• 제목/요약/키워드: $YBa_2$$Cu_3$$O-{7-$\delta$}$film.

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RF 마그네트론 스퍼터링법에 의한 a-축 배향 $YBa_2Cu_3O_{7-\delta}$박막의 제조 (Preparation of a axis oriented $YBa_2Cu_3O_{7-\delta}$ thin films by RF magnetron sputtering)

  • 이재준;김영환;신진;이경희;최상삼;한택상
    • 한국재료학회지
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    • 제4권4호
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    • pp.459-465
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    • 1994
  • a-측으로 배향된 $YBa_2Cu_3O_{7-\delta}$ 고온 초전도 박막을 $LaAIO_{3}$(100)단결정 기판에 이중 타게트 off-axis rf마그네트론 스퍼터링법으로 증착하였다. 박막은 기판온도(Ts)$590^{\circ}C$$680^{\circ}C$사이에서 단일공정으로 증착하는 one-step방법과, $590^{\circ}C$의 저온에서 a-축으로 배향된 YBCO박막(두께-30nm)을 면저 만들어 틀로 작용시킨 후 그 틀위에 나머지 부분을 기판온도를 승온하면서 증착하는 방법인 two-step방법 등 두 가지 방법을 사용하여 증착시켰다. one-step방법에서는 $T_s$가 증가함에 따라 감소하였으며, ($00 \ell$)피크는 증가하였다. Two-step방법으로 증착한 박막은 증착속도가 감소함에 따라 (h00)피크가 우세하게 나타났다. 박막의 미세구조는 a-축, c- 축 배향성이 혼재하여 핀홀과 같은 결함들이 생성되었다. 모든 경우 $T_s$가 감소함에 따라 a-축 배향성은 우세하였으나 전기적 특성은 저하되었고, 긴 전이온도 폭을 가졌다.

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Microstructure and Property Relationship of Laser Ablated YBCO Thin Films from Modified Melt-Textured Grown Targets

  • Kim, C.H.;Hahn, T.S.;Hong, K.S.
    • Progress in Superconductivity
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    • 제2권1호
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    • pp.15-19
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    • 2000
  • [ $YBa_2Cu_3O_{7-\delta}$ ] thin films were deposited by laser ablation using modified melt-textured grown targets. As the laser energy density was increased, the films showed an increasing c-axis orientation and an improvement of superconducting properties. However, at 4 $J/cm^2$, the degree of c-axis alignment and $J_c$ of the film were considerably reduced. These were attributed to the enhanced a-axis outgrowths. It was shown that the increased laser energy density resulted in the formation of $Y_2O_3$ inclusions during the c-axis film growth, and that these inclusions nucleated the a-axis outgrowths.

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TFA-MOD법에 의한 금속기판 위 YBCO 박막 제조 (Fabrication of YBCO films on metal tapes by the TFA-MOD process)

  • 신거명;송규정;박찬;문승현;유상임
    • Progress in Superconductivity
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    • 제7권1호
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    • pp.92-96
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    • 2005
  • YBCO thin films on metal substrates were prepared by the metal-organic deposition using trifluoroacetates (TFA-MOD). To compensate the loss of Ba element from the precursor films due to the reaction with $CeO_2$ cap layer, we have employed Ba-excessive precursor solutions of $YBa_{2+x}Cu_{3}O_{7-{\delta}}$ ($0{\le}x{\le}0.1$). The precursor solutions were dip-coated on the metal substrates with $CeO_2$ cap layer, initially heated up to $400^{\circ}C$, and finally fired at the various high temperatures for 2 h in a reduced oxygen atmosphere. With this approach, YBCO films possessing critical temperature over 85 K could be successfully prepared on the metal substrates. The highest $T_{c,zero}$ value of 86 K was obtained from the Ba-excessive YBCO film of x=0.005 in $YBa_{2+x}Cu_{3}O_{7-{\delta}}$ fired at $750^{\circ}C$ for 2 h. However, unexpected $T_c$ suppression even in Ba-excessive YBCO samples requires further identification.

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High Temperature Superconducting Pseudo-Lumped Element Bandpass Filter

  • Min, Byoung-Chul;Choi, Young-Hwan;Kim, Hong-Teuk;Moon, Seung-Hyun;Lee, Seung-Min;Oh, Byung-Du
    • Progress in Superconductivity
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    • 제1권1호
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    • pp.42-46
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    • 1999
  • A high-temperature superconducting 1.78 GHz bandpass filter, designed for PCS applications, is presented. The structure consists of microstrip pseudo-lumped elements, which enables miniaturization of the filter. A 5-pole microstrip filter could be realized on a 37 mm $\times$ 9 mm $LaAlO_3$ substrate, using double-sided high-temperature superconducting $YBa_2Cu_3O{7-\delta}$ thin film. This filter showed 0.7 % fractional bandwidth, 0.3 dB insertion loss, and 12 dB return loss in the passband at 60 K.

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S-parameter Circle-fit과 Lorentzian-fit 방법으로 측정된 고온초전도체 박막의 유효표면저항 비교 (A Comparative Study on the Effective Surface Resistance of High-$T_c$ Superconductor Films as Measured by Using the S-parameter Circle-fit and the Lorentzian-fit Methods)

  • 김민정;정호상;이재훈;이상영
    • Progress in Superconductivity
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    • 제9권2호
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    • pp.146-151
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    • 2008
  • Measurements of surface resistance ($R_s$) of high temperature superconductor (HTS) films with accuracy are essential for microwave applications of HTS materials. In using the dielectric resonator method, uncertainties in the unloaded quality factor of the resonator cause significant errors in the measured $R_s$ of HTS films. We compare the Rs values of $YBa_2Cu_3O_{7-{\delta}}$ films calculated from the $Q_0$ as determined from the Lorentzian fit with that from the $Q_0$ as determined from the S-parameter circle-fit at temperatures between 15 K and 77 K. The two sets of values appeared to differ by 5%, 7%, 6%, and 11% at temperatures of 15, 60, 70, and 77 K, respectively, from each other, implying that careful error analysis needs to be performed in obtaining the $R_s$ of HTS films by using the Lorentzian-fit method, with the ones determined from the S-parameter circle-fit used as the reference.

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DCA-MOD 방법으로 제조하는 YBCO 박막의 임계전류밀도에 미치는 전구체 조성의 효과 (Effects of Precursor Composition on the $J_c$ of YBCO thin Films Prepared by DCA-MOD Method)

  • 김병주;김혜진;이종범;이희균;홍계원
    • Progress in Superconductivity
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    • 제9권1호
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    • pp.91-95
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    • 2007
  • [ $YBa_2Cu_3O_{7-{\delta}}$ ] films have been prepared on $LaAlO_3$ (100) single-crystal substrates by the metal organic deposition using dichloroacetate precursors (DCA-MOD). DCA precursor solutions with different composition such as; Yttrium-excess(15 at%), barium-poor(25 at%), and a stoichiometric(Y:Ba:Cu=1:2:3) were prepared in order to investigate the effects of precursor composition on the properties of YBCO films prepared by DCA-MOD method. Coated films were calcined at low temperature up to $500^{\circ}C$ in flowing humid oxygen atmosphere. Conversion heat treatment was performed $800^{\circ}C$ for 2 h in flowing Ar gas containing 1000 ppm oxygen with a humidity of 9.45%. For the film prepared using excess yttrium composition, high critical current density ($J_c$) of $>2MA/cm^2$ was obtained whereas, for the films prepared using barium-poor composition, $J_c$ was lower than $1MA/cm^2$.

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High Temperature Superconducting Pseudo-Lumped Element Bandpass Filter

  • Choi, Young-Hwan;Kim, Hong-Teuk;Moon, Seung-Hyun;Lee, Seung-Min;Oh, Byung-Du;Min, Byoung-Chul
    • 한국초전도학회:학술대회논문집
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    • 한국초전도학회 1999년도 High Temperature Superconductivity Vol.IX
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    • pp.107-111
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    • 1999
  • A high-temperature superconducting 1.78 GHz bandpass filter, designed for PCS applications, is presented. The structure consists of microstrip pseudo-lumped elements, which make the miniaturization of the filter possible. A 5-pole microstrip filter can be realized on 37 mm ${\times}$ 9 mm LaAlO$_3$ substrate, using double-sided high-temperature superconducting YBa$_2Cu_3O_{7-{\delta}}$ thin film. This filter shows 0.7% fractional bandwidth, 0.3 dB insertion loss, and 12 dB return loss in the passband at 60 K.

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Effect of weak interlayer coupling on critical fluctuation in high $T_c$ superconductors

  • Kim, Jin-Tae;Kang, W.N.;Chung, S.H.;Ha, D.H.;Yoo, K.H.;Kim, M.S.;Lee, Sung-Ik;Park, Y.K.;Park, J.C.
    • Progress in Superconductivity
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    • 제1권1호
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    • pp.1-8
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    • 1999
  • The magnetization and/or resistivity of high $T_c$ superconductors ($YBa_2Cu_3O_{7-\delta}$(YBCO) single crystal, $Bi_2Sr_2CaCu_2O_8$ (Bi-2212) single crystal, $Tl_2Ba_2CaCu_2O_8$ (Tl-2212) film, $HgBa_2Ca_2Cu_3O_8$ (Hg-1223) film) have been measured as a function of magnetic field H and temperature T. The extracted fluctuation part of the magnetization and conductivity exhibits a critical behavior consistent with the three-dimensional XY model. The dynamic critical exponent z does not sensitively vary with a type of the superconductors. The value of z ranges from 1.5 to $1.8{\pm}0.1$. However, the static critical exponent ${\nu}$ is the most largely increased in Tl-2212 that has a weaker interlayer coupling strength than YBCO; the value of ${\nu}$ is 0.669, 0.909, 1.19, and 1.338 for YBCO, Bi-2212, Hg-1223, and Tl-2212 respectively. The results indicate that the weak interlayer coupling along the c-axis of high $T_c$ superconductors near $T_c$ does not influence the dynamic critical exponent z (the same value of superfluid $^4He$), but significantly increases the static critical exponent ${\nu}$.

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