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검색결과 51건 처리시간 0.035초

Comparison of Different Solid-Phase Extraction Methods for the Analysis of Heterocyclic Amines from Pan-Fried Pork Meat (가열 조리된 돼지고기의 Heterocyclic Amines 분석을 위한 Solid-phase 추출 방법의 비교)

  • Lee, Jae-Hwan;Back, Yu-Mi;Lee, Kwang-Geun;Shin, Han-Seung
    • Food Science of Animal Resources
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    • 제28권5호
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    • pp.637-644
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    • 2008
  • Four different extraction and purification methods were evaluated to determine the heterocyclic amines (HCAs) in fried pork patties. Pork patties were cooked in the teflon-coated electric frying pan at $230^{\circ}C$ for 8 min per side. HCAs in the fried pork patties were extracted and purified using four different solid-phase extraction (SPE) methods and quantitated by LC-MS (API-ESI). Recovery of four different extraction and purification methods was evaluated by comparing the HCAs amounts quantified by the standard addition method. Validation of extraction and purification methods for fried pork patties was determined to establish accurate sample preparation. The recoveries of HCAs from different SPE methods were calculated. The recovery yields were 15.7-68.7% (Polar amine group) and 25.0-74.7% (less-polar amine group) in method A. Method D provided recovery yields ranging from 14.1% to 68.7% in polar amine groups and from 3.0% to 72.3% in less-polar amine groups, respectively. Modified procedures of Method A and D were the most suitable extraction and purification method for HCAs analysis from fried pork patties.

A Short Test of English Silent Word Reading for English Language Learners

  • Kalindi, Sylvia C.;McBride, Catherine;Chan, Shingfong;Chung, Kien Hoa Kevin;Lee, Chia-Ying;Maurer, Urs;Tong, Xiuhong
    • Child Studies in Asia-Pacific Contexts
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    • 제5권2호
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    • pp.95-105
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    • 2015
  • We developed a test of English silent word reading, following work by Mather, Hammill, Allen and Roberts (2004) and Bell, McCallum, Krik, Fuller, and McCane-Bowling (2007), in order to tap Hong Kong Chinese children's reading of English as a foreign language. We created one subtest of individual word reading and another of word reading contextualized within sentences; together, these tests require no more than 10 minutes for administration. In Study 1, we administered the entire test to 552 second grade Hong Kong Chinese children between the ages of 70 and 121 months old, from five different primary schools. The association between the subtests of English silent word reading and contextual reading was positively correlated (.78). In Study 2, 77 Hong Kong Chinese second graders were tested on our newly developed English silent word reading test, together with non-verbal IQ, an English word reading and a Chinese character recognition test (both read aloud). With age and non-verbal IQ statistically controlled, there was a significant correlation between English silent word reading and the more standard English word reading, read aloud, (.78); the association between English silent word reading and Chinese character recognition was also positively correlated (.49). This newly created test is a quick and reliable measure, suitable for both educators and researchers to use to identify poor readers who learn English as a foreign or second language.

Relationship between Intelligence and Emotional Intelligence (유아의 지능과 정서 지능의 관계)

  • 신미리;박정옥
    • Journal of Gifted/Talented Education
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    • 제13권1호
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    • pp.97-116
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    • 2003
  • The purpose of this study was to examine the relationship between children's cognitive intelligence and emotional intelligence and to examine the relationship of each subordinate factors. Also, this study investigated whether there is a difference in emotional intelligence according to level of intelligence and gender. The subjects consisted of 104 children enrolled in a kindergarten in the Kangnam area. These children were given two tests, Multimensional Cognitive Abilities Tests for Children(MCAT-C) and Emotional Intelligence Test(EIT). The results of this study are as follows. First, there was a significant relationship between cognitive intelligence(IQ) and emotional intelligence. And there were some correlation between intelligence(IQ) and regulation of emotion(the subordinate factor of emotional intelligence). Second, there was a statistically significant difference in the total score of emotional intelligence, empathy, regulation of emotion(the subordinate factor of emotional intelligence) according to intelligence level. Third, there was a statistically significant difference in emotional intelligence according to gender. Girls received relatively higher scores than boys in the total score of emotional intelligence, empathy, regulation of emotion(subordinate factors of emotional intelligence).

Fabrication and performance and stability tests of Bi-2223 pancake magnet

  • Sohn, M.H.;Cha, M.K.;Lee, J.K.;Cho, Y.S.;Ha, H.S.;Jang, H.M.;Lee, N.J.;Kim, B.J.;Kim, H.K.;Kim, Y.C.;Jeong, D.Y.
    • 한국초전도학회:학술대회논문집
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    • 한국초전도학회 2000년도 High Temperature Superconductivity Vol.X
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    • pp.241-247
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    • 2000
  • 77 K와 self-field에서 22 A 의 Ic 를 갖는 길이 120 m, 19-심 Bi-2223상 선재를 제조하여, 두 개의 double pancake 코일로 구성된 proto-type 고온초전도 자석을 설계, 제작하여 이 자석에서의 4.2 K와 77 K에서의 I-V 특성과 운전 특성을 평가한 결과, 이 자석은 77 K 등온조건에서는 9.5 A 의 Ic를, 77 K 헬륨가스 속에서는 8.3 A 의 Ic를 나타내었고, 4.2 K 등온조건에서는 93.7 A 의 Ic와 102 A 의 Iq를, 4.2K헬륨가스 속에서는 88.4A의 Ic 와 92.0 A 의 Iq를 나타내어, 이 자석은 4.2 K 와 77 K 의 등온조건에서 각각 0.58 T 와 0.06 T 의 자장을 발생하였는데, 이는 해석적 방법으로 계산한 결과와 잘 일치하였다. 그리고 이 자석이 전도냉각되어 4.2 K 에서 운전될 때의 안정성 특성평가로서, Ic 보다 약간 큰 전류인 89 A 를 인가한 결과, 전류인가 후 82.6초 후에 quench가 발생하였는데, 이 quench는 네 번째 pancake의 전류도입선부 연결부에서와 약간 늦지만 첫 번째 pancake의 전류도입선부 연결부에서 거의 동시에 개시되어 전체로 파급된 것으로 사료되었는데, Ic 가 낮은 첫번째 pancake에서 더 높은 전압 강하가 나타났다. 또한 장착된 heater를 통하여 77 K 에서 8.9 A 의 전류로 운전되고 있는 코일에 146 joule 의 열을 가했을 때 quench 가 일어났는데, 이때 quench 는 방위각 방향의 Bi-2223/Ag 선재를 따라서 보다 Kapton 절연층을 관통하는 선재의 반경방향으로 훨씬 빨리 전파하였다.

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Evaluation of the in vitro biological activity of selected 35 chemicals (35종의 특정 화학성분들의 in vitro 활성 평가)

  • Shin, Han-Jae;Sohn, Hyung-Ok;Park, Chul-Hoon;Lee, Hyeong-Seok;Min, Young-Keun;Hyun, Hak-Chul
    • Journal of the Korean Society of Tobacco Science
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    • 제29권1호
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    • pp.30-40
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    • 2007
  • The objective of this study was to investigate the contribution of various smoke constituents to the toxicological activity of total particulate matter(TPM) or the gas/vapor phase(GVP). These components included phenol compounds, aromatic amines, polycyclic aromatic hydrocarbons, heterocyclic amines, and carbonyl compounds. The mutagenic and cytotoxic potencies were assessed using the Salmonella mutagenicity assay with S. typimurium TA98 strain and the neutral red uptake cytotoxicity assay(NRU) with BALB/c 3T3 fibroblast cells, respectively. The Salmonella mutagenicity test showed that heterocyclic amines exhibited significantly higher levels of toxicity compared to other smoke constituents. Among them, 2-amino-3,4-dimethylimidazo[4,5-f]quinoline(MeIQ) was shown the most mutagenic compound with a specific mutagenicity of $7.9{\times}10^5\;revertants/{\mu}g$. An analysis of the possible contribution revealed that MeIQ account for only 0.85% of the 2R4F-TPM mutagenicity in TA98. NRU data demonstrated that high cytotoxic activity was obtained for hydroquinone, formaldehyde, and acrolein. Based on the results of the present study, the contribution of acrolein to the cytotoxicity of the GVP fraction was calculated as 61%. Thus, a large proportion of the cytotoxic activity of this complex mixture, cigarette smoke gas phase, can be attributed to the acrolein.

CLINICAL EVALUATION OF CHILDREN WITH INATTENTION AND HYPERACTIVITY IN A PSYCHIATRIC CLINIC (주의산만과 과잉운동을 주소로 하는 정신과 내원 아동들의 임상 평가)

  • Kweon, Yong-Sil
    • Journal of the Korean Academy of Child and Adolescent Psychiatry
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    • 제13권1호
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    • pp.93-103
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    • 2002
  • The aim of this study is to examine the diagnostic profiles and related clinical variables of children with attention and hyperactivity in psychiatric outpatient clinic. Seventy one children with age range of 5 to 14 were diagnosed by DSM-IV, and assessment battery including KEDI-WISC, KPI-C, ADS(ADHD Diagnostic System) were completed. The subjects were divided into 3 diagnostic groups:ADHD only(n=17), ADHD comorbid(n=27), Other diagnosis(n=27). The results were as follows:In ADHD comorbid group, tic disorder, developmental language disorder, borderline intellectual function, oppositional defiant/conduct disorder, and learning disorder were combined in descending order. Other diagnosis group consisted of tic disorder, borderline intellectual function, depression/anxiety, oppositional defiant/conduct disorder, and others. There were significant differences in IQ, PIQ, and VIQ among the three groups, and ADHD only group showed higher scores of IQ and VIQ than ADHD comorbid group. On the KPI-C, there were no significant differences in all subscales among the three groups. On the visual ADS, omission error and sensitivity showed significant differences among the three groups, and ADHD comorbid group represented higher omission error and lower sensitivity than other diagnostic group. The findings indicated that the inattention and hyperactivity symptoms could be diagnosed into diverse psychiatric disorders in child psychiatry, and ADHD children with comorbidity will show more problems in academic performance and school adjustment.

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Studies on the Culture of Ergot Fungus(IV) -Culture of Korean Ergot Fungus- (맥각균(麥角菌)의 배양(培養)에 관한 연구(硏究)(IV) -한국산(韓國産) 맥각균(麥角菌)의 배양(培養)-)

  • Kim, Byong-Kak;Shim, Mi-Ja;Choi, Eung-Chil;Park, Young-In
    • Korean Journal of Pharmacognosy
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    • 제6권1호
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    • pp.9-13
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    • 1975
  • To isolate ergot strains which are capable of growing and producing alkaloids in submerged culture, strains were isolated from the sclerotia parasitizing the Graminae plants in Korea and the experiments of submerged culture of these strains yielded the following results: 1) The mycelia which were respectively isolated from the sclerotia parasitizing Agropyron semicostatum $N_{EES}$, Arundinella hirta $T_{ANAKA}$ var. ciliata $K_{OIDSUMI}$, Ischaemum anthephoroides $M_{IQ}$. var. eriostachyum $H_{ONDA}$, and Phleum pretense L. grew in Medium D by submerged culture. 2) When the strain of the ergot of Agropyron semicostatum was inoculated into six different nutrient solutions for submerged culture, its mycelium grew well in Media C, D and F, but produced alkaloids only in Medium C, indicating that Medium C is relatively suitable for the strain. 3) The extraction of the alkaloids from the culture broth by ether and T.L.C. analysis of the extract showed that it contained at least two types of alkaloids.

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Carotenoids Components of Tunicata, Shellfishes and Its Inhibitory Effects on Mutagenicity and Growth of Tumor Cell (미색동물 및 패류의 Carotenoids 색소성분과 돌연변이 및 종양세포 증식의 억제효과)

  • 하봉석;백승한;김수영
    • Journal of the Korean Society of Food Science and Nutrition
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    • 제29권5호
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    • pp.922-934
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    • 2000
  • To investigate the composition of carotenoids present in marine organisms and the biological activity of the carotenoids, carotenoids of the muscles and tunic of tunicates and shellfishes were isolated and identified. Anitmutagenic activities of the carotenoids for S. typhimurium TA 98 and cytotoxic activity for cancer cell lines were determined. Total carotenoid contents in the muscle of tunicata ranged from 18.65 mg% to 2.39 mg%. The highest amount of the total carotenoid was found in the muscle of Halocynthia aurantium, followed by Styela clava (HERDMAN), H. roretzi, H. hilgendorfi f. igaboya, H. hilgendorfi f. retteri, S. plicata (LESUEUR) in order. Interestingly, total carotenoid content in the muscle of S. clava (HERDAMAN) was higher than that of H. roretzi. Total carotenoid content of all tunicata, other than H. aurantium and H. roretzi, were higher in muscle than tunic. The major carotenoids in H. roretzi, H. aurantium, S. plicata (LESUEUR), and S. clava (HERDAMAN) were cynthiaxanthin (25.1∼42.2%), halocynthiaxanthin (9.7∼26.3%), diatoxanthin (8.0∼18.7%) and β-carotene (7.7%∼21.7%). Similarly, cantaxanthin (19.6%), cynthiaxanthin (15.4%), halocynthiaxanthin (14.8%), and (3R, 3'R), (3S, 3'S)-astaxanthin (22.6%) in H. hilgendorfi f. retteri and fucoxanthin (26.6%), cynthiaxanthin (21.8%), halocynthiaxanthin (15.2%), and β-carotene (9.3%) in H. hilgendorfi f. igaboya were major carotenoids in both tunicate. However, the composition of carotenoids in muscle and tunic of tunicata was similar each other. Among the shellfishes examined, total carotenoid content of the muscle of Peronidia venulosa (Schrenck) and Corbicula fluminea, and of the gonad of Atrina pinnata and Chlamys farreri, was ranged from 2.51 to 6.83 mg% which were relatively higher than that of other shellfishes. The composition of the carotenoids of shellfishes, which might depend upon their living environments, was varied. But cynthiaxanthin (15.9∼39.0%) and zeaxanthin (9.6∼21.9%) in gonad of C. farreri, and muscles of Buccinum Volutharpa perryi (JAY) and Crassostrea gigas, cynthiaxanthin (21.5∼48.6%) and mytiloxanthin (14.6%) in muscle of C.fluminea and gonad of A. pinnata, and canthaxanthin (60.6%) and isozeaxanthin (20.5%) in muscles of P. venulosa (Schrenck), and β-carotene (23.7%∼37.8%) and zeaxanthin (18.2∼20.4) in muscles of Semisulcospira libertina and Meretrix lusoria were major carotenoids. Interestingly, diester type-carotenoids were present along with free type-carotenoids in muscles of C. gigas. antimutagenic effect of the carotenoids isolated from tunicata and shellfishes against 2-amino-3-methylimidazol [4,5-f]quinoline (IQ) for S. typhimurium TA 98 was proportional to the amount (20, 50 and 100㎍/plate) treated. Mutagenicity of IQ was significantly reduced by astaxanthin, isozeaxanthin, mytiloxanthin and halocynthiaxanthin, whereas the mutagenicity of aflatoxin B₁(AFB₁) was significantly reduced by β-carotene, isozeaxanthin, and mytiloxnthin. Growth inhibition effect of carotenoids isolated from tunicata and shellfishes for cancer cell was proportional to the amount (5, 10, and 20㎍/plate) treated. The growth of HeLa cell by β-carotene, cynthiaxanthin, astaxanthin and halocynthiaxanthin, NCI-H87 cell by β-carotene, astaxanthin, cynthiaxanthin, and halocynthiaxanthin, HT-29 cell by β-carotene, cynthiaxanthin, mytiloxanthin and halocynthiaxanthin, and MG-63 cells by β-carotene, cynthiaxanthin, astaxanthin, canthaxanthin and halocynthiaxanthin were statistically reduced.

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Single-Phase Impedance-Source Dynamic Voltage Restorer (단상 임피던스-소스 동적 전압 보상기)

  • Park, H.J.;Jung, Y.G.;Lim, Y.C.
    • Proceedings of the KIPE Conference
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    • 전력전자학회 2008년도 하계학술대회 논문집
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    • pp.458-461
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    • 2008
  • This paper deals with a single-phase impedance-source dynamic voltage restorer (Impedance-DVR) to mitigate voltage sag/swell for the critical loads. The proposed system is composed of passive filter and impedance-source topology inverter. As an ESS(Energy Storage System) of the proposed system is employed the Proton Exchange Membrane Fuel Cells (PEMFC). To calculate and control the compensation voltage, single-phase $^id-^iq$ theory in dq rotating reference frame and PI controller are used. Simulation results under voltage sag and swell are presented to show the performance.

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Standardization Trends in Open Radio Equipment Interface (ORI 표준화 동향)

  • Jo, G.D.;Lee, K.C.;Ahn, D.H.;Kwon, D.S.
    • Electronics and Telecommunications Trends
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    • 제28권3호
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    • pp.106-114
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    • 2013
  • 과거 이동통신용 기지국은 기저대역 처리부와 안테나를 포함하는 RF부가 일체형으로 제작되었으나, 4세대 이동통신에서는 기술/경제적인 이유로 BBU(Base Band Unit)와 RRH(Remote Radio Head)로 분리하여 구성되는 분산형 기지국 구조를 택하는 추세이다. BBU와 RRH 간 인터페이스로 널리 사용되어온 OBSAI, CPRI외에 2010년 ORI가 출현하여 표준화가 한창이다. ORI는 시장에서 널리 사용되는 CPRI(Common Public Radio Interface)의 Vendor Specific 부분으로 인해 제조사간 호환성이 보장되기 어려운 문제를 보완하기 위하여 탄생한 인터페이스 규격으로써, CPRI를 기반으로 하면서 표준으로써의 완성도를 높인 표준이라 할 수 있다. 또한 관련 표준으로는 유일하게 IQ 데이터 압축알고리즘의 표준화를 고려하고 있다. 본고에서는 ORI의 표준화 현황과 기술적인 이슈를 소개하고, 국내의 대응 현황을 알아본다.

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