• Title/Summary/Keyword: ${\gamma}$-Spectrometry

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Mineral Movement in Relation to Pollination in Two Perennial Plants (두 다년생 식물에 있어서 수분에 따른 무기물의 이도 양상)

  • 강혜순
    • Journal of Plant Biology
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    • v.34 no.2
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    • pp.151-158
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    • 1991
  • A new technique involving gamma-spectrometry was used to determine the effects of pollination on mineral uptake in petals, ovaries and leaves of tulips and daffodils. A gamma-emitting radionu'::lide solution containing selenium-75, cesium-137, manganese-54, and zinc-65 was applied to the roots of tulips and daffodils growing in water. Mineral uptake was monitored in plant parts over a 24 day period. Pollinated tulip flowers showed a rapid withdrawal of minerals from the petals and an increase in ovary mineral content, while such a source-sink relationship was not established in daffodils. In both species, the concentration of most minerals in petals and ovaries declined prior to abortion of the plant part. The roots and bulbs of the plants contained the vast majority of the labeled minerals. This study demonstrated a possibility that certain plant parts could be isolated and monitored for mineral uptake over time without destruction.uction.

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A study on the HTS-NAA/γ-spectrometry for the analysis of alpha-particle emitting impurities in silica (고순도 실리카중 알파방출 불순물 분석을 위한 HTS-NAA/γ-spectrometry 연구)

  • Lee, Kil Yong;Yoon, Yoon Yeol;Cho, Soo Young;Yang, Myung Kwon;Shim, Sang Kwon;Kim, Yongje;Chung, Yong Sam
    • Analytical Science and Technology
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    • v.18 no.1
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    • pp.5-12
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    • 2005
  • It has been established that soft error of high precision electronic circuits can be induced by alpha particles emitted from the naturally occurring radioactive impurities such as U, and Th. As the electronic circuits have recently become lower dimension and higher density, these alpha-particle emitting radioactive impurities have to be strictly controlled. The aim of this study is to develop of NAA (Neutron Activation Analysis) and gamma-spectrometry to improve the analytical sensitivity and precision of U and Th. A new NAA method has been established using the HTS (Hydrulic transfer system) irradiation facility which has been used to produce radioisotopes for industries and medicines instead of the PTS (pneumatic transfer system) irradiation facility which has been used in general NAA. When the ultratrace impurities have to be analyzed by NAA, background gamma-ray spectra induced from $^{222}Rn$ and its progenies in air is serious problem. This unstable background has been eliminated or stabilized by the use of a nitrogen purging system. Ultra trace amounts of U (0.1 ng/g) and Th (0.01 ng/g) in high purity silica used for EMC could be analyzed by the use of HTS-NAA and low background gamma-spectrometry.

Broad Beam Gamma-Ray Spectrometric Studies with Environmental Materials

  • El-Kateb, Abdul-Hamid Hussein
    • Journal of Radiation Protection and Research
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    • v.43 no.2
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    • pp.75-84
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    • 2018
  • Background: Gamma-ray spectrometry helps in radiation shielding problems and different applications of radioisotopes. Experimental arrangements including broad beam geometries are widely used. The aim is to investigate and evaluate the ${\gamma}-ray$ spectra via attenuation by environmental materials. Materials and Methods: The photo peak to nominated parts in the ${\gamma}-ray$ spectra and the attenuation coefficients ${\mu}_b/{\rho}$ from broad beam geometries are measured for the materials water, soil, sand and cement at the energies 0.662, 1.25, and 1.332 MeV with a $3{^{\prime}^{\prime}}{\times}3{^{\prime}^{\prime}}$ NaI(Tl) detector. Results and Discussion: The ${\gamma}-ray$ spectra vary according to changes in the effective atomic number $Z_{eff}$ of the attenuator, the photon energy and the solid angle. The peak to total ratios are the most sensitive parts to variations in the experimental conditions and overturn in the region 0.663 MeV to 1.332 MeV. This is indicated as inversion trend. The results are discussed in view of $Z_{eff}$ and the experimental conditions. The intensity build-up is larger at the lower energy and larger scattering angles in agreement with Klein-Nishina formula and other results. The build-up factor B is$${\sim_=}$$1 at high ${\gamma}-energies$ and small scattering angles. Conclusion: The sensitivity to material characteristics decrease gradually from peak: to total, to Compton valley, to Compton plateau ratios. Rigorous collimation is necessary at small energies. Cement, of the largest $Z_{eff}$, is characterized by the maximum broad beam mass attenuation coefficients ${\mu}_b/{\rho}$. The obtained results provide information to decide for the suitable experimental set-up based on aim of the work.

Assessment of Gamma-radiation dose Rate in the Ogcheon Lower Phyllite Area, Goesan County, Korea, Using Gamma-ray Spectrometry (감마선분광분석기를 이용한 괴산 옥천하부천매암대 일대의 감마선량 평가)

  • Yun, Uk;Cho, Byong-Wook
    • The Journal of Engineering Geology
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    • v.29 no.4
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    • pp.461-468
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    • 2019
  • Gamma-radiation dose rates were measured at 77 points around the Ogcheon lower phyllite zone (og2) in Goesan County, Korea, using gamma-ray spectrometry. Sample K contents were in the range 1.8-8.8% (average 4.6%), highest in Kgr. The eU contents were 0.2-217.9 ppm (average 16.7 ppm), highest in og2 (median 29.6 ppm). The eTh contents were 11.9-76.5 ppm (average 29.5 ppm) and the average eTh content of Kgr was 45.4 ppm, higher than those of Ogcheon meta-sedimentary rocks (og1, og2, and og3) (26.6-30.6 ppm). Except for some high-uranium sites in og2, 40K is the main radioactive material contributing to the gamma-radiation dose in the study area. Our results indicate that the outdoor effective dose rate of the area is 0.08-1.71 mSv y-1 (average 0.28 mSv y-1), with most areas apart from three points in og2 displaying dose rates <1 mSv y-1, which is the normal natural radiation background level.

Nuclide Identification of Gamma Ray Energy Peaks from an Air Sample for the Emergency Radiation Monitoring (비상시 환경방사능 모니터링을 위한 공기부유진 시료의 감마선에너지 스펙트럼에 대한 핵종판별)

  • Byun, Jong-In;Yoon, Seok-Won;Choi, Hee-Yeoul;Yim, Seong-A;Lee, Dong-Myung;Yun, Ju-Yong
    • Journal of Radiation Protection and Research
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    • v.34 no.4
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    • pp.170-175
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    • 2009
  • For the emergency radiation monitoring using gamma spectrometry, we should sufficiently survey the background spectra as environmental samples with systematic nuclide identification method. In this study, we obtained the gamma ray energy spectrum using a HPGe gamma spectrometry system from an air sample. And we identified nuclide of the gamma ray energy peaks in the spectrum using two methods -1) Half life calculation and 2) survey for cascade coincidence summing peaks using nuclear data. As the results, we produced the nuclide identification results for the air sample.

ANALYSIS OF RADIOACTIVE IMPURITIES IN ALUMINA AND SILICA USED FOR ELECTRONIC MATERIALS

  • Lee Kil-Yong;Yoon Yoon-Yeol;Cho Soo-Young;Kim Yong-Je;Chung Yong-Sam
    • Nuclear Engineering and Technology
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    • v.38 no.5
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    • pp.423-426
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    • 2006
  • A developed neutron activation analysis(NAA) and gamma-spectrometry were applied to improve the analytical sensitivity and precision of impurities in electronic-circuit raw materials. It is well known that soft errors in high precision electronic circuits can be induced by alpha particles emitted from naturally occurring radioactive impurities such as U and Th. As electronic circuits have recently become smaller in dimension and higher in density, these alpha-particle emitting radioactive impurities must be strictly controlled. Therefore, new NAA methods have been established using a HTS(Hydraulic Transfer System) irradiation facility and a background reduction method. For eliminating or stabilizing fluctuated background caused by Rn-222 and its progeny nuclides in air, a nitrogen purging system is used. Using the developed NAA and gamma-spectrometry, ultra trace amounts of U(0.1ng/g) and Th(0.01ng/g) in an alumina ball and high purity silica used for an epoxy molding compound (EMC) could be determined.

Preparation of Carrier-free Fe-59 by Korean TRIGA Mark Ⅱ Reactor (無擔體 鐵-59製造에 關한 硏究)

  • Park, Keung-Shik
    • Journal of the Korean Chemical Society
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    • v.9 no.2
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    • pp.96-100
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    • 1965
  • Possibility on carrier-free Fe-59 preparation by Korean TRIGA Mark Ⅱ reactor was investigated, namely average cross section on $Co^{59}$(n,p) $Fe^{59}$ reaction, separation by anion exchange resin and radiochemical purity. Radiochemical purity of Fe-59 separated was checked by the method of ${\gamma}$-ray spectrometry with 256-multichannel pulse height analyzer and of half life determination. This method permits Fe-59 preparation with radiochemical purity of > 99.9%.

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Long term activity measurement of the primary circuit water on the LVR-15 research reactor

  • Ladislav Viererbl;Vit Klupak;Hana Assmann Vratislavska
    • Nuclear Engineering and Technology
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    • v.56 no.4
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    • pp.1250-1253
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    • 2024
  • Activity measurement of the primary circuit water of fission reactors is one method that can provide early detection of a damaged fuel assembly in the reactor core. This is an important aspect in the safe operation of the reactor and for radiation protection of staff. Radionuclides in the primary circuit water are produced by the activation of stable nuclides and the fission of fissile nuclides, mainly the isotope 235U. In the LVR-15 research reactor, measurement of the activity of the primary circuit water has been regularly undertaken since 1996. A water sample is taken from the primary circuit every week and the activities are measured four days later using gamma spectrometry. The results of these long-term measurements from 1996 to 2022 are presented. The activity time dependences of the individual radionuclides are discussed in relation to fuel assembly damage and for events connected to contamination of the water by objects inserted into the primary circuit during experiments carried out near the reactor core.