• Title/Summary/Keyword: $360^{\circ}$

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Synthesis of CdS Nanocrystals with Different Shapes via a Colloidal Method

  • Bai, Jie;Liu, Changsong;Niu, Jinzhong;Wang, Hongzhe;Xu, Shasha;Shen, Huaibin;Li, Lin Song
    • Bulletin of the Korean Chemical Society
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    • v.35 no.2
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    • pp.397-400
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    • 2014
  • Size- and shape-controlled monodisperse wurtzite structured CdS nanorods have been successfully synthesized using a facile solution-based colloidal method. Depending on the control of injection/growth temperatures and the variation of Cd-to-S molar ratios, the morphology of the CdS nanocrystals (NCs) can be adjusted into bullet-like, rod-like, and dot-like shapes. X-ray diffraction (XRD), transition electron microscopy (TEM), and absorption spectroscopy were used to characterize the structure, morphology, and optical properties of as-synthesized CdS NCs. It was found that uniform CdS nanorods could be successfully synthesized when the injection and growth temperatures were very high (> $360^{\circ}C$). The aspect ratios of different shaped (bullet-like or rod-like) CdS NCs could be controlled by simply adjusting the molar ratios between Cd and S.

Observation of the Domain Structures in Soft Magnetic (Fe97A13)85N15/Al2O3 Multilayers

  • Stobiecki, T.;Zoladz, M.
    • Journal of Magnetics
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    • v.8 no.1
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    • pp.13-17
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    • 2003
  • The longitudinal magnetooptical Kerr effect was used to analyse magnetic domains in soft magnetic ${(Fe_{97}A1_3)}_{85}N_{15}$/$Al_{2}O_{3}$ multilayers in order to get microscopic understanding of interlayer exchange coupling. The measuring system consists of a Kerr microscope, a CCIR camera (with an 8-bit framegrabber), 16 bit digital camera and computer system for real-time image processing and to control external magnetic field and cameras. The strength of ferromagnetic (EM) coupling as a function of the spacer thickness of $Al_2O_3$ was investigated. It was found that strong FM-coupling, strong uniaxial anisotropy and coherent rotation of the magnetization have been observed for the spacer thickness in the range of 0.2 nm $\leq$ t $\leq$ 1 m, however, weak FM-coupling, patch domains and $360^{\circ}$-walls occur for the spacer thickness of t = 2.5 nm. At a spacer thickness of t $\geq$ 5 nm transition takes place from weak FM-coupling to the decoupled state where complex interlayer interactions and different types of the domain walls were observed.

PDMS/Glass Serpentine Microchannel Chip for PCR with Bubble Suppression in Sample Injection (시료주입시 기포발생이 억제된 반응조 형태의 중합효소연쇄반응용 PDMS/유리 바이오칩)

  • Cho Chul-Ho;Cho Woong;Hwang Seung-Yong;Ahn Yoo-Min
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.30 no.10 s.253
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    • pp.1261-1268
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    • 2006
  • This paper reports low-cost microreactor $(10{\mu}{\ell})$ biochip for the DNA PCR (polymerase chain reaction). The microbiochip $(20mm{\times}28mm)$ is a hybrid type which is composed of PDMS (polydimethylsiloxane) layer with serpentine micochannel $(360{\mu}m{\times}100{\mu}m)$ chamber and glass substrate integrated with microheater and thermal microsensor. Undesirable bubble is usually created during sample loading to PMDS-based microchip because of hydrophobic chip surface. Created bubbles interrupt stable biochemical reaction. We designed improved microreactor chamber using microfluidic simulation. The designed reactor has a coner-rounded serpentine channel architecture, which enables stable injection into hydrophobic surface using micropipette only. Reactor temperature needed to PCR reaction is controlled within ${\pm}0.5^{\circ}C$ by PID controller of LabVIEW software. It is experimentally confirmed that SRY gene PCR by the fabricated microreactor chip is performed for less than 54 min.

Omni Camera Vision-Based Localization for Mobile Robots Navigation Using Omni-Directional Images (옴니 카메라의 전방향 영상을 이용한 이동 로봇의 위치 인식 시스템)

  • Kim, Jong-Rok;Lim, Mee-Seub;Lim, Joon-Hong
    • Journal of Institute of Control, Robotics and Systems
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    • v.17 no.3
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    • pp.206-210
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    • 2011
  • Vision-based robot localization is challenging due to the vast amount of visual information available, requiring extensive storage and processing time. To deal with these challenges, we propose the use of features extracted from omni-directional panoramic images and present a method for localization of a mobile robot equipped with an omni-directional camera. The core of the proposed scheme may be summarized as follows : First, we utilize an omni-directional camera which can capture instantaneous $360^{\circ}$ panoramic images around a robot. Second, Nodes around the robot are extracted by the correlation coefficients of Circular Horizontal Line between the landmark and the current captured image. Third, the robot position is determined from the locations by the proposed correlation-based landmark image matching. To accelerate computations, we have assigned the node candidates using color information and the correlation values are calculated based on Fast Fourier Transforms. Experiments show that the proposed method is effective in global localization of mobile robots and robust to lighting variations.

The Effect of K Promoter on Ni-Co (Bimetallic) Catalyst for Dry Methane Reforming

  • Dharmasaroja, Nichthima;Phongaksorn, Monrudee;Tungkamani, Sabaithip;Ratana, Tanakorn;Sornchammi, Thana
    • International Journal of Advanced Culture Technology
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    • v.3 no.2
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    • pp.110-117
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    • 2015
  • 10 wt% (Ni-Co) catalysts with different Ni and Co content : 10%Ni, 9%Ni1%Co, 7%Ni3%Co, 5%Ni5%Co, 3%Ni7%Co, and 10%Co; were prepared using sol-gel method followed by incipient wetness impregnation method. To investigate the catalytic activity including the stability, dry methane reforming were demonstrated over the pelletized catalysts at $620^{\circ}C$ under atmospheric pressure in a $CH_4:CO_2:N_2$ feedstock for 360 min. The results showed that bimetallic catalysts with the Co content equal to or greater than 3% were more stable than monometallic catalysts (10%Ni and 10%Co). The temperature programmed hydrogenation interpreted that the additional of Co into Ni catalyst improved the carbon resistance from methane cracking. Promoted this type of bimetallic catalyst using 1wt% K (trimetallic catalyst) prevented the carbon formation on the catalyst. The temperature programmed desorption of $CO_2$ indicated that this trimetallic catalyst has a greater number of strong basic sites. Moreover, the appearance of K lowered the number of weak basic sites and decreased the conversion of methane by 12 %.

Residual strength capacity of fire-exposed circular concrete-filled steel tube stub columns

  • Alhatmey, Ihssan A.;Ekmekyapar, Talha;Alrebeh, Salih K.
    • Advances in concrete construction
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    • v.6 no.5
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    • pp.485-507
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    • 2018
  • Concrete-Filled Steel Tube (CFST) columns are an increasingly popular means to support great compressive loads in buildings. The residual strength capacity of CFST stub columns may be utilized to assess the potential damage caused by fire and calculate the structural fire protection for least post-fire repair. Ten specimens under room conditions and 10 specimens under fire exposure to the Eurocode smouldering slow-growth fire were tested to examine the effects of diameter to thickness D/t ratio and reinforcing bars on residual strength capacity, ductility and stiffness of CFST stub columns. On the other hand, in sixteen among the twenty specimens, three or six reinforcing bars were welded inside the steel tube. The longitudinal strains in the steel tube and load-displacement relationships were recorded throughout the subsequent compressive tests. Corresponding values of residual strength capacity calculated using AISC 360-10 and EC4 standards are presented for comparison purposes with the experimental results of this study. The test results showed that after exposure to $750^{\circ}C$, the residual strength capacity increased for all specimens, while the ductility and stiffness were slightly decreased. The comparison results showed that the predicted residual strength using EC4 were close to those obtained experimentally in this research.

Global Localization of Mobile Robots Using Omni-directional Images (전방위 영상을 이용한 이동 로봇의 전역 위치 인식)

  • Han, Woo-Sup;Min, Seung-Ki;Roh, Kyung-Shik;Yoon, Suk-June
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.31 no.4
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    • pp.517-524
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    • 2007
  • This paper presents a global localization method using circular correlation of an omni-directional image. The localization of a mobile robot, especially in indoor conditions, is a key component in the development of useful service robots. Though stereo vision is widely used for localization, its performance is limited due to computational complexity and its narrow view angle. To compensate for these shortcomings, we utilize a single omni-directional camera which can capture instantaneous $360^{\circ}$ panoramic images around a robot. Nodes around a robot are extracted by the correlation coefficients of CHL (Circular Horizontal Line) between the landmark and the current captured image. After finding possible near nodes, the robot moves to the nearest node based on the correlation values and the positions of these nodes. To accelerate computation, correlation values are calculated based on Fast Fourier Transforms. Experimental results and performance in a real home environment have shown the feasibility of the method.

Design and Analysis of Illumination Optics for Image Uniformity in Omnidirectional Vision Inspection System for Screw Threads (나사산 전면검사 비전시스템의 영상 균일도 향상을 위한 조명 광학계 설계 및 해석)

  • Lee, Chang Hun;Lim, Yeong Eun;Park, Keun;Ra, Seung Woo
    • Journal of the Korean Society for Precision Engineering
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    • v.31 no.3
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    • pp.261-268
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    • 2014
  • Precision screws have a wide range of industrial applications such as electrical and automotive products. To produce screw threads with high precision, not only high precision manufacturing technology but also reliable measurement technology is required. Machine vision systems have been used in the automatic inspection of screw threads based on backlight illumination, which cannot detect defects on the thread surface. Recently, an omnidirectional inspection system for screw threads was developed to obtain $360^{\circ}$ images of screws, based on front light illumination. In this study, the illumination design for the omnidirectional inspection system was modified by adding a light shield to improve the image uniformity. Optical simulation for various shield designs was performed to analyze image uniformity of the obtained images. The simulation results were analyzed statistically using response surface method, from which optical performance of the omnidirectional inspection system could be optimized in terms of image quality and uniformity.

Effect of Cerium loading on Stability of Ni-bimetallic/ZrO2 Mixed Oxide Catalysts for CO Methanation to Produce Natural Gas

  • Bhavani, Annabathini Geetha;Youn, Hyunki
    • Korean Chemical Engineering Research
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    • v.56 no.2
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    • pp.269-274
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    • 2018
  • All the $Ni-Co-Ce-ZrO_2$ mixed oxides are prepared by co-precipitations methods. Methanation of CO and $H_2$ reaction is screened tested over different fractions of cerium (2, 4, 7 and 12 wt.%) over $Ni-Co/ZrO_2$ bimetallic catalysts are investigated. The mixed oxides are characterized by XRD, CO-Chemisorption, TGA and screened methanation of CO and $H_2$ at $360^{\circ}C$ for 3000 min on stream at typical ratio $CO:H_2=1:1$. In $Ni-Co/CeZrO_2$ series 2 wt.% Ce loading catalyst shows most promising catalyst for $CH_4$ selectivity than $CO_2$, which directs more stability with less coke formation. The high activity is attributed to the better bimetallic synergy and the well-developed crystalline phases of NiO, $ZrO_2$ and $Ce-ZrO_2$. Other bimetallic mixed oxides NCoZ, $NCoC^{4-12}Z$ has faster deactivation with low methanation activity. Finally, 2 wt.% Ce loading catalyst was found to be optimal coke resistant catalyst.

Piezoelectric and Dielectric Characteristics of PAN-PZT Ceramics with BaCO3Addition (BaCO3첨가량에 따른 PAN-PZI계 세라믹스의 압전 및 유전특성)

  • 박타리;이동균;최지원;강종윤;김현재;윤석진;고태국
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.15 no.4
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    • pp.356-360
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    • 2002
  • The piezoelectric properties of $0.05Pb(Al_{0.5}Nb_{0.5})O_3-0.95Pb(Zr_{0.52}Ti_{0.48})O_3+0.7wt%Nb_2O_5+o.5wt%MnO_2$ ceramics with the additive of BaCO$_3$were investigated. As the addition of BaCO$_3$increased from 0 to 0.4 wt%, the dielectric constant ($\epsilon^T _{33}$), piezoelectric constant ($d_33$), electromechanical coupling factor ($k_p$), and mechanical quality factor ($Q_m$) increased, while the dielectric loss ($tan\delta$) decreased. The highest piezoelectric and dielectric properties were observed at $1200^{\circ}C$ of the sintered temperature with 0.4 wt% of $BaCO_3$, and the properties of $d_33$, $k_p$, and $Q_m$ were 339 pC/N, 60% and 1754, respectively.