• Title/Summary/Keyword: 검출기 감도

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가속기질량분석기술(加速器質量分析技術)(AMS)의 원리(原理) 및 응용(應用)

  • Park, Geung-Sik;U, Jeong-Ju
    • Analytical Science and Technology
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    • v.7 no.3
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    • pp.1069-1084
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    • 1994
  • 수 MV급 탄뎀형 가속기와 정전형, 자장형 질량분석기를 결합함으로써 존재비가 극히 작은 동위원소 측정이 가능해진다. 수 MeV로 가속이 되면 분해에 방해가 되는 모든 분자이온들이 제거되며, 탄뎀형 가속기에서는 음이온으로부터 가속이 개시되므로 몇몇 음이온을 형성하지 못하는 동중원소의 간섭으로부터 자유로워지기 때문에 고감도분석이 실현될 수 있다. 이외에 음이온을 형성하는 동중원소들은 주로 이온함인 최종 검출기에서의 유효 전하에 따른 에너지손실 차이를 이용하여 효과적으로 제거할 수 있다. 현재는 주로 장반감기 방사성동위원소인 $^{10}Be$, $^{14}C$, $^{26}Al$, $^{36}Cl$$^{129}I$ 등의 측정법이 확립되어 천연시료 중에서 동위원소 존재비 $10^{-12}$에서 $10^{-15}$까지의 정량이 가능하며, 원자수로 환산한 검출하한을 $10^5$개가 된다. 또한 해당 원소를 기준으로 소요 시료량은 대부분 mg 정도로 충분하다. 지금까지는 불가능했던 이러한 특징으로 인해 지난 수년간 AMS(Accelerator Mass Spectrometry)가 활용되어 온 연구분야는 지구과학(기후학, 우주화학, 빙하학, 수문학, 해양학, 퇴적학, 화산학 및 광물탐사), 인류 및 고고학(연대측정), 그리고 물리학(천체물리, 핵 및 입자물리) 등으로 다양하다. 이외에 생의학 및 재료과학 분야에서도 AMS를 활용하고자 하는 노력이 계속되고 있다. 본 해설에서는 가속기질량분석기술의 특징, 원리, 장치 및 활용분야 등을 소개하고자 하며, 이로써 관련 분야의 연구 활성화에 기여하고자 한다.

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전계방출 전자원을 이용한 SEMAP(Scanning Electron Microscopy with Polarization Anlysis) 개발

  • Lee, Sang-Seon;Kim, Won-Dong;Hwang, Chan-Yong
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.02a
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    • pp.581-581
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    • 2012
  • 나노스케일에서의 자구체(magnetic domain), 자화벽(magnetic domain wall)에 대한 연구가 활발하게 진행되고 있으며 특히 자화벽의 위치를 임의로 제어할 수 있는 기술을 응용한 메모리 소자에 대한 연구가 활발하다. 반면에 이러한 연구에 필수적인 자구체, 자화벽 이미징 장비는 매우 미비한 상황이다. 이와 같은 자성이미징(magnetic domain image), 자화벽(magnetic domain wall)을 연구하는데 있어 가장 핵심적인 장비가 SEMPA(Scanning Electron Microscopy with Polarization Analysis)이다. 일반적으로 SEM의 경우 고 에너지 빔의 전자 빔을 주사 시키고 이때 발생되는 이차 전자의 수를 2차원상의 영역에 따라 달라지는 비로 형상을 측정하게 된다. 이때 전자의 수 뿐만 아니라 이들의 spin polarization을 측정할 수 있다면 형상뿐 만 아니라 표면에서의 스핀 상태를 동시에 측정할 수 있게 된다. 기 개발된 W-filament source를 이용한 SEMPA는 field emission source에 비하여 전자빔의 세기가 약하며 이차 전자의 수도 적어 spin polarization 감도가 현저히 떨어진다. 또한 초고진공($1{\times}10^{-10}torr$)에서 사용할 수 없어 측정시료의 contamination을 방지할 수 없다. 이러한 문제점들을 보안하기 위하여 field emission source를 이용한 FE-SEMPA를 개발 중이며 2차전자의 spin polarization감도를 증가시키기 위하여 monte carlo simulation과 전산시늉등울 통해 스핀 검출기를 개발 및 연구결과를 발표하고자 한다.

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Permanent Magnet Synchronous Motor Dirve based on Maximum Torque Sensitivity (영구자석 동기전동기의 최대 토오크 감도운전)

  • 윤병도;김기용;이병송
    • The Proceedings of the Korean Institute of Illuminating and Electrical Installation Engineers
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    • v.5 no.1
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    • pp.46-56
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    • 1991
  • In this paper, the variable speed control of permanent magnet synchronous motor driven by a sinus¬oidal PWM inverter based on maximum torque sensitivity is presented. The developed torque or speed control is achieved by the field orientation technique. For the field orientation, the resolver is used as the rotor positioning sensor mounted on the motor shaft without pull-out of the synchonism at any speed. To show the validity of proposed control method, the simulation and experimental results are provided. The advantages of the proposed control method are to achieve the fast current and speed responses.

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Vital Sign Sensor Based on Second Harmonic Frequency Drift of Oscillator (발진기의 2채배 고조파 주파수 천이를 이용한 생체신호 측정센서)

  • Ku, Ki-Young;Hong, Yunseog;Lee, Hee-Jo;Yun, Gi-Ho;Yook, Jong-Gwan;Kim, Kang-Wook
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.27 no.3
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    • pp.299-306
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    • 2016
  • In this paper, a vital sign sensor based on impedance variation of resonator is proposed to detect the respiration and heartbeat signals within near-field range as a function of the separation distance between resonator and subject. The sensor consists of an oscillator with a built-in planar type patch resonator, a diplexer for only pass the second harmonic frequency, amplifier, SAW filter, and RF detector. The cardiac activity of a subject such as respiration and heartbeat causes the variation of the oscillation frequency corresponding impedance variation of the resonator within near-field range. The combination of the second harmonic oscillation frequency deviation and the superior skirt frequency of the SAW filter enables the proposed sensor to extend twice detection range. The experimental results reveal that the proposed sensor placed 40 mm away from a subject can reliably detect respiration and heartbeat signals.

Development and Characteristic Study of a Portable Gas Chromatography (소형 GC 모듈의 개발 및 특성)

  • Lee, Myeong-Gi;Oh, Jun-Sik;Jung, Kwang-Woo
    • Journal of the Korean Chemical Society
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    • v.55 no.2
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    • pp.157-162
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    • 2011
  • In the present study, we developed a portable GC module for real-time, quantitative determinations of gas mixtures in air sample. Capillary or packed column was coiled together with a heater wire and thermocouple in a small case. Together with the small and light weight sensors and valves as well as the rechargeable carrier gas canister, which permits collection and separation of samples, this system can determine the components of complex mixtures of air contaminants at low concentrations with a duty cycle of 10 min. When measured the various samples with a FID and TCD, the system showed, for a capillary column, a good resolution (R=8.3), high sensitivity, reproducibility, and linear dynamic range greater than three orders of magnitude. These results indicate that the portable GC module is expected to be used for a wide range of applications, particularly for in situ environmental monitoring, chemical processes, and regulation of contaminant emission.

Thermoluminescent Response of Thin LiF:Mg,Cu,Na,Si Detectors to Beta Radiation (얇은 LiF:Mg,Cu,Na,Si 검출기의 베타선장에 대한 TL 반응)

  • Nam, Y.M.;Kim, J.L.;Chang, S.Y.;Cho, H.W.;Kim, H.J.
    • Journal of Radiation Protection and Research
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    • v.24 no.1
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    • pp.39-43
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    • 1999
  • Thermoluminescent (TL) response characteristics of a thin LiF:Mg,Cu,Na,Si Teflon detectors have been studied for use in beta radiation detection. The detectors were fabricated from a mixture of LiF:Mg,Cu,Na,Si phosphor and Teflon powder which was molded into a thin disk form of $50mg/cm^2$ thickness. These detectors were irradiated to beta fields of $^{147}Pm,\;^{204}Tl\;and\;^{90}Sr/^{90}Y$ sources with a covering of Kapton foil ($2mg/cm^2$) and photon irradiation was carried out with a $^{137}Cs$ source at the Korea Atomic Energy Research Institute (KAERI). Batch uniformity was estimated to be 4.7% and the beta dose response presented linear relationship from 0.1 mGy to 100 Gy. The beta energy responses of thin detectors normalized to $^{137}Cs$ were presented as 0.46, 1.09 and 1.06 for $^{147}Pm,\;^{204}Tl\;and\;^{90}Sr/^{90}Y$ beta rays, respectively. The evaluated values for angular responses were $0.93{\pm}0.03\;(^{147}Pm),\;0.94{\pm}0.04\;(^{204}Tl),\;and\;0.92{\pm}0.05\;(^{90}Sr/^{90}Y)$. The results satisfied well a proposed ISO Standard for beta ray dosimeters.

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Simple Analytical Method for Acrylamide in the Workplace Air Adsorbed by Charcoal Tube (활성탄관을 사용하여 포집한 작업환경 공기중 아크릴아마이드의 분석법)

  • Yang, J.S.;Lee, M.Y.;Park, I.J.;Kang, S.K.
    • Analytical Science and Technology
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    • v.11 no.2
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    • pp.139-144
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    • 1998
  • For the ambient monitoring of acrylamide, the adequate condition of sampling and analysis was checked. The adequate adsorbents and desorption solvents were tested. The combination of charcoal tube as a adsorbent and acetone as a desorption solvent showed 87% desorption efficiency. Flame ionization detector was used to detect acrylamide. The detection limit was 0.814 mg acrylamide in 1 L acetone. It is the equivalent concentration of 0.0203 mg acrylamide in $1m^3$ air if the volume of air collected was 40L. The permissible exposure level (PEL) of acrylamide in the workplace air recommended by Occupational Safety and Health Administration (OSHA, USA) is 0.3 mg acrylamide in $1m^3$ air. So, it is very simple and economic analytical method for acrylamide to be set in the industrial hygiene laboratories.

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The Intrusion sensor using the variations of speckle patterns (스페클 패턴을 이용한 침입자 센서)

  • Park, Jae Hui;Gang, Sin Won
    • Journal of the Institute of Electronics Engineers of Korea SD
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    • v.38 no.3
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    • pp.82-82
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    • 2001
  • 스페클 패턴은 다중모드 광섬유 내를 전파하는 모드 사이의 간섭현상 때문에 발생하는 검은 무늬로서, 외부 섭동 (perturbation)의 크기에 따라 패턴이 바뀌게 된다. 이 현상을 이용하여 본 연구에서는 스페클 센서를 제작하여 실험을 통해 시설물을 원거리, 실시간 원격 감시가 가능하고 매우 민감한 침입자 센서로 응용 가능함을 확인하였다. 본 연구에서는 감도를 높이고 구조를 간단하게 하기 위해, 공간필터를 사용하는 대신 광검출기 홀더를 길이 가변이 가능하도록 지그를 제작하여 사용하였으며, 정류기와 FVC를 사용하여 외부 섭동의 지속시간과 크기를 알 수 있었다.

A Study on the Design and Implementation of FH Frequency Synthesizer for GSM Mobile Communication (GSM 이동통신을 위한 FH 주파수 합성기 설계 및 구현에 관한 연구)

  • 이장호;박영철;차균현
    • The Journal of Korean Institute of Communications and Information Sciences
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    • v.17 no.2
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    • pp.168-180
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    • 1992
  • Commumication technology has been continuously developed to overcome the distance and time for the transmission of information to the human society. Wireless mobile communication, which had been used mostly in the military and police is widely used these days for enterprise and individuals. Therefore the domestic usage of the advanced mobile phone service are progressively gaining wide popularity. The modulation techniques used usually in mobile communications were the analog techniques such as AM and FM, but they are getting replaced by the digital techniques, However, the major disadvantage of the digital communications is the increase of the transmission bandwidth. Therefore, it is very important to use efficiently the limited frequency bandwidth. The domestic research and development on the subject seems quite limited and in order to establish the technology of the digital mobile communications. This thesis presents the design of the frequency hopping synthesizer providing 124 channels with a channel spcing of 200KHz. VCD used in the synthesizer employs a semi-rigid cable for higher purity of signal spectrum, and a hybrid pgase detector is realized with a sample hold phase detector in conjuction with a tri-state phase detedctor.

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Detection of Elastic Waves Using Stabilized Michelson Interferometer (광로차 보상회로가 부착된 마이켈슨 간섭계에 의한 탄성파 신호검출)

  • Kim, Y.H.;So, C.H.;Kwon, O.Y.
    • Journal of the Korean Society for Nondestructive Testing
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    • v.13 no.4
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    • pp.32-41
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    • 1994
  • The stabilized Michelson interferometer was developed in order to measure micro dynamic displacement at the surface of solids due to elastic wave propagation. The stabilizer was designed to compensate light path disturbances using a reference mirror driven by piezoelectric actuator. Using stabilizer, the effect of external vibration was reduced and the quadrature condition was satisifed. As the results, the output of photodetector had maximum sensitivity and linearity. The minimum detectable displacement was 0.3nm at the band width of 10 MHz. The epicentral displacements due to the glass capillary breaks and the steel ball drop impact were measured using the developed interferometer and the results were compared with the calculated one.

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