• 대한금속재료학회지
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• 제56권12호
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• pp.861-869
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• 2018

To determine the origin of the inhomogeneous microstructure and texture observed in drawn and annealed high purity copper wires, two kinds of drawing process conditions and their influence was investigated. The regular condition, based on a symmetric die, and a condition designed intentionally to produce an inhomogeneous shear deformation using an asymmetric die were employed. The difference in intensity of <111>-<100> distributed texture between the two wires confirmed that the wire drawn under the asymmetric die condition experienced a higher amount of shear deformation. The extensive shear strain in the wire drawn under the asymmetric die condition gave rise to inhomogeneous primary and secondary recrystallization behavior. After annealing at $200^{\circ}C$, grains with <100> texture, which were larger than the surrounding recrystallized grains, were extensively present on one half circle of the wire drawn under the asymmetric die condition, while larger grains with <100> were sparsely observed around the middle region of the wire drawn under the regular condition. Interestingly, the area where the larger grains with <100> texture existed was identical to the area where the high shear strain occurred during drawing in both wires. During annealing at $400^{\circ}C$, grains with <112> texture started to grow abnormally at the center of both wires as a result of secondary recrystallization. After annealing at $900^{\circ}C$ grains with <112> due to secondary recrystallization occupied the entire region of the wire drawn under the regular condition. On the other hand, in the wire drawn under the asymmetric die condition and then annealed at $900^{\circ}C$, the <100> oriented grains as a result of the normal grain growth of the larger <100> grains which were observed after annealing at $200^{\circ}C$, coexisted with the abnormally grown <112> grains. These results indicate that dynamic recrystallization induced by the shear strain during drawing plays an important role in the inhomogeneity of the microstructure and texture of wires after annealing.

• 소성∙가공
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• 제16권6호
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• pp.467-472
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• 2007

In this study, the effects of initial texture on the twinning formation of AZ31 Mg rolled sheet was investigated. Uniaxial compression tests were carried out on samples cut along the normal direction(ND) and roiling direction(RD), respectively, of rolled AZ31 Mg alloy sheet at various temperatures (RT, 200, 250, 300, 350, $400^{\circ}C$) with the fixed strain rate($10^{-2}/s$). The results showed that deformation twining occurred actively only in the RD specimens, which promoted homogeneous deformation as compared to the ND specimens. The effect of temperature on the formation of deformation twins was also investigated, and the slip/twin transition temperature was found to be approximately $250^{\circ}C$.

• 대한전자공학회:학술대회논문집
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• 대한전자공학회 1999년도 추계종합학술대회 논문집
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• pp.544-547
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• 1999

This paper proposes a high-speed texture mapping algorithm and apply it for the realtime face animation. The mapping process devide into pixel correspondences, Z-buffering, and pixel value interpolation. Pixel correspondences and Z-buffering are calculated exactly through the algorithm. However, pixel values interpolation is approximated without additional calculations. The algorithm dramatically reduces the operations needed for texture mapping. Only three additions are needed in calculation of a pixel value. We simulate the 256$\times$240 pixel facial image with about 100 pixel face width. Simulation results shows that frame generation speed are about 60, 44, 21 frames/second in pentium PC 550MHz, 400MHz, 200MHz, respectively,

• 센서학회지
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• 제29권4호
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• pp.255-260
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• 2020

In this study, we developed a method of improving the surface-enhanced Raman spectroscopy (SERS) response characteristics by depositing a nanoporous Ag metal thin film through cluster source sputtering after forming a pyramidal texture structure on the Si substrate surface. A reactive ion etching (RIE) system with a metal mesh inside the system was used to form a pyramidal texture structure on the Si surface without following a complicated photolithography process, unlike in case of the conventional RIE system. The size of the texture structure increased with the RIE process time. However, after a process time of 60 min, the size of the structure did not increase but tended to saturate. When the RF power increased from 200 to 250 W, the size of the pyramidal texture structure increased from 0.45 to 0.8 ㎛. The SERS response characteristics were measured by depositing approximately 1.5 ㎛ of nanoporous Ag metal thin film through cluster sputtering on the formed texture structure by varying the RIE process conditions. The Raman signal strength of the nanoporous Ag metal thin film deposited on the Si substrate with the texture structure was higher than that deposited on the general silicon substrate by up to 19%. The Raman response characteristics were influenced by the pyramid size and the number of pyramids per unit area but appeared to be influenced more by the number of pyramids per unit area. Therefore, further studies are required in this regard.

• 한국초전도학회:학술대회논문집
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• 한국초전도학회 2000년도 High Temperature Superconductivity Vol.X
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• pp.304-307
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• 2000

고순도 니켈분말을 사용하여 성형, 소결, 압연 및 중간소둔 공정을 통해 cube-texture를 갖는 니켈테이프를 제조하였다. 제조된 니켈테이프의 texture는 성형압력, 성형체의 소결 온도 및 시간, 냉간 압하율 및 중간열처리에 따라 달라지는 것을 관찰하였다. 200kgf/cm$^2$ 의 성형압력으로 제조한 성형체를 1000$^{\circ}$C의 온도에서 8시간열처리한 소결체를 100${\sim}$50 $_{\mu}$m로 압연된 tape을1000$^{\circ}$C 1시간 열처리 할 때 가장 우수한 texture를 가지는 tape을 제조할 수 있었다. 긴 니켈테이프를 제조하기 위해 50cm 길이의 mold에서 성형한 green-pellet을 불활성 분위기(Ar:96%-H$_2$:4%)에서 1000$^{\circ}$C, 8시간동안 열처리하여 소결하였다 400mm길이에 17${\sim}$20mm 두께의 소결체를 압연하여 100$_{\mu}$m두께의 긴 니켈 테이프를 제조하였다. 제조한 테이프의 texture는 소형으로 제조한 테이프에 비해 떨어졌으며 이는 압연 시 시료에 너무 큰 인장력을 가했기 때문으로 사료된다.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2009년도 춘계학술대회 논문집
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• pp.421-424
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• 2009

Superplastic deformation behavior and texture evolution after equal channel angular pressing (ECAP) of Zn-0.3Al alloy were investigated in this study. ECAP was conducted at temperatures from $40^{\circ}C$ to $160^{\circ}C$ on the plate type specimens of 5 mm thickness and 20 mm width. The specimens obtained by ECAP showed typical texture with basal poles tilted away from the ND toward ED. A series of compression and tensile tests was carried out at temperatures from RT to $200^{\circ}C$ under the strain rate from 0.03 to 10/s. After ECAP of the Zn-Al alloy, elongation was dramatically increased up to 1000% at above $60^{\circ}C$. The effects of ECAP on the texture and anisotropy in the superplastic deformation bebavior were found to be negligible.

• 기술사
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• 제18권2호
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• pp.16-22
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• 1985

This study was carried out to evaluate the quality of soybean sprouts grown under three different sources of light. The soybean was germinated under light through blue (251 ux), red (751 ux) and white (50 to 200 lux) polyethylene films at 25$^{\circ}C$ for 10hr./day. Vitamin C, chlorophyll, cellulose and total protein contents were determined and texture was evaluated by tasting soybean sprouts soup. protein pattern in the soybean sprouts were investigated using polyacrylamide gel electrophoresis. Vitamin C, chlorophyll and cellulose contents were increased by white light intensity. The texture of the sprouts grown under white light (50 lux, 100 lux) was better than darkness, but fought under 200 lux. Vitamin C contents of soybean sprouts grown under various sources of light (in order of light : blue > white > red) were higher than theses of ones grown in the darkness. Biosynthesis of chlorophyll was not correlated to Vitamin C content. Total protein contents of cotyledon was not changed significantly under light irradiation. But the soybean sprouts grown under different quality of light, hypocotyl was higher than those grown darkness. (37% and 20% higher for blue light and white light) Densitometric tracing of disc polyacrylamide gel electrophoretic patterns showed that protein of hypocotyl under white light had more high molecular weight protein.

• 한국유기농업학회지
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• 제23권2호
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• pp.301-309
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• 2015

본 연구에서는 무농약 산머루 즙의 양을 각각 50 g, 100 g, 150 g, 200 g 수준으로 다르게 첨가하여 양갱을 제조하고 색도, 당도, 기계적 조직감, 관능평가를 조사하였다. 무농약 산머루 양갱의 색도는 명도(L)값과 황색도(b)값이 무농약 산머루 즙의 첨가농도가 증가할수록 감소하였으나, 반대로 적색도(a)값은 증가하는 경향을 나타내었다. 당도는 대조군이 2.31 Brix로 가장 낮게 나타났으며 무농약 산머루 즙의 첨가량이 증가할수록 당도가 점차 높아져 유의적인 차이를 보였다. 기계적 조직감은 무농약 산머루 즙의 첨가량이 증가할수록 경도는 증가하는 경향을 나타냈지만, 탄력성, 응집성, 점착성, 씹힘성 등은 모두 감소하는 경향을 나타내었다. 관능검사 결과는 색, 향, 맛 등의 전체적 선호도에서 무농약 산머루 즙 150 g 첨가군이 가장 높은 점수를 얻었다.

• 한국초전도학회:학술대회논문집
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• 한국초전도학회 2000년도 High Temperature Superconductivity Vol.X
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• pp.56-60
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• 2000

Cube texture를 갖는 Ni기판위에 MOCVD(Metal Chemical Vapor Deposition)를 이용하여 NiO, CeO$_2$, YBCO 박막을 제조하였다. NiO(200)와 CeO$_2$(200) buffer layer는 450${\sim}$470$^{\circ}$C에서 10분간 MOCVD방법으로 (100)<001>Ni 기판위에 직접 증착하였다. 제조된 NiO, CeO$_2$ buffer layer는 조직이 치밀하며 표면의 상태가 매우 좋으며 Ni기판 위에 epitaxial하게 성장하였다. NiO는 Ni기판과 NiO<100>//Ni<100>의 방위관계를 가지고 성장하였으며, CeO$_2$는 증착조건에 따라 CeO$_2$ <100>//Ni<100> 및 CeO$_2$ <110>//Ni<100> 의 방위관계를 가지고 성장하였다. 증착된 NiO막과 CeO$_2$막에서 균열은 발생하지 않았다. MOCVD법으로 표면에 biaxial texture를 갖는 ceramic buffer를 증착시킨 NiO/Ni및 CeO$_2$/Ni 기판위에 YBCO박막을 MOCVD법으로 제조하였다. YBCO막은 기판온도 800$^{\circ}$C,증착압력 10torr, 산소분압을 0.7torr로 하여 10분간 행하였다. 공급원료의 조성에 따라 YBCO의 막의 texture와 형성되는 상이 변화되었다. NiO/Ni및 CeO$_2$/Ni 기판 위에 증착된 YBCO막은 c축 배향성을 가지고 성장하였으며, -scan 및 ${\varphi}$ -scan으로 측정한 (500)면의 in-plane과 (110)면의 out-of-plane의 FWHM(Full Width Half Maximum)값은 각각 10$^{\circ}$ 미만으로 우수하였다.

• 한국진공학회지
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• 제11권4호
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• pp.194-200
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• 2002

MOCVD(metal-organic chemical vapor deposition) Cu 박막을 여러 조건에서 열처리를 행하여 그 전기적 특성과 미세구조의 변화를 통해 적절한 열처리 조건을 찾고 그 효과를 조사하였다. Ar 1 torr, $400^{\circ}C$에서 열처리를 거친 Cu 박막의 비저항이 1.98 $\mu$Ω.cm로 가장 낮게 나타났으며, 결정성의 경우도 $I_{(111)}/I_{(200)}$의 비가 2.03에서 3.11로 열 처리를 거치지 않았을 경우와 비교해서 약 50% 정도 향상된 값을 나타내었다. 열처리 후의electromigration(EM) 테스트에서는 Ar 1 torr, $400^{\circ}C$에서 열처리를 거친 배선이 EM에 대한 가장 높은 저항성을 보였다. 이것은 열처리 후 낮은 비저항, (111) 결정면의 성장, 그리고 표면 거칠기의 감소에서 기인한 것이다.