• Title/Summary/Keyword: $YBa_2$$Cu_3$$O-{7-$\delta$}$film.

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Preparation of a axis oriented $YBa_2Cu_3O_{7-\delta}$ thin films by RF magnetron sputtering (RF 마그네트론 스퍼터링법에 의한 a-축 배향 $YBa_2Cu_3O_{7-\delta}$박막의 제조)

  • Lee, J.J.;Kim, Y.H.;Shin, J.;Lee, K.H.;Choi, S.S.;Hahn, T.S.
    • Korean Journal of Materials Research
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    • v.4 no.4
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    • pp.459-465
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    • 1994
  • A-axis oriened YBCO thin flims were grown on $LaAIO_{3}$ single crystal substrate by off-axis rf magnetron sputtering method. We used two kinds of process to get a-axis oriented fi1ms;one-step process and two-step process. In one-step process, films are grown in single step in which substrate temperature( $T_s$) is in the range of $590^{\circ}C$ to $680^{\circ}C$. On the other hand, in two step process a-axis oriented thin film templates i f about 30nm thickness is deposited at low temperature first, and subsequently films are grown at elevated temperature to the final thickness of about 100nm. In the case of one step process($T_s$ ~)$600^{\circ}C$), prefered a-axis orientation is dominant and Cu-rich phases segregate at the surface. Segregations decrease and ($00 \ell$) peaks increase upon increasing $T_s$. The films prepared by two step method appeared to have strong(h00) peaks as the deposition rate increased. Microstructure shows pin holes resulted from mixed phases of a-axis and c-axis oriented films. In both cases of one step and two step process, as TS decreases, prepared films show stronger a-axis orientation. However electrical properties of the films are depressed with lower $T_c$ and wider $\Delta T$ as $T_s$ decreases.

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Microstructure and Property Relationship of Laser Ablated YBCO Thin Films from Modified Melt-Textured Grown Targets

  • Kim, C.H.;Hahn, T.S.;Hong, K.S.
    • Progress in Superconductivity
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    • v.2 no.1
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    • pp.15-19
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    • 2000
  • [ $YBa_2Cu_3O_{7-\delta}$ ] thin films were deposited by laser ablation using modified melt-textured grown targets. As the laser energy density was increased, the films showed an increasing c-axis orientation and an improvement of superconducting properties. However, at 4 $J/cm^2$, the degree of c-axis alignment and $J_c$ of the film were considerably reduced. These were attributed to the enhanced a-axis outgrowths. It was shown that the increased laser energy density resulted in the formation of $Y_2O_3$ inclusions during the c-axis film growth, and that these inclusions nucleated the a-axis outgrowths.

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Fabrication of YBCO films on metal tapes by the TFA-MOD process (TFA-MOD법에 의한 금속기판 위 YBCO 박막 제조)

  • Shin Geo-Myung;Song Kyu-Jung;Park Chan;Moon Seung-Hyun;Yoo Sang-Im
    • Progress in Superconductivity
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    • v.7 no.1
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    • pp.92-96
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    • 2005
  • YBCO thin films on metal substrates were prepared by the metal-organic deposition using trifluoroacetates (TFA-MOD). To compensate the loss of Ba element from the precursor films due to the reaction with $CeO_2$ cap layer, we have employed Ba-excessive precursor solutions of $YBa_{2+x}Cu_{3}O_{7-{\delta}}$ ($0{\le}x{\le}0.1$). The precursor solutions were dip-coated on the metal substrates with $CeO_2$ cap layer, initially heated up to $400^{\circ}C$, and finally fired at the various high temperatures for 2 h in a reduced oxygen atmosphere. With this approach, YBCO films possessing critical temperature over 85 K could be successfully prepared on the metal substrates. The highest $T_{c,zero}$ value of 86 K was obtained from the Ba-excessive YBCO film of x=0.005 in $YBa_{2+x}Cu_{3}O_{7-{\delta}}$ fired at $750^{\circ}C$ for 2 h. However, unexpected $T_c$ suppression even in Ba-excessive YBCO samples requires further identification.

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High Temperature Superconducting Pseudo-Lumped Element Bandpass Filter

  • Min, Byoung-Chul;Choi, Young-Hwan;Kim, Hong-Teuk;Moon, Seung-Hyun;Lee, Seung-Min;Oh, Byung-Du
    • Progress in Superconductivity
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    • v.1 no.1
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    • pp.42-46
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    • 1999
  • A high-temperature superconducting 1.78 GHz bandpass filter, designed for PCS applications, is presented. The structure consists of microstrip pseudo-lumped elements, which enables miniaturization of the filter. A 5-pole microstrip filter could be realized on a 37 mm $\times$ 9 mm $LaAlO_3$ substrate, using double-sided high-temperature superconducting $YBa_2Cu_3O{7-\delta}$ thin film. This filter showed 0.7 % fractional bandwidth, 0.3 dB insertion loss, and 12 dB return loss in the passband at 60 K.

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A Comparative Study on the Effective Surface Resistance of High-$T_c$ Superconductor Films as Measured by Using the S-parameter Circle-fit and the Lorentzian-fit Methods (S-parameter Circle-fit과 Lorentzian-fit 방법으로 측정된 고온초전도체 박막의 유효표면저항 비교)

  • Kim, Min-Jeong;Jung, Ho-Sang;Lee, J.H.;Lee, Sang-Young
    • Progress in Superconductivity
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    • v.9 no.2
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    • pp.146-151
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    • 2008
  • Measurements of surface resistance ($R_s$) of high temperature superconductor (HTS) films with accuracy are essential for microwave applications of HTS materials. In using the dielectric resonator method, uncertainties in the unloaded quality factor of the resonator cause significant errors in the measured $R_s$ of HTS films. We compare the Rs values of $YBa_2Cu_3O_{7-{\delta}}$ films calculated from the $Q_0$ as determined from the Lorentzian fit with that from the $Q_0$ as determined from the S-parameter circle-fit at temperatures between 15 K and 77 K. The two sets of values appeared to differ by 5%, 7%, 6%, and 11% at temperatures of 15, 60, 70, and 77 K, respectively, from each other, implying that careful error analysis needs to be performed in obtaining the $R_s$ of HTS films by using the Lorentzian-fit method, with the ones determined from the S-parameter circle-fit used as the reference.

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Effects of Precursor Composition on the $J_c$ of YBCO thin Films Prepared by DCA-MOD Method (DCA-MOD 방법으로 제조하는 YBCO 박막의 임계전류밀도에 미치는 전구체 조성의 효과)

  • Kim, Byeone-Jin;Kim, Hye-Joo;Lee, Jong-Beum;Lee, Hee-Gyoun;Hong, Gye-Won
    • Progress in Superconductivity
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    • v.9 no.1
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    • pp.91-95
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    • 2007
  • [ $YBa_2Cu_3O_{7-{\delta}}$ ] films have been prepared on $LaAlO_3$ (100) single-crystal substrates by the metal organic deposition using dichloroacetate precursors (DCA-MOD). DCA precursor solutions with different composition such as; Yttrium-excess(15 at%), barium-poor(25 at%), and a stoichiometric(Y:Ba:Cu=1:2:3) were prepared in order to investigate the effects of precursor composition on the properties of YBCO films prepared by DCA-MOD method. Coated films were calcined at low temperature up to $500^{\circ}C$ in flowing humid oxygen atmosphere. Conversion heat treatment was performed $800^{\circ}C$ for 2 h in flowing Ar gas containing 1000 ppm oxygen with a humidity of 9.45%. For the film prepared using excess yttrium composition, high critical current density ($J_c$) of $>2MA/cm^2$ was obtained whereas, for the films prepared using barium-poor composition, $J_c$ was lower than $1MA/cm^2$.

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High Temperature Superconducting Pseudo-Lumped Element Bandpass Filter

  • Choi, Young-Hwan;Kim, Hong-Teuk;Moon, Seung-Hyun;Lee, Seung-Min;Oh, Byung-Du;Min, Byoung-Chul
    • 한국초전도학회:학술대회논문집
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    • v.9
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    • pp.107-111
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    • 1999
  • A high-temperature superconducting 1.78 GHz bandpass filter, designed for PCS applications, is presented. The structure consists of microstrip pseudo-lumped elements, which make the miniaturization of the filter possible. A 5-pole microstrip filter can be realized on 37 mm ${\times}$ 9 mm LaAlO$_3$ substrate, using double-sided high-temperature superconducting YBa$_2Cu_3O_{7-{\delta}}$ thin film. This filter shows 0.7% fractional bandwidth, 0.3 dB insertion loss, and 12 dB return loss in the passband at 60 K.

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Effect of weak interlayer coupling on critical fluctuation in high $T_c$ superconductors

  • Kim, Jin-Tae;Kang, W.N.;Chung, S.H.;Ha, D.H.;Yoo, K.H.;Kim, M.S.;Lee, Sung-Ik;Park, Y.K.;Park, J.C.
    • Progress in Superconductivity
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    • v.1 no.1
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    • pp.1-8
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    • 1999
  • The magnetization and/or resistivity of high $T_c$ superconductors ($YBa_2Cu_3O_{7-\delta}$(YBCO) single crystal, $Bi_2Sr_2CaCu_2O_8$ (Bi-2212) single crystal, $Tl_2Ba_2CaCu_2O_8$ (Tl-2212) film, $HgBa_2Ca_2Cu_3O_8$ (Hg-1223) film) have been measured as a function of magnetic field H and temperature T. The extracted fluctuation part of the magnetization and conductivity exhibits a critical behavior consistent with the three-dimensional XY model. The dynamic critical exponent z does not sensitively vary with a type of the superconductors. The value of z ranges from 1.5 to $1.8{\pm}0.1$. However, the static critical exponent ${\nu}$ is the most largely increased in Tl-2212 that has a weaker interlayer coupling strength than YBCO; the value of ${\nu}$ is 0.669, 0.909, 1.19, and 1.338 for YBCO, Bi-2212, Hg-1223, and Tl-2212 respectively. The results indicate that the weak interlayer coupling along the c-axis of high $T_c$ superconductors near $T_c$ does not influence the dynamic critical exponent z (the same value of superfluid $^4He$), but significantly increases the static critical exponent ${\nu}$.

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