• The Korean Journal of Ceramics
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• 제2권2호
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• pp.76-82
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• 1996

PLZT ceramics having two nominal compositions, $Pb_{1-3x/2}La_xV_{x/2}(Zr_{03}Ti_{03})O_3$ and $Pb_{1-x}La_x(Zr_{0.2}Ti_{0.5})_{1-x/4}V_{x/4}O_3$ (V: vacancy) with x=0.00~0.30, were prepared. The physical, structural, and dielectric properties were investigated by X-ray diffraction, scanning electron microscopy, Raman spectroscopy, and measurements of bulk density and dielectric constant. The two series with A-stie and B-site vacancies showed different physical, structural, dielectric properties, and, specially, Curie temperature. In comparison to PLZT with B-site vacancies, PLZT with A-site vacancies showed high Curie temperatures and low maxima of dielectric constant. Consequently, it is evident that the properties of PLZT ceramics depend on the vacancy formula adopted as a batch composition in preparation.

• 한국자기학회지
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• 제16권1호
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• pp.11-13
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• 2006

[ $M\"{o}ssbauer$ ] spectra of $Ti_{1-x-y}Co_xFe_yO_2(0.01{\leq}x,\;y{\leq}0.05)$ prepared with $^{57}Fe$ enriched iron have been taken at various temperatures ranging from 80 to 300K. The Mossbauer spectrum of $Ti0.94Co_{0.03}Fe_{0.03}O_2$ consists of a ferromagnetic (six-Lorentzian), a paramagnetic phase (doublet) and armorphous phase over all temperature ranges. Isomer shifts indicate $Fe^{3+}$ for the ferromagnetic phase and the paramagneic phase of $Ti_{1-x-y}Co_xFe_yO_2$ samples. It is noted that the magnetic hyperfine field of ferromagnetic phase had the value about 1.5 times as large as that of u-fe. The XRB data for $Ti_{1-x-y}Co_xFe_yO_2$ showed mainly rutile phase with tetragonal structures without any segregation of Co and Fe into particulates within the instrumental resolution limit. The magnetic moment per (Co+Fe) atom in $Ti0.94Co_{0.03}Fe_{0.03}O_2$, under the applied field of 1T was estimated to be about $0.332{\mu}_B$ which is ten times as large as that of $Ti0.97Co_{0.03}Fe_{0.03}O_2,\;0.024{\mu}_B$ per Co atom, suggesting a high spin configuration of Co and fe ions.

• 천문학회지
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• 제52권2호
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• pp.41-47
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• 2019

We report on the timing properties of the 'Crab twin' pulsar PSR B0540-69 measured with X-ray data taken with the Swift telescope over a period of 1100 days. The braking index of the pulsar was estimated to be $n=0.03{\pm}0.013$ in a previous study performed in 2015 with 500-day Swift data. This small value of n is unusual for pulsars, and a comparison with an old estimate of $n{\approx}2.1$ for the same target determined ~10 years earlier suggests a dramatic change in the braking index. To confirm the small value and therefore the large change of n, we used 1100-day Swift observations including the data used in the earlier determination of n = 0.03. In this study we find that the braking index of PSR B0540-69 is $n=0.163{\pm}0.001$, somewhat larger than 0.03. Since the measured value of n is still much smaller than 2.1, we can confirm the dramatic change in the braking index for this pulsar.

• 한국통신학회논문지
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• 제40권2호
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• pp.355-362
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• 2015

본 연구에서는 X-밴드 레이더에서 사용하는 9.385[GHz] 서큘레이터를 Y형 WR112 도파관속에 페라이트를 삽입하여 제작을 하였다. 페라이트 설계는 B/R(Below Resonance) 모드 방식을 사용하여, 페라이트 내부에서 전계 분포가 120도의 회전이 발생하는 조건과 페라이트의 내부의 직류 자계의 세기와 외부 자계의 세기를 계산하였다. 또한, 임피던스 정합을 포함하여 대역폭, 선택도, 삽입손실 등, 서큘레이터의 성능 향상을 위하여 두 개의 페라이트 사이에 같은 형태의 유전체를 삽입하였다. 최적의 페라이트 형태 및 유전체를 얻기 위하여 CST MWS를 이용하였다. 9.385[GHz]에서 시뮬레이션 결과는 정재파비 1.02, 분리도 -40dB, 삽입손실 0.2dB의 결과를 얻었고, 측정 결과는 정재파비 1.03, 분리도 -38dB, 삽입손실 1.2dB 이었다. 분리도, 정재파비는 시뮬레이션 결과와 잘 일치 하였지만, 삽입손실은 약 1dB 정도 크게 발생하였다.

• 한국세라믹학회지
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• 제40권5호
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• pp.405-409
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• 2003

The effect of substitution of Gd ions for Ca ions in the B $i_{1.84}$P $b_{0.34}$S $r_{1.91}$(C $a_{1-x}$ G $d_{x}$)$_{2.03}$ C $u_{3.06}$ $O_{ 10+{\delta}}$/ (x=0.0~0.06) was investigated by measuring x-ray diffraction patterns, lattice constants, do resistivity and Hall effect. We found the solubility limit of Gd in the 110 K phase to be x < 0.015. Within the solubility limit, the c-axis seemed to decrease with increasing x. In the region of the 110 K single phase, the critical temperature $T_{c}$ gradually decreased with an increasing the Gd concentration x, corresponding to a small change of the carrier concentration.

• 대한전기학회논문지
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• 제41권1호
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• pp.56-62
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• 1992

The GaAs bulk crystals are grown by the Synthesis Solute Diffusion(SSD) method and its properties are investigated. The crystal growth rate at optimum condition is 0.28 cm/day and their temperature dependence is R(T) = 2.92 x 10S04T exp(-1.548eV/kS1BTT) [cmS02T/day.K]. Etch pits density distribution along radial direction is order of 10S04TcmS0-2T and 10S03TcmS0-2T at the edge and middle of the wafers, respectively, and it increased exponentially along vertical direction of ingot. Moreover,it is uniformly distributed as order of 10S03TcmS0-2T in radial direction of In doped GaAs. The carrier concentration and mobilities are measured to 0.34-2.1 x 10S016T cmS0-3T and 2.3-3.3x10S03T cmS02T/V.sec, respectively.

• 한국세라믹학회지
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• 제47권6호
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• pp.603-607
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• 2010

Turquoise blue pigment of Vanadium-zircon blue (DCMA number 14-42-2), which was already commercialized, was stable to be reproduced but insufficient to give strong blue. However, it possible to obtain more intense blue by partially substituting cobalt ions into the willemite($Zn_2SiO_4$) lattice classified into DCMA number 7-10-2 for blue ceramic pigment. By the composition of willemite $Co_xZn_{2-x}SiO_4$(X=0.01, 0.03, 0.05, 0.07, 0.09 mole), this study used reagent grade zinc oxide, cobalt oxide and silicon dioxide as starting materials, carrying out the synthesis with solid reaction method by adding $H_3BO_3$ as a mineralizer. The firing temperature was between $1200^{\circ}C$ and $1400^{\circ}C$. The characteristics of synthesized pigment were analyzed by X-ray diffraction, Raman spectroscopy and SEM and the characteristics of color tones were analyzed by UV-Vis spectroscopy and CIE-$L^*a^*b^*$ measurement. As a result, the optimal composition was $Zn_{1.95}Co_{0.05}$ with 1wt% of $H_3BO_3$ as a mineralizer and firing condition was $1350^{\circ}C$/3 h. $L^*a^*b^*$ value was 29.25, 41.03, -59.93 for on glaze pigment and 37.03, 36.41, -60.03 for under glaze pigment.

• 한국잠사곤충학회지
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• 제15권2호
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• pp.29-33
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• 1973

잠품종에 따라서 차이가 견사섬도와 견층용해도가 견사의 탄성적성질에 미치는 영향에 대하여 알아보았다. 즉 21개품종의 견사에 대하여 견사섬도 (X$_1$)와 견층용해도 (X$_2$)를 측정하고, X$_1$ 및 X$_2$의 변화와 절단강도(Y$_1$), 절단신도 (Y$_2$) 및 양구율 (Y$_3$)과의 관계를 알아 본결과 다음과 같은 식을 찾았다. A. 견사섬도의 영향 $Y_1$= -0.4$\chi$$_1$＋5.03 $Y_2$=1.2$\chi$$_1$＋2.7 $Y_3$= -25.2$\chi$$_1$＋140.95 B. 견층 용해도의 영향 $Y_1$= -2.4$\chi$$_2$＋3.43 $Y_2$=20$\chi$$_2$＋3.7 $Y_3$= -120$\chi$$_2$＋78.37.

• 한국세라믹학회지
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• 제38권12호
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• pp.1104-1109
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• 2001

110K상의 산화물 고온초전도체를 B $i_{1.84}$P $b_{0.34}$S $r_{1.91}$C $a_{2.03}$C $u_{3.06}$ $O_{10+}$$\delta$/의 출발조성비로 고상반응법(solid-state reaction)에 의해 합성하였다. 이렇게 합성된 Bi계 110K상의 산화물 고온초전도 물질을 다시 분말 상태로 만든 후, Ag 금속분말을 10wt%, 30wt%, 50wt%의 각 비율로 혼합하였다. Ag 금속분말이 혼합된 시편들을 86$0^{\circ}C$~875$^{\circ}C$로 24시간 동안 최종 소결시켰다. 그후, 각 시편들에 대하여 x-선, $T_{c}$, SEM 등을 측정하여 Ag 혼합량에 대한 초전도특성 및 표면의 grain 크기변화 등에 대한 조사를 진행하였다. Ag 혼합량이 증가됨에 따라 Ag peak의 강도는 증가되었고, 시편 내 2223 상의 비율은 감소하고 2212상의 비율은 증가되었다.비율은 증가되었다.

• 대한화학회지
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• 제9권3호
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• pp.142-147
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• 1965

p-Phenylenediamine dihydrochloride의 結晶構造를 X-線 廻折法을 利用하여 解明하였다. 이結晶은 三斜晶係에 屬하며, 空間群은 $C_i1-P{\bar\1}$ 이고, 格子常數는 $a= 4.38{\pm}0.02, b=5.90{\pm}0.02, c=8.76{\pm}0.03{\AA}, {\alpha}=1101{\pm}1, {\beta}=96{\pm}1^{\circ}$이다. 그리고 單位格子속에는 들어있는 化學單位數,Z는 1이다. 各原子의 座標는 a, b 및 c軸에 따른 二次原的인 電子密度의 投影 및 ($F_o-F_c$) 合成에 依하여 얻었다. 이 結晶構造와 이미 硏究된 aliphatic diamine의 hydrogen halide 들의 構造와를 比較하였다.