• Title/Summary/Keyword: $In_{2}O_{3}$

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Coloration Study of Red/Yellow β-FeOOH Nanorod using NH4OH Solution (NH4OH를 이용한 적황색 β-FeOOH 나노로드 길이에 따른 색상제어 연구)

  • Yu, Ri;Kim, IllJoo;Yun, JiYeon;Choi, Eun-Young;Pee, Jae-Hwan;Kim, YooJin
    • Journal of Powder Materials
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    • v.23 no.5
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    • pp.343-347
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    • 2016
  • Fe-based pigments have attracted much interest owing to their eco-friendliness. In particular, the color of nanosized pigments can be tuned by controlling their size and morphology. This study reports on the effect of length on the coloration of ${\beta}$-FeOOH pigments prepared using an $NH_4OH$ solution. First, rod-type ${\beta}$-FeOOH is prepared by the hydrolysis of $FeCl_3{\cdot}6H_2O$ and $NH_4OH$. When the amount of $NH_4OH$ is increased, the length of the rods decreases. Thus, the length of the nanorods can be adjusted from 10 nm to 300 nm. The color of ${\beta}$-FeOOH changes from orangered to yellow depending on the length of ${\beta}$-FeOOH. The color and phase structure of ${\beta}$-FeOOH is characterized by UV-vis spectroscopy, CIE Lab color parameter measurements, transmission electron microscopy (TEM), scanning electron microscopy (SEM), and powder X-ray diffraction (XRD).

The design of 111m high steel towers with 220kv double circuits crossing 12 km wide Bangladesh River (230KV 2회선승 111M 높이 철탑설계 (I) (강폭 12km인 Bangladesh Jamana강 횡단용))

  • 이재숙
    • Journal of the Korean Professional Engineers Association
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    • v.15 no.4
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    • pp.12-24
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    • 1982
  • East Parts of Bangladesh have been benifited by low cost energy generated by domestic natural gas but West parts where energy generated by imported fuel. Bangladesh Government authority has very much concerned to transmit the low cost electricity to the West from the East for past several years. To solve such concerns, cross-country 230kv double circuits Power transmission line was proposed, however there was a big obstacle for the realization of this line to cross the Jamuna river which has 12 km long width with a deep muddy river bed. A consultant engineering firm named Merz-Mclellan anyway finalized this plan and a world-wide bid was announced on June 31, 1979. Due to the expected difficulty to construct the towers on sea like area, only three construction groups have participated. including a Korean joint venture organization of Samsung-Korean Developement corporation-Kolon Electric Machinery company. After 3 months bid evaluation, contract was awarded to Korean Consosium and KEM Co was in charge of designing steel towers with anchor bolts and base plates beside to electrical engineering field. Then KEM Co have faced and over-comed many unenpected technical difficulties such as forced eccentricity joint on base plate, distorsion issue of 60mm thick plates welding, threading anchor bolts, tad heat treatment of some anchor bolts, disagreement from Consultant Engineer on multiplying factor of leg stresses for 45$^{\circ}$ wind and on reducing O.L.F for wind loads on cables for such 1220km long spans. After spending two years long period for designing and engineering towers, base plates, and anchor bolts, first shipment of tower was finally realized on Nov. 8, 1981 and on the other hand KDD has proceeded concrete caisson work on schedule at Jamuna river site and expected to complete tower erection and stringing of cables within this year of 1982 which was original completion target.

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A Study of Predictors of Children's Dual Gender Identity (아동의 양성형 성역할 정체감 예측요인)

  • Hong, Yean-Ran;Chei, Chung-Suk;Park, Jin-Ok
    • The Korean Journal of Emergency Medical Services
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    • v.9 no.1
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    • pp.5-13
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    • 2005
  • Purpose : The purpose of this study was to investigate dual gender identity, masculine gender identity, feminine gender identity, undifferentiated gender identity with related to Sex, home environments, parental child-rearing attitude of warmth, parental child-rearing attitude of control, role division of parents and determine predictors for dual gender identity. Method : Study subjects were $6^{th}$ grade of primary students with 2,118. Data was collected from Oct to Nov 2003 by using structured questionnaire. Results : ${\cdot}$ Among the children, 345 had masculine gender identity, 529 had feminine gender identity, 526 had undifferentiated gender identity, and 718 had dual gender identity. ${\cdot}$ There were significant differences in the children's sex, mother's age, father's age, mother's educational level, father's educational level, existence of mother's job, father's job, social economic status, sex of siblings, mother's job satisfaction, family structure, family atmosphere, child-rearing attitude(warmth and control), role division of parents($p{\leq}0.001$) among 4 groups. ${\cdot}$ The significant predictors for dual gender identity were children's sex (OR = 0,196, P =0.001), father's age(OR = 31.053, p = 0.020), mother's educational level(OR = 43,980, p = 0.001), father's job(OR=27.465, p = 0.001), social economic status(OR=O.941, p=0.001), sex of siblings(OR = 0.329, p = 0.005), mother's job satisfaction(OR = 0.673, p =0.001), family structure(OR = 0.887, p = 0.001), family atmosphere(OR = 23.786, p = 0.001), parental Child-rearing attitude of warmth(OR = 8.043, p = 0.001) and child-rearing attitude of control(OR = 0.666, p = 0.005), role division of parents(OR = 3.009, p = 0.001). Conclusions : These findings suggest the necessity of broad understandings about factors which influence dual gender role, and construction of combinative model. Also they suggest parent education for establishment of children's dual gender identity.

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Separation of Optical Isomers of DNS-Amino Acids in High-Performance Liquid Chromatography (고성능 액체크로마토 그래피에 의한 Dansyl-아미노산 광학이성질체의 분리)

  • Sun Haing Lee;Tae Sub O;Kyung Sug Park
    • Journal of the Korean Chemical Society
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    • v.30 no.2
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    • pp.216-223
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    • 1986
  • Separation of optical isomers of DNS derivatized amino acids by a reversed-phase high-performance liquid chromatography has been studied by adding a complex of an optically active amino acid (L-arginine) with the metal ion (Cu(II), Zn(II), Cd(II), Ni(II)) to the mobile phase. The separations are affected by the concentrations of acetonitrile, chelate and buffer. They are also affected by the pH and the kinds of metal and buffer. A separation mechanism, which is based on steric effect of the ligand exchange reaction for the formation of ternary complexes by the D,L-DNS-amino acids and the chiral additive associated with the stationary phase, is proposed to interpret the elution behaviors of D, L-dansyl-amino acids.

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Performance analysis for the Characteristics of Double/ Single Effect Hybrid type Absorption Chiller (일중/이중효용 하이브리드 타입 흡수식 냉동기 성능 특성에 관한 수치적 연구)

  • You, Da-Young;Song, Tae-Min;Lee, Jung-Byoung;Kim, Hyung-Jin;Im, Ick-Tae;Moon, Sang-Done;Park, Chan-Woo
    • Proceedings of the SAREK Conference
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    • 2009.06a
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    • pp.272-278
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    • 2009
  • The characteristics of hybrid type absorption chiller are studied numerically to use a waste hot water effectively. In the case of the full load, the concentration and temperature of LiBr solution are increase about $11^{\circ}C$, 1.3% respectively at the single effect generator by hot water. As a result, the heat of the high temperature generator are decrease, so the energy can be saved. As the partial load decreased the consumption ratio of fuels are decreased and the reduction ratio of fuels are increased. The variation of COP with the inlet temperature of hot water is higher than that of the flow rate of hot water. The effect of mean temperature difference with solution and hot water of the generator are higher that of flow rate of hot water, it can effect on COP which is sensitive to heat of generator.

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Grafting of MMA onto MCC through free radical method and its application to all natural cellulose composite film preparation (Microcrystalline cellulose에 자유 라디칼을 이용한 methyl methacrylate의 그래프팅 반응과 이를 이용한 천연복합필름의 제조)

  • Lee, Soo;Park, Sang-Hee;Jin, Seok-Hwan;Lee, Sun-Young
    • Journal of the Korean Applied Science and Technology
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    • v.25 no.4
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    • pp.459-468
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    • 2008
  • Methyl methacrylate(MMA) was grafted onto microcrystalline cellulose(MCC) with ceric ammonium nitrate(CAN) as a redox initiator at the various conditions. The cellulose triacetate(CTA) composite films added MCC and MMA-grafted MCC powders were prepared on a glass plate. The graft yield(GY) and graft efficiency(GE) of the grafted MCC were calculated with the simple equations by the weight balance method. The double bond of C=O on the grafted MCC surfaces was confirmed by the fourier transform infrared spectroscopy with attenuated total reflection(FT-IT ATR) spectrophotometer. After grafting, the degree of crystallinity of cellulose powders was decresed by judging from x-ray diffraction(XRD) data. Scanning electron microscope(SEM) photos showed the only solvent and CAN solution could change the roughness of MCC powders and the effect of powder dispersions in composite matrix. The tensile strength of MCC/CTA composite films was decreased with increase of MCC powder contents. When 5% grafted MCC was added, the tensile strength of grafted MCC/CTA composite films was increased from 82.3 MPa to 97.2 MPa. The thermal property of powders was also analyzed by the thermogravimetric analysis(TGA).

Characteristics of superconducting fault current limiters with various pattern shape (초전도 전류제한기의 패턴형상별 특성)

  • Choi, H.S.;Chung, H.S.;Choi, C.J.;Lee, S.I.;Chung, S.B.;Oh, G.K.;Lim, S.H.;Han, B.S.;Chung, D.C.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.07a
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    • pp.529-532
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    • 2003
  • Quench behavior of resistive superconducting fault current limiters (SFCLs) with various pattern shapes was investigated. The pattern shapes employed were meander, bi-spiral, and spiral shapes of identical line width, gap and margin. SFCLs were fabricated from YBCO thin films grown on two-inch diameter $Al_2O_3$ substrates under the same conditions. Resistance rise of current limiting elements was low at a spiral shape before the whole quench completion, which may act as a disadvantage for simultaneous quench in serial connection between current limiting elements, but the temperature tended to have similar values at higher voltages. On the other hand, bi-spiral shape was severe at insulation level between current limiting lines. When these aspects were considered, we concluded that a meander shape was appropriate to design for a resistive SFCL based on thin films except the concentration of electric field at edge areas of strip lines.

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A Study on the Improvement of Spot Welding Quality of Wire Cu Alloy by Taguchi Method for Dynamic Characteristics (동특성 다구찌 기법을 통한 Cu합금 와이어의 스폿용접 품질향상 연구)

  • Suk, Ho-sam;Kim, Yeun-sung;Yoo, Choon-burn
    • Journal of Korean Society for Quality Management
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    • v.45 no.4
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    • pp.1003-1020
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    • 2017
  • Purpose: The purpose of this study is to find the optimum working conditions for spot welding of wire Cu alloys to achieve high-level quality. The parts subject to spot welding are brush card assemblies, which are the main module of the electric movement method of the car seat. Methods: In this study, the signal-to-noise ratio(SN ratio) and the loss function [L(y)] are used as Taguchi method for dynamic characteristics. Results: The results of the study are as follows. First, the analysis of variance using SN ratio showed 6 significant factors(p = 0.1% or less) among 7 factors except press force. Second, the optimal design of the dynamic characteristics is the tip exchange cycle: 50,000 ea., the welding time is 110 ms, the pressing force is 11 kgf/cm2, the rise time is 40 ms, and the tip dressing is 3,000 ea., Tip angle is 12o and electric current is 1,800 A. Conclusion: The validity of the spot welding process of the manufacturer's brush card assembly was verified and proved to be consistent with the study results. The results of this study are expected to standardize the welding conditions and guarantee the quality level required by the customers.

Development of Instructional Materials and Test Items for Students' Spatial Ability (중학교 학생의 공간능력을 위한 학습자료와 문항개발)

  • Jung, In-Chul;ChoiKo, Sang-Sook;Park, Min-Goo
    • Journal of the Korean School Mathematics Society
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    • v.12 no.1
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    • pp.71-97
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    • 2009
  • The study was to develop the instruments including instructional materials and test items for enhancing spatial ability. A mixed methodology was chosen to achieve the purpose of the study. To find students' achievement, 5 units of instructional materials were developed through the qualitative method and test items were tested through the quantitative method with 152 of the 8th-graders. The strategies to develop the instructional materials were: firstly to focus on mathematics properties for developing spacial ability; secondly, to allow students to follow hierarchical procedure o[ mathematical properties from 2-d to 3-d; thirdly, to recognize what the manipulative can do and can not; and fourthly, to guide students tn develop the process oriented thought, not the result oriented thought. For the test, 25 items were analyzed to assess students' achievement using validity, difficulty, and discriminator.

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초고속 자기부상형 터보복합분자 펌프 기술 개발

  • Park, Yong-Tae;No, Seung-Guk;Kim, In-Chan;O, Hyeong-Rok
    • Proceedings of the Korean Vacuum Society Conference
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    • 2011.08a
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    • pp.88-88
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    • 2011
  • 복합분자펌프는 기존의 터보분자펌프 turbine blade에 spiral grooved를 추가하여 초고진공(10-8 Pa)에서 저진공(330Pa)까지 넓은 압력범위에서 사용할 수 있고 이 펌프를 사용함으로서 완전 oil free한 진공시스템을 만들 수 있는 특징을 가지고 있다. 특히, 회전체를 비접촉으로 지지하는 자기베어링 방식을 적용함으로써, 진동은 극히 작고 베어링수명은 길면서 중저진공에 대한 배기속도가 크고 임의의 방향으로 접속이 가능하여 반도체 및 디스플레이 제조 공정과 같은 첨단산업의 다양한 분야에 쉽게 적용되고 있으며, 그 적용 분야와 시장은 계속 성장하고 있다. 고 진공과 배기 속도의 달성을 위해서, 고속으로 이동하는 격면과 기체분자를 충돌시켜, 기체 분자를 원하는 방향으로 유도하는 작동원리를 가지고 있다. 특히 공기분자의 밀도가 매우 낮은 희박가스 상태에서 고속 회전하는 blade로 공기분자를 쳐 내면서 작동됨으로써 날개의 상하 압력차에 의한 공기력보다도 날개의 고속회전이 매우 중요시 되고 압력으로는 10-1 Pa 이하의 분자영역에서 그 성능을 최고로 발휘 할 수 있다. 이러한 복합 펌프의 주요 장점은 다음과 같다. 1. 10-8 Pa (10-10torr)~10 Pa (1 torr) 까지 넓은 영역에서 배기가 가능하다. 2. 탄화수계의 대하여 높은 압축특성을 가지고 있고, 윤활유를 사용하지 않으므로 얻을 수 있는 진공상태가 고청정하다(oil free). 3. 정밀 5축제어 자기베어링으로 완전히 부상하여 회전함으로서 마모가 없고 진동이 최소화하였을 뿐만 아니라, 또한 운전음도 거의 없다. 4. 설치조건에 제한이 없고 고장이 거의 없다. 본 논문에서는 이러한 복합분자펌프의 개발을 위하여, 상기 연구기관에서 수행된 내용을 소개하고 있으며, 펌프 시스템의 기본 설계 및 자기베어링 시스템의 설계 결과 및 수치해석 결과를 나타내었다.

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