• Title/Summary/Keyword: $FeCl_3 $

Search Result 921, Processing Time 0.026 seconds

Production of yuzu granules using enzyme treated yuzu pulp powder and evaluation of its physiochemical and functional characterization (유자박 식이섬유를 이용한 유자과립 제조 및 이화학적 특성조사)

  • Seong, Hyeon Jun;Lee, Bo-Bae;Kim, Duck-Hyun;Lee, Seung-Hyun;Ha, Ji-Young;Nam, Seung-Hee
    • Korean Journal of Food Science and Technology
    • /
    • v.53 no.4
    • /
    • pp.382-390
    • /
    • 2021
  • In this study, solubilized yuzu pulp powder (EYP) was produced using enzyme treated yuzu pulp powder (YP) and used to manufacture yuzu granules (0-20% EYP content). The physicochemical, product stability, and functional properties of Yuzu granules were compared among five enzyme treatments. Among the five treatments, CL had the highest YP solubilization yield (48.68%). Microstructural observation of EYP using FE-SEM revealed that its surface became irregular and porous after enzymatic treatment. Compared to YP, EYP had 2 times lower insoluble dietary fibers and 3 times lower hemicellulose and cellulose content. Among the yuzu granules, IV (yuzu granules with 15% EYP) had an excellent water and oil holding capacity and flowability. IV granule had the highest narirutin and hesperidin content of 3.4 mg and 2.2 mg/g DW, respectively and the highest antioxidant (68.4%) and tyrosinase inhibitory activities (82.5%). Therefore, EYP or granule with EYP can be used as a functional component in food industry or pharmaceutical field.

The Characterization of PM, PM10, and PM2.5 from Stationary Sources (고정배출원의 먼지 크기별 (PM, PM10, PM2.5) 배출 특성 연구)

  • Kim, JongHo;Hwang, InJo
    • Journal of Korean Society for Atmospheric Environment
    • /
    • v.32 no.6
    • /
    • pp.603-612
    • /
    • 2016
  • The objective of this study was to estimate the emission characteristics for PM, $PM_{10}$, and $PM_{2.5}$ in the various stationary sources. The particulate matters collected in the various stationary sources such as power plants (Coal and B-C oil), incinerators(municipal and industrial waste), and glass furnaces. The PM and $PM_{10}$, PM and $PM_{2.5}$, $PM_{10}$ and $PM_{2.5}$ samples were collected using the cyclone type $PM_{10}$, $PM_{2.5}$ samplers and 30 species(19 inorganic species, 9 ionic species, OC and EC) were analyzed by ICP, IC, and TOR/IMPROVE methods. The mass concentrations of PM, $PM_{10}$, $PM_{2.5}$ from nine stationary sources ranged $0.63{\sim}9.58mg/Sm^3$, $0.26{\sim}7.47mg/Sm^3$ and $0.13{\sim}6.34mg/Sm^3$, respectively. The level of $PM_{10}$, $PM_{2.5}$ portion in PM calculated 0.63~0.99, 0.38~0.94, respectively. In the case of emission trend for species, power plant showed high concentrations for Al, Mg, Na, Si, V and $SO_4{^{2-}}$, respectively. Also, Ca, Fe, K, Si, $Cl^-$, and $K^+$ showed high in incinerator. In the case of glass furnace, Na, Pb, K, Si, $Na^+$ and $SO_4{^{2-}}$ represented high concentrations. Power plant showed higher EC/OC concentrations than other sampling sites. These results suggest the possible role for complement establishment process of emission inventory and emission management for PM.

Chemical Composition of Respirable PM2.5 and Inhalable PM10 in Iksan City during Fall, 2004 (익산지역 가을철 대기 중 호흡성 및 흡입성 먼지입자의 화학조성)

  • Kang, Gong-Unn
    • Journal of Environmental Health Sciences
    • /
    • v.36 no.1
    • /
    • pp.61-71
    • /
    • 2010
  • Intensive measurements of airborne respirable $PM_{2.5}$ and inhalable $PM_{2.5}$ were conducted in the downtown area of Iksan city. The $PM_{2.5}$ and $PM_{2.5}$ samples were collected twice a day in the Iksan city of Korea from October 17 to November 1, 2004. The purpose of the study was to determine the inorganic water-soluble components and trace elements of $PM_{2.5}$ and $PM_{2.5}$ in the atmospheric environment and estimate the contribution rate of major chemical components from a mass balance of all measured particulate species. The chemical analysis for PM samples was conducted for water-soluble inorganic ions using ion chromatography and trace elements using PIXE analysis. The mean concentrations of respirable $PM_{2.5}$ and inhalable $PM_{2.5}$ were $51.4{\pm}29.7$ and $79.5{\pm}39.6\;{\mu}g/m^3$, respectively, and the ratio was 0.62. The ion species of $NO_3$, $SO_4^2$, and $NH_4^+$ were abundant in both $PM_{2.5}$ and $PM_{2.5}$. These components predominated in respirable $PM_{2.5}$ fraction, while $Na^+$, $Mg^{2+}$, $Ca^{2+}$ mostly existed in coarse particle mode. Elemental components of S, Cl, K, and Si were abundant in both $PM_{2.5}$ and $PM_{2.5}$. These elements, except for Si, were considered to be emitted from anthropogenic sources, while Si, Al, Fe, Ca existed mainly in coarse particle mode and were considered to be emitted from crustal materials. The averaged mass balance analysis showed that ammonium nitrate, ammonium sulfate, crustal component, and other trace elements were composed of 18.4%, 13.2%, 4.8%, 3.5% for PM2.5 and 17.0%, 11.6%, 13.7%, 4.4% for $PM_{2.5}$, respectively.

Agricultural Water Quality along the Keum River (금강수계 농업용수의 수질)

  • Lee, Jong-Tae;Lee, Jin-Il;Nam, Yun-Gyu;Han, Kyu-Heung
    • Korean Journal of Environmental Agriculture
    • /
    • v.18 no.2
    • /
    • pp.122-125
    • /
    • 1999
  • The water quality of the Keum river was surveyed at 4 sites from April to September in 1995 and 1997. Average values of inorganic contents analyzed in 1997 were pH 7.2, EC 0.18dS/m, $NH_4-N$ 0.60mg/l, $K^+$ 4.12mg/l, $Ca^{2+}$ 12.12 mg/l, $Mg^{2+}$ 2.75mg/l, $Na^+$ 15.1mg/l, $NO_3-N$ 1.97mg/l, $PO_4^{3-}$ 0.15mg/l, $PO_4^-$ 18.9mg/l, $Cl^-$ 21.8mg/l, Fe 0.22mg/l, COD 19.7mg/l. On the basis of these values, it was suitable for the irrigation source. Water pH of the Keum river ranged from 6.7 to 8.0. EC of the Daecheong-dam was maintained below 0.13dS/m, but those of the middle and lower stream were ranged from 0.13dS/m to 0.32dS/m. Monthly average values of all the ration contents were the highest in April and were decreased thereafter. And it was slightly increased in September. However $NO_3-N$, $SO_4^{2-}$ contents were higher in June than any other months. All the inorganic contents were the highest at Taepyeong-ri, Yeongi-gun due to sewage water and livestock wastes. The inorganic contents were negatively correlated with precipitation, generally.

  • PDF

Physico-chemical Characteristics of the Inhibitory Substance on the Germination of Mung Bean (녹두 발아 조해물질(阻害物質)의 이화학적(理化學的) 성질(性質))

  • Kim, Kwang-Hyeon
    • Journal of the Korean Society of Food Science and Nutrition
    • /
    • v.14 no.1
    • /
    • pp.57-60
    • /
    • 1985
  • The inhibitory substance on the growth of mung bean seedling was amorphous crystal that had a single spot on silica gel thin layer chromatography under ultra-violet irradiation in dark room. The Rf value was 0.85 in n-butanol-acetic acid-formic acid-water(15 : 12 : 3 : 10) system, and 0.92 in n-butanol-acetic acid-water(4 : 1 : 5) system, respectively. Biochemical reaction of the inhibitor was negative to $FeCl_3$, pyrimidine, ninhydrine, folin, fehling, Salkowski and Ehrlich reaction, but the inhibitor had a blue fluorescence from irradiation of ultra-violet rays and had maximum absorption at 252nm on UV spectrum. On IR spectrum, the Peaks of the inhibitor appeared at $3300{\sim}3500,\;2900{\sim}3000,\;1600{\sim}1700,\;and\;1400cm^{(-1)}$. The strain tested was identified to be similar Streptomyces iuteogriseus by morphorogical and physiological characteristics.

  • PDF

A Study for Characteristics of PM10 in the Subway Passenger Cabins (지하철 전동차 객실에서의 PM10 오염특성 파악에 관한 연구)

  • Oh, Mi-Seok;Park, Duck-Shin;Park, Eun-Young
    • Journal of Korean Society for Atmospheric Environment
    • /
    • v.27 no.5
    • /
    • pp.523-533
    • /
    • 2011
  • This study had the aim of characteristics of $PM_{10}$ in subway cabins. $PM_{10}$ was measured by times of day (rush and non rush hours) and seasons with real time $PM_{10}$ sampler on the subway cabins of line 7. Filter samples were collected for evaluation of their elemental composition as well as identification of major sources of $PM_{10}$ using a receptor model, PMF. $PM_{10}$ concentration were the highest in the winter season both in the rush and non rush hours at 152.8 ${\mu}g/m^3$, 90.2 ${\mu}g/m^3$ respectively. The $PM_{10}$ concentrations in rush hour were 30% higher compared to non rush hours. Based on the chemical information, the composition rare of inorganic elements was 52.5%, anions were 10.2% and others were 37.3%. Fe was the most abundant element and significantly correlated (p.0.01) with Mn (r=0.97), Ti (r=0.91), Cr (r=0.88), Ni (r=0.89) and Cu (r=0.88). Characterized $PM_{10}$ sources by PMF in the cabin were soil and road dust related sources (27.2%), railroad related sources (47.5%), secondary nitrate sources (16.2%) and a Cl-factor mixed with a secondary sulfate source (9.1%).

Loess Dyeing of Soybean Fabrics (대두직물의 황토염색)

  • Lee, Sol;Lee, Shin-Hee
    • Fashion & Textile Research Journal
    • /
    • v.17 no.6
    • /
    • pp.1004-1012
    • /
    • 2015
  • The purpose of this study is to investigate the loess dyeability of soybean fabric using loess as colorants. Recent days, various textile products such as inner wears, sheets and interior goods are manufactured using materials dyed with loess emphasizing its improved metabolism, anti-bacterial, deodorizing properties, and far infrared ray emissions. Soybean fabric was dyed with loess solution according to concentration of loess, dyeing temperature and dyeing time. To improve washing fastness, soybean fabric and dyed soybean fabric with loess were mordanted by mordanting agents such as sodium chloride(NaCl), Acetic acid(CH3COOH) and Aluminium Potassium Sulfate(AlK(SO4)2·12H2O). Dyeability and color characteristics of dyed soybean fabric were obtained by CCM observation. Particle size distribution of loess, the dyeability(K/S) of soybean fabric, morphology and washing durability of loess dyed soybean fabric were investigated. The results obtained were as follows; Mean average diameter of loess was 1.08µm. The main components of loess used in this study were silicon dioxide(SiO2), aluminium oxide(Al2O3), and iron oxide(Fe2O3). The content of these three component was above 75 weight %. The dyeability of soybean fabric was increased gradually with increasing concentration of loess. The optimum dyeing temperature and dyeing time were 90℃ and 60minutes expectively. The fastness to washing according to concentration of loess and mordanting method indicated good grade result as more than 4 degree in all conditions.

Production of a novel endo-inulinase from Arthrobacter sp. S37 (새로운 endo-inulinase 생산 균주의 선발 및 효소의 생산)

  • Kim, Kyoung-Yeon;Kang, Su-Ll;Kim, Su-Il
    • Applied Biological Chemistry
    • /
    • v.39 no.2
    • /
    • pp.99-103
    • /
    • 1996
  • A bacterial strain producing a novel endo-inulinase, hydrolysing inulin into oligosaccharides was isolated from soil and identified as Arthrobacter sp. S37 The enzyme production was induced by inulin and jerusalem artichoke extract. The maximum enzyme production was obtained with medium containing 1.5% jerusalem artichoke extract, 1.0% yeast extract, $0.5%\;NaNO_3,\;0.05%\;MgSO_4{\cdot}7H_2O,\;0.05%\;KCl,\;0.0016%\;FeCl_3{\cdot}6H_2O\;and\;0.05%\;KH_2PO_4$. The optimum temperature and pH for the enzyme production were $30^{\circ}C$ and 8.0, respectively. Under the optimum condition, the enzyme activity in the culture broth reached at maximum, 10.8 units/ml after cultivation for 24 hours.

  • PDF

Discoloration of Woods (2) - 36 Commercial Hardwoods Grown in Korea - (목재(木材)의 오염(汚染)에 의한 변색(變色) (2) - 한국산(韓國産) 활엽수재(闊葉樹材)의 화학적(化學的) 변색(變色) -)

  • Ahn, Kyung-Mo;Kong, Young-To;Jo, Jae-Myeong
    • Journal of the Korean Wood Science and Technology
    • /
    • v.14 no.1
    • /
    • pp.55-60
    • /
    • 1986
  • Discoloration sensitivities of woods grown in this country haven't reported yet. Therefore we examined discoloration sensitivities of domestic wood specimens to iron (0.1 %, $FeCl_3.6H_2O$), alkali (pH 12.0, NaOH). acid (pH 1.0, $C_2H_2O_4$) and exposing to sunlight (40 hrs), Thirty-six hardwood species were collected and examined. All specimens were prepared from heartwoods of the collected species. But the specimens of 4 Betula species were divided into sapwoods and heartwoods. By iron stain, the color differences (${\Delta}E$) of 21 wood specimens including one Betula sapwood showed above 12.0, which means strong discoloration sensitivities, and of 3 specimens including one Betula sapwood showed below 2.5, which means weak discolorations. The most strong iron discoloration species was Jungkukgulpi-namu (Pterocarya stenoptera). By alkali stain, the color differences (${\Delta}E$) of 3 wood specimens showed above 9.0, which means strong discoloration sensitivities, and of 18 wood specimens including 4 Berula sapwoods showed below 2.5, which means weak discolorations. By acid stain, the color differences (${\Delta}E$) of 6 wood specimens showed above 10.0 which means strong discoloration sensitivities, and of 12 wood specimens including one Betula sapwoods showed below 2.5, which means weak discolorations. By exposing to sunlight, the color differences (${\Delta}E$) of 31 wood specimens including one Betula sapwoods showed below 6.5, which means, strong discoloration sensitivities, and of only one specimens showed below 2.5, which means weak discoloration. The most strong discoloration species by exposing to sunlight was Guirung-namu (Prunus padus). In general, it was shown that hardwoods grown in Korea were most subject to change of color by exposing to sunlight and next were by iron stain. Domestic hardwoods showed some differences in discoloration sensitivities from domestic softwoods previously reported.

  • PDF

EFFECTS OF SURFACTANTS ON THE FENTON DEGRADATION OF PHENANTHRENE IN CONTAMINATED SEDIMENTS

  • Jee, Sang-Hyun;Ko, Seok-Oh;Jang, Hae-Nam
    • Environmental Engineering Research
    • /
    • v.10 no.3
    • /
    • pp.138-143
    • /
    • 2005
  • Laboratory batch experiments were conducted to evaluate the Fenton degradation rates of phenanthrene. Fenton reactions for the degradation of phenanthrene were carried out with aqueous and slurry phase, to investigate the effects of sorption of phenanthrene onto solid phase. Various types of surfactants and electrolyte solutions were used to evaluate the effects on the phenanthrene degradation rates by Fenton's reaction. A maximum 90% removal of phenanthrene was achieved in aqueous phase with 0.9% of $H_2O_2$ and 300 mg/L of $Fe^{2+}$ at pH 3. In aqueous phase reaction, inhibitory effects of synthetic surfactants on the removal of phenanthrene were observed, implying that surfactant molecules acted as strong scavenger of hydroxyl radicals. However, use of $carboxymethyl-{\beta}-cyclodextrin$ (CMCD), natural surfactant, showed a slight enhancement in the degradation of phenanthrene. It was considered that reactive radicals formed at ternary complex were located in close proximity to phenanthrene partitioned into CMCD cavities. It was also show that Fenton degradation of phenanthrene were greatly enhanced by addition of NaCl, indicating that potent radical ion ($OCI^-$) played an important role in the phenanthrene degradation, although chloride ion might be acted as scavenger of radicals at low concentrations. Phenanthrene in slurry phase was resistant to Fenton degradation. It might be due to the fact that free radicals were mostly reacting with dissolved species rather than with sorbed phenanthrene. Even though synthetic surfactants were added to increase the phenanthrene concentration in dissolved phase, low degradation efficiency was obtained because of the scavenging of radicals by surfactants molecules. However, use of CMCD in slurry phase, showed a slight enhancement in the phenanthrene degradation. As an alternative, use of Fenton reaction with CMCD could be considered to increase the degradation rates of phenanthrene desorbed from solid phase.