• Textile Coloration and Finishing
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• v.30 no.3
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• pp.180-189
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• 2018

To study the effect of stereoisomeric structures of curing agents on curing behaviors, thermal and mechanical properties of epoxy resins, DGEBA(diglycidyl ether of bisphenol A) epoxy resin and 3,3'- and 4,4'-DDS(diaminodiphenyl sulfone) curing agents were selected. The curing initiation temperature and activation energy of DGEBA/3,3'-DDS was lower than DGEBA/4,4'-DDS. DGEBA/3,3'-DDS has a faster curing rate and higher degree of cure than DGEBA/4,4'-DDS, suggesting that 3,3'-DDS has higher reactivity than 4,4'-DDS. Tensile strength and fracture toughness of DGEBA/3,3'-DDS was lower than those of DGEBA/4,4'-DDS, indicating that mechanical properties of the epoxy resin can be different only by the stereoisomeric difference in chemical structure of the curing agent.

• Transactions of Materials Processing
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• v.13 no.1
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• pp.15-20
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• 2004

In order to evaluate spring-back behavior in automotive sheet forming processes, a panel shape idealized as a double S-rail has been investigated. After spring-back has been predicted for double S-rails using the finite element analysis, results has been compared with experimental measurements for three automotive sheets. To account for hardening behavior such as the Bauschinger and transient effects in addition to anisotropic behavior, the combined isotropic-kinematic hardening law based on the Chaboche type model and a recently developed non-quadratic anisotropic yield function have been utilized, respectively.

• Proceedings of the KSME Conference
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• 2001.06a
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• pp.523-528
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• 2001

In this study we tried to determine the work-hardening exponent using continuous indentation test. Work-hardening exponent, which was determined by Hollomon equation, in tensile test, is an important parameter to determine plastic deformation and brittle/ductile property of materials. For using Hollomon equation, true stress and true strain were defined by indentation depth and indentation load. Using them the new equation, which is constituted by indentation depth, indentation load and work-hardening exponent, was induced. Indentation depth was calibrated because of elastic deflection and pile-up/sink-in phenomena. Work-hardening exponents of various steels derived by it showed good agreement to the results of tensile tests. In addition to experiments, FEM simulation was accomplished to investigate changes of real contact depth with materials properties changes. Through this simulation it is concluded that the real contact depth is changed by Y/E value which affect the early stage of indentation, and work-hardening exponent which the latter stage.

• Proceedings of the KSME Conference
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• 2000.11a
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• pp.256-261
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• 2000

In this study, we derived work-hardening exponent using continuous indentation test technique. Continuous indentation test technique is a powerful method to evaluate mechanical properties, such as hardness, modulus, ${\sigma}-{\varepsilon}$ curves and etc. It has many merits conventional indentation test has. The relationship between true stress and mean contact pressure and between strain and indentation depth were derived. While the indenter pushes the materials, the region around the indenter is deflected elastically. It is called elastic deflection. And pile-up phenomenon related to plastic deformation around the indenter increased the contact depth, and sink-in phenomenon decreases. So we calibrated contact depth change by considering elastic deflection and pile-up/sink-in. Using calibrated contact depth we redefined the relationship between true stress and mean contact pressure and between strain and contact depth. Through these relationship we could derive work-hardening exponent by analyzing load-depth curves. And it showed good agreement with tensile test results.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.12 no.2
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• pp.49-54
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• 2013

Recently welding of aluminum material is actively carried out to make lightweight in the fields of LNG vessels, aircraft, chemical plants, etc. To obtain high strength, hardness and elongation, elements such as manganese, zinc, silicon, etc should be added in aluminum alloy, which has been improved on the mechanical properties like precipitation hardening, age hardening, loosening, corrosion resistance acid resistance. Ar gas is used as a shielding gas of MIG welding for aluminum, also $N_2$, $O_2$, $CO_2$, $H_2$ etc can be added depending on the composition of the alloy. In this study, Ar + $O_2$, Ar, and He were used for welding, hardness, penetration status and changes in composition of penetrated parts were compared and analyzed. This made it possible to know the status and changes of the process in the penetrated parts depending on used gas throughout this study.

• Transactions of the Korean Society of Mechanical Engineers
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• v.12 no.6
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• pp.1335-1342
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• 1988

In this paper, mechanical properties of mild steel plate which was pretreated by prestress and prestrain loading conditions were studied. The variation of the mechanical properties of the test materials is evaluated in the light of Taylor's work hardening theory. Through this experimental study, it is recognized that material showed unstable phenomena after cyclic loading and it will recover its stability after a certain period of time accompaning the increment of hardness and the yield strength of the material. Also, the strength of smooth specimen, the notch strength of notch specimen and propagation behavior of fatigue specimen which were subjected to prestress and prestrain reveal that the optimal conditions may occur in the first, the middle and the later half of stage II of Taylor's work hardening theory, respectively.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2008.10a
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• pp.154-157
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• 2008

It is important to know the variations of the mechanical properties in the hydroforming process for the safe and durable design purposes. In this study, strain hardening behavior during hydroforming has been investigated by hydroforming of engine cradle as a model process. The variation of mechanical properties such as local hardness and flow stress were used as an index of strain hardening during respective processes. By using the inter-relationships between hardness-flow stress-effective strain at variable pre-strains, the strain hardening behavior during hydroforming has been successfully analyzed. The comparison of predicted hardness with measured hardness confirmed that the methodology used in this study was feasible and the strain hardening behavior can be quantitatively estimated.

• Proceedings of the Materials Research Society of Korea Conference
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• 2003.03a
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• pp.244-244
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• 2003

나노인덴테이션은 시편에 압자를 침투시켜 재료의 기계적 특성을 파악할 수 있는 경도시험법이다. 압입범위를 나노미터범위로 조절할 수 있어 기존에 접근할 수 없었던 극 미소부분에로 응용이 넓어지고 있다. 경도시험시 재료의 탄성 및 소성 작용에 의해 재료는 변형되고, 표면변화 관찰을 통해 표면아래 부분에서 이루어지고 있는 거동을 예측할 수 있다. 이러한 관점에서 나노인덴테이션 시험시에도 발생하는 파일업과 싱크인 현상에서 재료가 나노미터 범위에서 어떠한 양상으로 변형을 하는지를 고찰하는 것은 의미가 있을 것이다. 본 연구에서 파일업과 싱크인의 양상을 파악하고 그 양을 정량화하기 위하여 가공경화양에 따른 표면변화와 압입하중 변화에 따른 표면변화를 관찰하였다. 어닐링한 봉상 알루미늄을 압축변형을 0%, 5%, 20%, 40%, 50% 로 변형시켜 가공경화를 일으켰고, 표면은 전해연마하여 나노압입시험이 가능하도록 하였다. 각각의 시편을 나노인덴테이션 압입하중을 변화시켜 재료에서 하중 변화에 따라 나타나는 표면변화를 관찰하였고, 위의 각 조건에서 파일업양을 정량화 하였다. 연구결과에 대해 ANSYS 유한요소분석 프로그램을 사용하여 재료의 변형양상을 시뮬레이션 하였고, 실제 실험데이터와 비교 분석하였다.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2000.04a
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• pp.40-43
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• 2000

A process optimal design methodology applicable to steady-state forming with a strain-hardening material is presented. in this approach the optimal design problem is formulated on the basis of a rigid-viscoplastic finite element process model and a derivative based approach is adopted as an optimization technique The process model the schemes for the evaluation of the design sensitivity considering the effect of strain-hardening and an iterative procedure for design optimization are described. the validity of the proposed approach is demonstrated through application to die shape optimal design in extrusion.

• Textile Coloration and Finishing
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• v.20 no.4
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• pp.8-14
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• 2008

Flame-retardant cotton fabrics were prepared by UV curing of photocurable aqueous formulations of phosphorous-containing methacrylate monomers and 2-hydroxy-2-methyl-1-phenyl-1-propanone as flame retardants and a photoinitiator respectively, which is an environmentally friendly and energy-saving process. The characterization of the UV-coated cotton fabric was made by ATR, TGA and limited oxygen index measurement. UV cured coating onto cotton fabrics reduced the first thermal decomposition temperature and mass loss as well as increase in the amount of char residue compared with the untreated cotton fabric presumably due to modified thermal decomposition process. The LOI values up to 28.5 and 27.2 were obtained by the UV curing of MMEP and TMEP respectively. The treatment was durable to five laundering cycles, which was more prominent in the case of trifunctional TMEP treatment.