 및 열역학적 고찰)

  • Byun, Hun-Soo;Choi, Tae-Hyun
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.8 no.4
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    • pp.573-580
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    • 1998
  • Self-propagating high temperature synthesis (SHS) technique was used to synthesize the spinel phase of $MgAl_2O_4$ from MgO and Al powder. Thermit reaction products of MgO and Al, The reaction products were heat treated at the temperature $800^{\circ}C$ preheating. Processing factors such as DTA/TG, combustium product and maxium temperature, synthesis of MgO and Al from "$MgO+2Al+3/2O_2$\rightarrow$MgAl_2O_4$". An activation energy (${\Delta}H^{\circ}$)-264.8 kcal/mol and reaction of maxium temperature 5634 K was calculated to form a $MgAl_2O_4$ spinel from unreacted materials. Pellet were increased volume 6% after thermit reaction. reaction.

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An Update Technology Trend in Iron Oxide (산화철의 기술개발동향)

  • Sohn Jin-Gun
    • Resources Recycling
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    • v.12 no.6
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    • pp.3-7
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    • 2003
  • For the manufacture of iron oxide, the hydro-process and the pyre-process are conventionally used. Both processes use a huge amount of chemicals in reaction which affect the environment harmfully. This paper introduced the new environment friendly processes; the bio-chemical process and the self propagating high temperature synthesis process.