• Title/Summary/Keyword: 결정소성학

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A thermoelastic simulation on the (100) Si-wafer ((100) 실리콘 웨이퍼에 대한 열탄성모사)

  • Doo Jin Choi;Hyun Jung Woo
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.4 no.1
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    • pp.71-75
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    • 1994
  • In this study, a thermoelastic stress index of (100) oriented single crystalline silicon wafer and a relationship between thermal stress and critical plastic deformation temperatures were simulated. The simulated results for the thermoelastic stress index indicated a maximum value on <110> direction and a minimum on <100>. Then, it could be predicted that silicon wafer is plastically deformable over 1000 K, based on the relationship between the thermal stress derived from the thermoelastic stress index and the critical plastic deformation temperature.

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Evaluation of Plastic Anisotropy in the Steel Sheets Using EMAT (EMAT를 이용한 판재의 소성이방성 평가)

  • Ahn, B.Y.;Kim, Y.G.;Lee, S.S.
    • Journal of the Korean Society for Nondestructive Testing
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    • v.17 no.4
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    • pp.270-277
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    • 1997
  • Plastic anisotropy is one of important factors which determine the drawability of a steel sheet. It has been mainly measured by mechanical tensile test. From the ultrasonic velocities propagating along the relative directions to the rolling direction, CODF(crystallite orientation distribution function) can be measured and ODC's(orientation distribution coefficients) has some correlations with the plastic anisotropy. In this study the correlations between the plastic anisotropy and ODC's of the cold rolled steel sheet were measured. From the results of ultrasonic velocity measurements the average normal anisotropy, $\bar{\gamma}$ and the average planar anisotropy, ${\Delta}r$ could be predicted within the accuracy of ${\pm}0.082$ and ${\pm}0.096$, respectively. Acoustic resonance method was applied to measure the ultrasonic velocities and EMAT's were used for generating and detecting the ultrasonic waves.

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The study on the burnability of domestic fly ash and Japanese fly ash as a cement raw material (시멘트 원료로서 국내산 석탄재와 일본산 석탄재의 소성성 비교 연구)

  • Yoon-Cheol Lee;Se-Yong Lee;Kyung-So Min;Seok-Je Lee;Tae-Gyun Park;Dong-Woo Yoo
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.33 no.6
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    • pp.210-215
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    • 2023
  • Raw mix burnability is an especially crucial factor in cement manufacturing technology, and it depends on the physical, chemical and mineralogical properties of each raw material. In this article, we compared the difference of burnability between the domestic and Japanese fly ash as cement raw materials by using Lafarge and Polysius evaluation method. Regardless of the type or amount of fly ash used, it was found to be more combustible when using fly ash. In both case, burnability improves as the amount of fly ash increases, especially the improvement in bunarbility is remarkable up to 3%. In conclusion, as the amount of fly ash increases within the range allowed by cement quality, burnability of raw materials improves, and thus the fuel cost required for the firing of clinker can also be expected to be reduced.

Physicochemical properties and sintering behavior of pottery stone as a raw material in porcelain products (국내 도석 광물의 물리화학적 물성 및 도자기 원료로서 소결 특성 평가)

  • Kim, Jong-Young;Kim, Ung-Soo;Hwang, Kwang-Taek
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.29 no.5
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    • pp.192-202
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    • 2019
  • Physicochemical properties and sintering characteristics of pottery stone (Taebaek, Haenam, Aphae, Haengnam) were evaluated as a raw material for porcelain products. Due to acid leaching procedure, the concentration of iron oxide ($Fe_2O_3$) was decreased to < 1.0 wt%, which affects the whiteness of sintered samples. Mean particle size of acid leached samples is $5.7{\sim}10{\mu}m$ with narrow particle size distribution (PSD), which is lower than that of the pristine ($8{\sim}18{\mu}m$) with broad PSD. According to phase analysis by X-ray diffraction, most of pottery stones (PS) have Quartz phase as a main phase with Pyrophyllite as a second phase, however, Haenam PS shows halloysite phase. The absorption rate was in order of Taebaek (A, B, C)~Aphae (A, B) < Taebaek (Special A) < Haengnam < Haenam, and the samples sintered in reductive atmosphere showed lower absorption rate. This result might be due to the concentration of feldspar contained in PS, working as a flux in sintering process. Comparing the color of the sintered samples, the whiteness of refined PS (Taebaek special A, Haenam, Hangnam) is higher than acid leached PS (Taebaek A/B/C, Aphae A/B). The whiteness (L*) for refined PS is 95~97 %, which is higher than acid leached (82~96 %). This might be due to lower iron oxide concentration of the refined PS (0.11~0.58 %) than those of the acid leached PS (0.41~1.91 %) even though most of iron oxide was removed by acid leaching.

Finite Element Analysis for Rate-Independent Crystal Plasticity Model (속도 독립성 결정소성모델의 유한요소해석)

  • Ha, Sang-Yul;Kim, Ki-Tae
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.33 no.5
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    • pp.447-454
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    • 2009
  • Rate-independent crystal plasticity model suffers from the non-uniqueness of activated slip systems and the determination of the shear slip rates on the active slip systems. In this paper, a time-integration algorithm which circumvents the problem of the multiplicity of the slip systems was developed and implemented into the user subroutine VUMAT of a commercial finite element program ABAQUS. The magnitude of the slip shears on the active slip systems in f.c.c Cu single crystal aligned with the specific crystallographic orientation was investigated to validate our solution procedure. Also, texture developments under various deformation modes such as simple compression, simple tension and plane strain compression were compared with the results of the rate-dependent model by using the rate-independent crystal plasticity model. The computation time employing the rate-independent model is much more reduced than the those of the rate-dependent model.

특집: 미래주도형 성형공정과 수치 해석기술 - 판재의 이방성과 집합조직

  • Jo, Jae-Hyeong
    • 기계와재료
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    • v.23 no.3
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    • pp.82-95
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    • 2011
  • 다결정압연판재는 열가공공정을 거쳐서 생산되므로 공정의 특성을 반영하는 미세조직/집합조직 특성을 가지게 된다. 결정립들은 특정방향으로 배향하고 결정립의 형상과 크기도 변화한다. 이러한 변화는 거시적으로 다결정판재의 이방성으로 귀결이 되는데, 근본적으로 판재를 구성하는 단결정들의 기계적 물성이 각각의 방향별로 이방성을 띄기 때문이다. 본 자료에서는 압연공정시 다결정판재의 수직/평면이방성의 발생원인을 집합조직과 결정소성학을 이용하여 제시하고자 하였다.

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Microwave Sintering Behavior and Electrical Properties of BaTiO$_3$ Ceramics (BaTiO$_3$ 세라믹의 마이크로파 소성 및 전기적 특성)

  • Bai, Kang;Kim, Ho-Gi
    • Journal of the Korean Ceramic Society
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    • v.35 no.11
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    • pp.1203-1211
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    • 1998
  • The microwave sintered BaTiO3 samples were obtained by using the microwave sintering device which can precisely control the sintering temperature and the sinter time by using IR optical thermometer and PID temperature controller. During microwave sintering the internal temperature of samples were mesur-ed by the optical fiber thermometer to compare the sintering behaviors between microwave- and con-ventionally sintered ones. The former showed the faster rate of grain growth with sintering time and the larger grain size than the latter. Also they showed the similar pattern of dielectric properties with tem-perature changes from 2$0^{\circ}C$ to 16$0^{\circ}C$.

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Fabrication and Characteristics of Sensing Materials for BaTiO3 Gas Sensors (BaTiO3가스센서 감지물의 제조와 특성 연구)

  • 서동진;장경욱;임실묵;김좌연;최병현;박경순
    • Journal of the Korean Ceramic Society
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    • v.40 no.12
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    • pp.1177-1182
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    • 2003
  • The porous sensing materials for BaTiO$_3$ gas sensors were fabricated by adding the graphite powders. The crystalline structure and microstructure of the porous BaTiO$_3$-based ceramics were studied. All the sintered bodies showed a tetragonal perovskite structure. The porosity increased with increasing graphite contents. This is mainly due to an enhanced evolution of CO and $CO_2$ gases resulting from the exothermic reactions of graphite and oxygen during the sintering. It was found that the discrepancy in the resistivities measured in air and CO atmospheres at high temperatures (>∼20$0^{\circ}C$) became remarkable with increasing temperature. The sensitivity of CO gas increased with porosity, since the reactions between CO gas and $O_2$$^{[-10]}$ and between CO gas and $O^{[-10]}$ are active due to the formation of many reaction sites. The porous BaTiO$_3$-based ceramics could be promising as a sensing material for CO gas sensors.

Factors Influencing the Strength of Alumina Ceramic shell Molds Bound with Colloidal Silica (콜로이달 실리카로 결합된 알루미나 세라믹 쉘 몰드의 강도에 미치는 요인)

  • Gang, Jong-Bong;Mun, Jong-Su;Jo, Beom-Rae;Choe, Seung-Ju;Kim, Hak-Hak
    • Korean Journal of Materials Research
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    • v.6 no.12
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    • pp.1179-1185
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    • 1996
  • 고온용 세라믹 쉘 몰드를 용융 알루미나와 콜로이달 실리카를 사용하여 제조한 후, 세라믹 쉘 몰드의 강도에 영향을 주는 요인을 분석하였다. 세라믹 쉘 몰드의 강도는 바인더의 실리카 입자의 크기가 작을수록 크며 또한 실리카 농도에 비례하여 증가함을 보이며 저온에서의 강도 발현은 콜로이달 실리카의 필름 형성에 의한 입자들의 결합임을 알 수 있었다. 세라믹 쉘 몰드의 소성 강도는 부착 스타코의 크기가 작을수록 크며 소성 온도에 비례하여 증가함을 보였다. 고온에서의 강도 발현은 알루미나 입자와 콜로이달 실리카 바인더의 결합뿐만 아니라 알루미나 입자사이의 결합도 영향을 줌을 알 수 있었다. 쉘 몰드의 결정상은 130$0^{\circ}C$이하에서 소성한 경우 $\alpha$-알루미나만 존재함을 보여 실리카는 비정질로 계속 남아 있음을 알 수 있고 140$0^{\circ}C$ 이상에서 소성한 경우 뮬라이트가 생성됨을 보였다.

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Characterization of artificial aggregates fabricated with direct sintering method (직화소성법으로 제조된 인공골재의 특성 분석)

  • Kim, Kang-Duk;Kang, Seun-Ggu
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.21 no.1
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    • pp.34-40
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    • 2011
  • The bulk density, water absorption and microstructure of the artificial aggregates were controlled as a function of sintering temperature (1100 and $1200^{\circ}C$) and time (10~60 min) in the fabrication process of the artificial aggregates by the direct sintering process using dredged soil, the inorganic wastes. Also, the physical properties of the artificial aggregates fabricated according to the different sintering methods such as the direct sintering method used in this study and the increasing temperature sintering method used in the previous report, were compared and analysed. The bulk density of aggregates sintered at $1200^{\circ}C$ by the direct sintering method showed below 1.0, and the thickness of a shell and the pore size of the black core were increased with sintering temperature. Also, in the same sintering temperature, the area of black core was decreased, the thickness of shell was increased and the water absorption was decreased with sintering time. The black core of artificial aggregates of bulk density below 1.0 had the similar microstructure, regardless of sintering methods. In contrast, the shell of aggregates fabricated by the increasing temperature sintering method showed more dense microstructure than that by direct sintering method, hence the water absorption of aggregate sintered using direct sintering was relatively high. Thus, the direct sintering method is suitable for fabrication of artificial aggregates in ceramic carriers or absorbents applications.