• Journal of Life Science
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• v.12 no.5
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• pp.589-594
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• 2002

Changes in the content of volatile terpenoids were investigated with heat-treated carrot. As heat treatment temperature became higher, the amount of volatile terpenoids decreased significantly. According to heat-treatment period, the volatile terpenoids, a-pinene and total terpenoids, decreased drastically during the initial 30-minutes of heat treatment but the rate of decrease slowed down afterwards. When changes in the content of volatile terpenoids in carrot juice were investigated according to sterilization temperature and period, the content decreased quickly with higher sterilization temperature. According to sterilization period, the content of volatile terpenoids decreased drastically during the initial 20-minutes of sterilization but decreased gradually afterwards. The amount of total terpenoids decreased more when sterilization was done at 10$0^{\circ}C$ for 20 minutes compared to sterilization at 6$0^{\circ}C$ and 8$0^{\circ}C$ for 60 min. In order to reduce the amount of volatile terpenoids in carrot juice, sterilization at high temperature for a short period of time would be more effective compared with sterilization at low temperature for a long period of time.

• Journal of Applied Biological Chemistry
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• v.50 no.3
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• pp.148-154
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• 2007

Volatile components of the essential oils of Satsuma mandarin (C. unshiu), Dangyuza (C. grandis), Yuza (C. junos), Byungkyul (C. playtymamma), Jinkyul (C. sunki), and Hakyul (C. natsudaidai) grown in Jeju Island were isolated from the fruit peels by hydro distillation and determined by GC-MS. GC-MS analysis identified 58 compounds, with main components being d-limonene $(64.01{\sim}79.34%),\;{\beta}-myrcene\;(3.01{\sim}26.53%),\;{\gamma}-terpinene\;(0.11{\sim}12.88%),\;{\beta}-pinene\;(0.78{\sim}4.74%),\;and\;{\alpha}-pinene\;(1.01{\sim}2.55%)$. Differences in compositions and contents of the essential oils were observed among citrus varieties. Effects of citrus oils on growth inhibitions of Escherchia coli, Staphyllococcus epidermidis, and Candida albicans were investigated using disc diffusion assay and minimal inhibitory concentration (MIC) assay. The essential oils inhibited growths of the test organisms, exhibiting higher levels of activity against Gram-positive S. epidermidis (MIC values $0.04{\sim}0.17mg/mL$), whereas Gram-negative E. coli was moderately resistant (MIC values $1.66{\sim}20.30mg/mL$). MIC of citrus essential oils ranged from $0.82{\sim}23.69mg/mL$ against C. albicans. The essential oils obtained from C. sunki, C. grandis, and C. playtymamma showed the highest antimicrobial activities against S. epidermidis and C. albicans, indicating their potential as natural antimicrobial agents.

• Food Science and Biotechnology
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• v.18 no.1
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• pp.18-24
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• 2009

The volatile compounds of dried sancho (Zanthoxylum schinifolium), an aromatic plant were extracted by simultaneous distillation and extraction (SDE) method and identified by gas chromatograph-mass spectrometry (GC-MS). Selected chiral constituents of sancho oil were characterized by enantiodifferentiation using multidimensional gas chromatograph (MDGC)-MS. A total of 57 compounds were identified and quantified, and the major compounds were identified estragole, nonanoic acid, octanoic acid, $\beta$-phellandrenene, and limonene. Among them, estragol (63.9%) was found as the predominantly abundant component of sancho. $\alpha$-pinene and nerolidol, and $\beta$-pinene and linalool were determined to be enantiomerically pure (100%) for their (S)-form and (R)-form, respectively. The enantiomeric composition of limonene in sancho revealed 83.9% purity for the (S)-enantiomer, whereas (E)- and (Z)-rose oxides showed mixtures of both enantiomers. The enantiomeric excess (%) for citronellal was 22.6% with the (R)-enantiomer as major enantiomer. The enantiomeric composition of these compounds can be used as parameter for authenticity control of sancho.

• The Research Journal of the Costume Culture
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• v.18 no.2
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• pp.371-381
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• 2010

The pine needles can be used for four seasons in normal living and it can be taken friendly everywhere as it is distributed over 50% in Korea. The pine needles consist of vitamins, protein, minerals, essential oil and enzyme related to antimicrobial activity. It has effect like high blood pressure, neuralgia and hanged over by terpene, glucokinin, rutin, apigenic acid and tannin. Also the extract of them can be used for dyeing of fabrics. However, the extract components and effects of them are not well known yet. Therefore, the purpose of this study was to investigate the volatile components of the pine needles extract and functionality. The pine needles extract was dyed into various fabrics(nylon, silk, wool and soybean) and mordanted with Al, Cu, Cr, Fe and Sn. The extracted aroma compounds were compared by gas chromatography-mass spectrometry. The major volatile compounds of pine needles verified by using SPME were alpha-pinene, beta-pinene, beta-phellandrene, caryophyllene, ethanon, benzen. A total of 15 compounds were identified by using the SPME fibers. In the UV-visible spectra, the maximum absorption of wavelength of the pine needles ethanol extract appeared at 460, 630nm for chlorophyll component and at 237, 281nm for tannin component with the pine needles distilled water extract. Most of sample showed high antibacterial effect in none mordant but wool fabric showed high antibacterial effect in mordants. The result of UV block test showed a superior ability of blocking ultraviolet ray infiltration in all sample.

• Korean Journal of Agricultural Science
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• v.46 no.1
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• pp.33-44
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• 2019

This study was conducted to examine the components of phytoncide from a pine forest in the southern temperate zone. Recent studies have found that a large amount of phytoncide is released not only from cypress trees but also from pine trees. Because the amount released is the highest during summer, we selected a warm climate region in the southern temperate zone and measured the concentration in the month of August. To capture the phytoncide from the forest atmosphere, we used the adsorption tube method with a mini pump and successfully gathered 9 L of forest air at a flow rate of 150 mL/min. We performed duplicate sampling from two different tubes installed at the same location and derived the mean value. A gas chromatography/mass spectrometer detector with thermal desorption spectroscopy was utilized to perform quantitative and qualitative analyses of the captured material. The results showed that the average phytoncide particle of the pine forest in the southern temperate zone contained a number of components as follows in descending order: ${\alpha}$-Pinene (39%, $0.28ng/m^3$), followed by ${\beta}$-Pinene (16%, $0.11ng/m^3$), D-Limonene (8%, $0.06ng/m^3$), camphor (6%, $0.04ng/m^3$), camphene (6%, $0.04ng/m^3$), and p-Cymene (5%, $0.04ng/m^3$). There were also 13 additional phytoncide components in trace amounts. The results of this study are expected to provide a useful dataset for building a "Healing-forest".

• Korean Journal of Agricultural Science
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• v.49 no.4
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• pp.983-993
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• 2022

The purpose of this study is to provide information on a forest healing environment using the analysis of nature volatile organic compounds (NVOCs) and thermal comfort in Chungnam National University Experimental Forest, with the aim of using the Experimental Forest as a healing environment for health promotion. We analyzed NVOCs and thermal comfort of Chungnam National University Experimental Forest measured on September 12^th, 2021. As a result of the NVOC analysis, a total of seven substances were detected, mainly including alpha pinene and beta pinene. The detection amount for each time period was highest at the time of sunset. The thermal comfort was analyzed by time-dependent changes and changes according to clothing and exercise amount. The results showed that the predicted mean vote of the experimental forest is within the range of 'slightly cool' and 'slightly warm' sensation, and thus a comfortable thermal environment could be controlled by the amount of clothing and activity. Based on the analysis, this study provides information on the healing environment of the experimental forest at Chungnam National University. It also indicates that the forest can be used as a health promotion and healing environment with thermal comfort by composing a physical activity program of appropriate intensity for each time period.

• Atmosphere
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• v.34 no.2
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• pp.187-202
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• 2024

We analyzed the observed characteristics of monoterpene and developed an empirical formula for monoterpene concentration in the pine-dominated mixed forest of the National Center for Forest Therapy. Monoterpene was measured at 0800, 1200 and 1700 LST once a month using sorbent tube sampling coupled with thermal desorption gas chromatography and mass spectrometry. Monoterpene concentration is low in winter and shows a maximum in June and July. The major components of monoterpene are alpha-pinene, camphene and beta-pinene. During the warm period from May to November, monoterpene concentration is higher at 0800 and 1700 LST than at 1200 LST. The empirical formula takes into account the vegetation variables, temperature-controlled emission, oxidation processes and dilution by wind. The vegetation variable accounts for the difference in observed monoterpene concentration between two sites. The observed monoterpene concentration normalized by the vegetation variable increases exponentially with air temperature. The oxidation process explains the lower monoterpene concentration at 1200 LST than at 0800 and 1700 LST during the warm period. The monoterpene estimates using the empirical formula shows a correlation of 0.52 with the observation for the development period (2018~2020), while it shows a correlation of 0.72 for the validation year (2021). Such higher correlation for the validation year than for the development period is due to the fact that variability of monoterpene concentration is better explained by air temperature in 2021 than in the development period. However, the developed formula underestimates the monoterpene concentration in May and June, showing the limitation in accurately capturing the monthly variation of monoterpene.

• Journal of the Society of Cosmetic Scientists of Korea
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• v.17 no.1
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• pp.29-38
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• 1991

As the suitable place of the forest bathing, Two places of the needle-leaf trees, which are located in the Oh-Saek mineral spring near place from the Sorak mountain, were selected. And then, Headspace gas trapping apparatus were setted in that two places and the aromatic components of the forest were adsorbed by Tenax-TA column for 24 hours. And Tenax-TA column were analyzed by the GC SE GC-MS. The analyzed components were found to contain up to between 70-80% of pollutants, which are Toluene, Methyl Chloride, Hexane, p-Xylene, Benzene, ... etc. On the other hand, the aromatic components of the forest, which give aromatheraphitical effectness, are as follow: alpha-Pinene, Limonene, 1, 8-Cin-eol, Benzaldehyde, . . . etc.

• Journal of Society of Preventive Korean Medicine
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• v.10 no.2
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• pp.131-145
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• 2006

Perilla frutescens is known as the herb helps digestion, tonifies stomachache, and decreases fever in oriental medicine. And it is reported it possess the anti-pyretic effect, anti-inflammatory effect, anti-allergy effect, anti-tumor effect etc. The components isolated from this herb consist of perilla aldehyde, d-limonene, ${\alpha}-pinene$, cyanin, linoleic acid, palmitic acid, menthol, rosmarinic acid and luteolin etc. But there is no effective tools to determine the quality of this herb. In this study, we aimed to analyze the changes of liquid chromatogram pattern, one of major standardization method, to determine the quality of Perilla frutescens.

• Journal of Korean Society for Atmospheric Environment
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• v.32 no.4
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• pp.349-359
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• 2016

Researchers have traditionally assumed that aerosol particles containing secondary organic aerosols (SOAs) are to be in liquid state with low viscosity even at low relative humidity. However, recent measurements showed that SOAs can have high viscosity under certain conditions. Herein, new different techniques for measurements of viscosities of SOA particles are introduced. Moreover, laboratory studies for the viscosities and the phases of biogenic SOAs produced by ${\alpha}$-pinene, isoprene, limonene, and ${\beta}$-caryophyllene of atmospheric relevance are reviewed. Future studies for determination of the phases of atmospheric aerosol particles are also suggested.