• Corrosion Science and Technology
• /
• 제22권5호
• /
• pp.330-340
• /
• 2023

The objective of this study was to analyze effects of aging time on property degradation of super austenitic stainless steel of PRE 52.8 and super duplex stainless steel of PRE 48.7. To analyze corrosion properties based on aging time, a critical pitting temperature test was performed in a solution of 6% FeCl₃ + 1% HCl and an anodic polarization test was performed in deaerated 0.5N HCl + 1N NaCl solution at a temperature of 50 ℃. Surface hardness was measured to analyze mechanical properties. It was found that corrosion properties and mechanical properties deteriorated rapidly as aging time increased. Critical pitting temperature had the most effect on critical aging time at which property changes occurred rapidly, followed by pitting potential and hardness. This trend was found to be closely related to the fraction of sigma phase. Rate of sigma phase formation was found to be significantly faster in duplex stainless steel than in austenitic stainless steel.

• 한국안광학회지
• /
• 제10권1호
• /
• pp.9-15
• /
• 2005

CR 렌즈에 가한 미세응력 크기의 시각화를 위한 편광기는 광원-편광판-시료-편광판-CCD-컴퓨터-chrome 변환 로 구성하였고, 각 편광판의 단계별 광 파의 $E_1$, $E_2$의 성분을 분석하여, 주 응력차 ${\sigma}_1-{\sigma}_2$와 무늬 차수(n)를 유도하였다. 시료의 광 축이 주 응력 방향과 일치하는 것으로부터 2 차원 모델을 결정할 수 있다. 광파에 작용하는 이중 굴절성과 위상 지연은 주 응력차(${\sigma}_1-{\sigma}_2$)에 비례하며, 최종 광 파의 세기는 $sin^2({\Delta}/2)$에 비례하고, ${\Delta}/2=n{\pi}$ (n=0, 1, 2, ${\ldots}$)일 때 흡광이 일어난다. 미세 응력에 의한 광탄성은 chrome 변환을 이용하여 분석 가능하였으며, 이미지는 뚜렷하였다.

• Journal of Microbiology
• /
• 제45권6호
• /
• pp.534-540
• /
• 2007

The Streptomyces coelicolor A3(2) genome contains six operons (rrnA to F) for ribosomal RNA synthesis. Transcription from rrnD occurs from four promoters (p1 to p4). We found that transcripts from the p1 and p3 promoters were most abundant in vivo in the early exponential phase. However, at later phases of exponential and stationary growth, transcripts from the p1 promoter decreased drastically, with the p3 and p4 transcripts constituting the major forms. Partially purified RNA polymerase supported transcription from the p3 and p4 promoters, whereas pure reconstituted RNA polymerase with core enzyme (E) and the major vegetative sigma factor ${\sigma}^{HrdB}$ ($E{\cdot}{\sigma}^{HrdB}$) did not. In order to assess any potential requirement for additional factor(s) that allow transcription from the p3 and p4 promoters, we fractionated a partially purified RNA polymerase preparation by denaturing gel filtration chromatography. We found that transcription from the p3 and p4 promoters required factor(s) of about 30-35 kDa in addition to RNAP holoenzyme ($E{\cdot}{\sigma}^{HrdB}$). Therefore, transcription from the p3 and p4 promoters, which contain a consensus -10 region but no -35 for ${\sigma}^{HrdB}$ recognition, are likely to be regulated by transcription factor(s) that modulate RNA polymerase holoenzyme activity in S. coelicolor.

• 열처리공학회지
• /
• 제19권2호
• /
• pp.103-108
• /
• 2006

Microstructural evolution of Pt-aluminide coated Ni-based superalloy has been investigated with ductilization heat treatment. The Pt coat was prepared on the superalloy and then aluminide coating was conducted using a pack cementation process. Samples were heat-treated at $1050^{\circ}C$ for 2 hrs and the microstructure and element analysis were preformed. A various precipitated compounds were observed within the coating layer and the diffusion region in the Pt-aluminide coating and heat treatment, indicating that the bi-phase compounds of $PtAl_2$ and NiAl were performed during the Pt-aluminide coating, whereas $M_{23}C_6$, MC, $Ni_3Al$ and ${\sigma}$ phases were precipitated in the inter-diffusion region. The bi-phase compounds of $PtAl_2$ and NiAl were transformed into the single phase compound of $PtAl_2$ with the heat treatment, increasing the amount of carbide and ${\sigma}$ phase.

• 한국전자파학회논문지
• /
• 제18권7호
• /
• pp.757-765
• /
• 2007

OFDM(Orthogonal Frequency Division Multiplexing) 시스템은 이동성이 있는 고속 데이터 전송에 적합한 전송 방법으로 널리 알려져 있지만, 위상 잡음과 직교 불균형(IQ imbalance)에 매우 민감한 특성을 보이는 단점이 있다. 그러므로, 본 논문에서는 위상 잡음 특성에 따른 위상 잡음 분산을 계산한 다음, 직교 불균형이 있는 OFDM 시스템의 통신 성능을 분석하였다. 시뮬레이션 결과, 위상 잡음의 분산과 직교 불균형의 크기 변화에 따라 통신 성능이 변화하는 것을 분석하였다. 분석 결과, 진폭 불균형이 ${\varepsilon}$=0.2; 0.3; 0.4이고, 위상 불균형이 ${\phi}=10^0$이고, 위상 잡음의 분산 ${\sigma}^2=0.012$일 때, BER은 $10^{-5}$에서 각각 2.88 dB, 3.61 dB, 4.69 dB의 SNR penalty가 존재한다.

• 대한용접접합학회:학술대회논문집
• /
• 대한용접접합학회 2004년도 추계학술발표대회 개요집
• /
• pp.174-176
• /
• 2004

The duplex stainless clad vessel with 38m & over thickness shall be performed to PWHT based on the ASME code. In this case, it is well-known that precipitators such as carbides and sigma($\sigma$) phase are formed at gram boundary between ferrite and austenite phase. Therefore, a weld test for simulating this situation has been planned and performed by 3309LMo71-1 for barrier layer and E2209Tl-1 for 2nd & over layer and then carried out to investigate the overlaid weld metal. Based on the test results, it could be concluded that PWHT should be carried out after the completion of 1st(barrier) layer and then 2 & over layer should be applied.

• 대한전기학회:학술대회논문집
• /
• 대한전기학회 2005년도 학술대회 논문집 정보 및 제어부문
• /
• pp.436-438
• /
• 2005

본 논문에서는 전력선 위상 측정을 위해 A/D 변환기 및 위상계측 연산장치를 집적한 하이브리드 센서칩의 구현 기법을 제시하였다. 개발한 위상계측 연산장치는 recursive sliding-DFT에 기반하였으며 곱셈기의 시분할 공유 구조를 사용하여 칩의 구현 면적을 최소화 하였다. 60Hz의 전력선 신호를 중심주파수로 하는 AD 변환장치는 sigma-delta ADC를 기반으로 하여 8-bit 정밀도를 제공하며 아날로그부의 구현을 최소화하도륵 설계하였다. 설계한 하이브리드 센서칩은 컴퓨터 시뮬레이션 및 FPGA 구현을 통해 동작을 검증하였으며, 검증 완료후 $0.35{\mu}m$ CMOS 공정기술로 구현하였다. 전력선 위상을 측정하기 위해 구현된 4채널 하이브리드 센서 칩의 설계면적은 $5{\times}5m^2$ 의 약 20%정도를 차지하였다.

• 대한용접접합학회:학술대회논문집
• /
• 대한용접접합학회 2004년도 춘계 학술발표대회 개요집
• /
• pp.156-158
• /
• 2004

The microstructural evolution in a 304 stainless steel weld during FSW was examined. The SZ and TMAZ showed typical dynamically recrystallized and recovered microstructures, respectively, The microstructural observation revealed that sigma phase was formed at the advancing side of the stir zone. A possibility was suggested that the rapid formation of the sigma phase is related to the transformation of austenite to delta-ferrite in the stir zone, from introduction of high strain and dynamic recrystallization during FSW.

• 한국항해항만학회:학술대회논문집
• /
• 한국항해항만학회 2006년도 International Symposium on GPS/GNSS Vol.1
• /
• pp.179-184
• /
• 2006

Rapid and high-precision positioning with a Global Navigation Satellite System (GNSS) is feasible only when very precise carrier-phase observations can be used. There are two kinds of mathematical models for ambiguity resolution. The first one is based on both pseudorange and carrier phase measurements, and the observation equations are of full rank. The second one is only based on carrier phase measurement, which is a rank-defect model. Though the former is more commonly used, the latter has its own advantage, that is, ambiguity resolution will be freed from the effects of pseudorange multipath. Galileo will be operational. One of the important differences between Galileo and current GPS is that Galileo will provide signals in four frequency bands. With more carrier-phase data available, frequency combinations with long equivalent wavelength can be formed, so Galileo will provide more opportunities for fast and reliable ambiguity resolution than current GPS. This paper tries to investigate phase only fast ambiguity resolution performance with four Galileo frequencies for short baseline. Cascading Ambiguity Resolution (CAR) method with selected optimal frequency combinations and LAMBDA method are used and compared. To validate the resolution, two tests are used and compared. The first one is a ratio test. The second one is lower bound success-rate test. The simulation test results show that, with LAMBDA method, whether with ratio test or lower bound success rate validation criteria, ambiguity can be fixed in several seconds, 8 seconds at most even when 1 sigma of carrier phase noise is 12 mm. While with CAR method, at least about half minute is required even when 1 sigma of carrier phase noise is 3 mm. It shows that LAMBDA method performs obviously better than CAR method.

• 한국결정성장학회지
• /
• 제22권4호
• /
• pp.178-182
• /
• 2012

결정립 성장은 여러 가지 재료의 성질에 미치는 큰 영향으로 재료공학에서 매우 중요하다. 그래서 본 연구에서는 PC에서 대규모 상장 모델을 사용하여 이방성 결정립 계면에너지의 2차원 결정립 성장에 미치는 효과를 조사하였다. 컴퓨터 모사에서는 $2000{\times}2000$의 그리드 시스템과 약 7300개의 초기 결정립 개수가 사용되었다. 결정립계 에너지의 이방성의 비, ${\sigma}_{max}/{\sigma}_{min}$는 1부터 3까지 변경되었다. 이방성이 증가함에 따라 결정립 성장 지수, n은 2.05에서 2.37로 증가하였다. 결정립 크기의 분포는 등방성인 경우에는 중앙에 평탄한 영역을 보였으나 이방성의 경우에는 중앙의 평탄한 영역이 사라지고 매우 느리게 사라지는 작은 결정립에 기인하여 작은 결정립 크기의 분포가 약간 증가하였다. 마지막으로 모사된 결정립 미세구조가 이방성에 따라 비교, 분석되었다.