• Journal of Conservation Science
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• v.27 no.4
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• pp.395-401
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• 2011

After pressurized impregnation treatment, which has been proposed as an effective conservation method for stone cultural property, was executed with methyl metacrylate (MMA), MMA-butyl acrylate (PMB73) mixture and MMA-vinyl trimethoxy silane (PMV5) co-monomer mixture, the physical-chemical properties on the sand stone and the granite impregnated were evaluated. Compared to the case of granite, the impregnation ratios of sand stone showed larger values in the range of 3.2 to 3.7 wt% and these were increased up to 32% when the decompression process was applied to autoclave. The physical properties of sand stone such as anti-moisture property, flexural strength, impact property and ultrasonic velocity were also higher values than those of granite, which can be interpreted by high impregnation ratio resulted in many void within sand stone. The impact failure energy was 1.22 J for PMMA, 1.84 J for PMB73, and 2.8 J for PMV5, respectively. Since the inorganic affinity of treatment agent is more effective than the molecular structure of acrylic agent, PMV5 improved inorganic property indicates the optimum impact property.

• Journal of the Korean Wood Science and Technology
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• v.43 no.6
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• pp.792-797
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• 2015

In this study, three softwood species were treated with water-soluble melamine resin by different concentration and treatment time under vacuum pressure for improving mechanical property, abrasion resistance, and incombustibility. After the treatment, a compreg was manufactured and then evaluated on physical properties. Additionally, incombustibility of compreg was determined by comparing with a wood that was treated by spraying a water-soluble fire retardant on surface. As concentration of resin increased, bending strength and Brinell hardness increased as well as abrasion resistance, but there was no correlation on treatment and mechanical properties by treatment time. The wood impregnated by water-soluble melamine resin under vacuum pressure showed better incombustibility than that of a water-soluble fire retardant sprayed wood. Therefore, this treatment could be used for improving incombustibility of wood.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2001.05a
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• pp.184-188
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• 2001

The squeeze infiltration process is potentially of considerable industrial importance. The performance enhancements resulting from incorporation of short alumina fiber into aluminum are well documented. These are particularly significant for certain automobile components. But the solidification process gets complicated with manufacturing parameters and factors for porosity formation do not fully understand yet. In this study porosity defects were observed under several infiltrating conditions ; a kind of matrix, an initial temperature of melt, and a volume fraction of reinforcement. The desimetry and the microscopic image analysis were done to measure the amount of porosity. A correlation between manufacturing parameters and defects was investigated through these.

• Korean Journal of Materials Research
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• v.7 no.5
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• pp.397-402
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• 1997

석탄계 핏치의 열처리 온도 및 압력에 따른 결정화도와 기공도 그리고 산화저항성 등을 관찰하였으며, hexagonal type 4D 탄소/탄소 복합재를 석탄계 핏치로 가압함침 및 탄화시킨 다음 가해준 압력이 고밀도화에 미치는 영향을 관찰하였다. 석탄계 핏치의 가압탄화 압력이 흑연화도에 크게 영향을 미치지 않았으며, 기공면적비에 있어서는 압력을 600bar로 상승시켜 줌으로써 상압 처리한 경우 보다 1.5배 정도 감소 하였다. $650^{\circ}C$까지 열처리하여 얻은 코우크스의 산화반응 개시온도는 처리압력이 증가함에 따라서 지연되었다. 탄소/탄소 복합재의 함침압력을 100bar에서 600bar로 상승시켜 줄 경우 밀도 증가율이 크게 향상 되었으며 기공도는 감소하였다.

• Fire Science and Engineering
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• v.26 no.4
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• pp.18-23
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• 2012

After produce the extracted wood to silicic acid gel, sodium carbonate and silicon dioxide with application of the making method for carbon dioxide, ignition time, ignition temperature, mass loss rate and critical heat flux are measured according to external radiation source (20, 25, 35 and 50 $kW/m^2$). From the results, pressure impregnation wood to use with water glass and carbon dioxide has fire retardant performance at heat flux (less than 20 $kW/m^2$) of Pre-Flashover fires. If we find out the excellent maxing ratio through continuously study, it might be decided to be able to be utilized as fire-retardant wood.

• Journal of the Korean Wood Science and Technology
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• v.43 no.3
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• pp.327-333
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• 2015

To measure the dimensional stability of three softwoods by vacuum pressurization of water soluble melamine-formaldehyde (MF) resin impregnation process, properties of resin treated compressed woods (compregs) were measured after impregnating the water soluble MF resin into three coniferous wood species for different impregnation times and resin concentrations. As the resin concentration was higher and impregnation time was longer, coefficients of volumetric shrinkage and anti-volumetric swelling efficiency increased, but coefficients of volumetric swelling, anti-volumetric swelling efficiency and absorption decreased. Also, weight percent gain increased remarkably as the resin concentration was high, but there was no uniform relationship with impregnation time.

• Korean Journal of Materials Research
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• v.5 no.5
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• pp.611-619
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• 1995

PAN계 탄소섬유와 페놀수지를 이용하여 rod를 인발성형 한 후, 다른 섬유분율을 갖는 두종류의 hexagonal type 4D 프리폼을 제작하였다. 석탄계 핏치를 가압함침 탄화공정을 통하여 함침한 후 탄화와 고온열처리를 하였다. 이와 같은 공정을 반복하여 고밀도화된 4D CRFC를 제조하였다. 열충결 시험 후 새로운 크랙이 생성되었을 뿐만 아니라 기존의 크랙이 확장되었으며 이와 같은 크랙들은 공기와의 접촉면을 제공하여 중량감소를 보였다. 공기 산화 저항성을 고온열처리 공정을 거친 것이 약 20% 우수하게 나타났다. 4D CFRC의 밀도와 섬유의 분율이 높을 수록 삭마 저항성이 커지고, 삭마량은 시간에 따라 선형적으로 증가하였으며 type II가 type I보다 삭마저항성이 우수하였다. 삭마 메카니즘을 관찰한 결과 1차적으 기질의탈리가 먼저 일어난 다음 섬유가 삭마되었다.

• Composites Research
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• v.30 no.3
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• pp.209-214
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• 2017

Titanium carbide (TiC) reinforced SKD11 matrix composites were successfully fabricated by a novel liquid pressing infiltration process. Microstructure, mechanical properties, and wear characteristics of the fabricated 60 vol% TiC-SKD11 composite are analyzed. The composite exhibits superior mechanical properties, such as hardness and compressive strength with 24% lower density as compared with SKD11. Improved wear resistance of the TiC-SKD11 composite originates from uniformly reinforced TiC having strong interfacial bonding strength between TiC/SKD11 interface.

• Composites Research
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• v.32 no.3
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• pp.158-162
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• 2019

Titanium carbide (TiC) reinforced Inconel 718 matrix composites were successfully fabricated by a novel liquid pressing infiltration process. Microstructure and mechanical properties of the fabricated 55 vol% TiC-Inconel 718 composite are analyzed. The composite exhibits superior mechanical properties, such as hardness and compressive strength as compared with Inconel 718. It is believed that Mo and Nb, which are alloying elements in the matrix, diffuse and solidify into the TiC reinforcement, resulting in generation of core-rim structure with excellent interfacial properties.

• Composites Research
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• v.31 no.4
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• pp.117-121
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• 2018

Various ceramic particulate such as TiC, $TiB_2$, $Al_2O_3$ reinforced SUS431 matrix composites were successfully fabricated by a novel liquid pressing infiltration process. Microstructures of the SUS431 composite were analyzed to determine manufacturability of composites. $Al_2O_3$-SUS431 composite had lots of defects due to poor wettability between the $Al_2O_3$ and steel matrix. On the other hand, TiC was uniformly dispersed in the SUS431 matrix than $TiB_2$ and $Al_2O_3$ due to good wettability and interfacial properties.