• Title/Summary/Keyword: $\Delta$ nd.

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The Influence on the Corrosion Fatigue Crack Propagation in Changing of the Second Phase Hardness of Dual Phase Steel (複合組織鋼의 第2相 硬度變化가 腐蝕疲勞 크랙傳播에 미치는 影響)

  • 오세욱;김웅집
    • Journal of Welding and Joining
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    • v.11 no.2
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    • pp.42-52
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    • 1993
  • The corrosion fatigue fracture behaviour of dual phase steel was investigated in 3% NaCl solution at 302MPa and 137MPa. Fatigue test was conducted by cantilever type of self-made rotary bending fatigue testing machine. The fatigue strength increased with increasing the hardness of 2nd phase. Corrosion pit originated at the boundary of the 2nd phase. The size and number of corrosion pits were influenced by the 2nd phase hardness, and pits remained constant in size just after they were transited into cracks. The life of crack initiation was effected by stress level. The shape of relation of .DELTA. K and da/dN has smaller scattering in it in 3% NaCl solution than that in air. The higher the 2nd phase hardness is, the greater the corrosion fatigue life becomes. Corrosion fatigue fracture behaviour was primarily effected by mechanical factor in case of high stress(302MPa), but by electro-chemical reaction in a lower stress(137MPa). As stress level got lower and hardness of the 2nd phase got higher, the roughness of fracture surface increased.

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Exchange Coupling in Massively Produced Nd2Fe14B+Fe3B Nanocomposite Powders

  • Yang, Choong Jin;Park, Eon Byung;Han, Jong Soo;Kim, Eung Chan
    • Journal of Magnetics
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    • v.9 no.2
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    • pp.27-33
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    • 2004
  • Magnetic properties of $Nd_4Fe_{77.5}B_{18.5}$ compound in term of exchange coupling between $Nd_2Fe_{14}B$ and $Fe_3B$ magnetic nano crystals in melt spun powders were characterized by varying the quenching speed in mass production line. The exchange coupled phenomenon was characterized as functions of nano crystal size and volume fraction of each magnetic phase which was possible by employing Henkel plot (${\delta}M$) and refined Mossbauer spectroscopy. The optimized magnetic properties obtained from the present volume production line were: $B_r= 11.73 kG,{_i}H_c/ = 3.082 kOe$, and $(BH)_{max} = 12.28 MGOe.$ The volume fraction of each magnetic phase for those conditions giving the grain size of 10 nm were ${\alpha}-Fe; 4.2%, Fe_3B; 60.1 %$, and $Nd_2Fe_{14}B; 35.7%$. The superior magnetic properties in the $Nd_2Fe_{14}Fe_3B$ based nanocomposites were confirmed to be dependant on the volume fraction of $Fe_3B$.

Magnetic Microstructures and Corrosion Behaviors of Nd-Fe-B-Ti-C Alloy by Ga Doping

  • Wu, Qiong;Zhang, Pengyue;Ge, Hongliang;Yan, Aru;Li, Dongyun
    • Journal of Magnetics
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    • v.18 no.3
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    • pp.240-244
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    • 2013
  • The influences of Gallium doping on the magnetic microstructures and corrosion behaviors of Nd-Fe-B-Ti-C alloys are investigated. The cooling rate for obtaining fully amorphous structure is raised, and the glassforming ability is improved by the Ga addition. The High Resolution Transmission Electron Microscopy image shows that the ${\alpha}$-Fe and $Fe_3B$ soft magnetic phases become granular surrounded by the $Nd_2Fe_{14}B$ hard magnetic phase. The rms and $({\Delta}{\varphi})_{rms}$ value of Nd-Fe-B-Ti-C nanocomposite alloy thick ribbons in the typical topographic and magnetic force images detected by Magnetic Force Microscopy(MFM) decreases with 0.5 at% Ga addition. The corrosion resistances of $Nd_9Fe_{73}B_{12.6}C_{1.4}Ti_{4-x}Ga_x$ (x = 0, 0.5, 1) alloys are enhanced by the Ga addition. It can be attributed to the formation of more amorphous phases in the Ga doped samples.

Second Harmonic Conversion of Nd:YAG Laser using $KH_2PO_4(KDP)$ Crystal ($KH_2PO_4(KDP)$ 결정을 이용한 Nd:YAG 레이저의 제3고조파 변환)

  • Chang, Yong-Moo;Kim, Byung-Tai;Kang, Hyung-Boo
    • Proceedings of the KIEE Conference
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    • 1989.07a
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    • pp.633-636
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    • 1989
  • The simulation results of the third harmonic conversion with 1.064 um Nd :YAG laser using polarization mismatch method are reported. The third harmonic conversion efficiency was over 65% for the Gaussian incident pulse of $300{\sim}400MW/cm^2$ peak intensity, and over 80% for $3{\sim}4GW/cm^2$ peak intensity pulse. The dependence of the third harmonic conversion efficiency' on the variation of incident polarization angle ${\theta}_p$ and angular discrepancy ${\Delta}{\theta}$ of phase matched angle ${\theta}_m$ is discussed.

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Retardation of Fatigue Crack Propagation by Single Overloading (단일과대하중에 의한 피로균열전파의 지연거동)

  • 김상철;함경춘;강동명
    • Journal of the Korean Society of Safety
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    • v.7 no.1
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    • pp.20-29
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    • 1992
  • Effects of strain hardening exponents on the retardation behavior of fatigue crack propagation are experimentally investigated. The retardation of fatigue crack propagation seems to be induced by the crack closure at crack tip. The phenomenon of crack closure becomes remarkable with the increment of strain hardening exponent and magnitude of percent peak load. The ratio of crack growth increment(a$\_$d//w$\_$d/) is influenced by a single overloading (a$\_$d/) and estimated plastic zone size (W$\_$d/=2r$\_$y/) is increased according with the increasing of strain ha.dening exponents. The number of retarded crack growth cycles were (N$\_$d/) decreased as the baseline stress intensity factor .ange( K$\_$b/) was increased. Within the limitation of these experimental results obtained under the single overload, an empirical relation between crack retardation ratio (Nd/N*), strain hardening exponent (n) and percent peak load (%PL) has been proposed as; Nd/N*= exp [PL $.$ PL$.$A(n)+B(n) ] where, A(n)=${\alpha}$n+${\beta}$, B(n)=${\gamma}$n+$\delta$, PL=%PL/100 and ${\alpha}$=0.78, ${\beta}$=0.54, ${\gamma}$=0.58 and $\delta$=-0.01, It is interesting to note that all these constants are identical for materials such as aluminum(A3203), steel(S4SC), steel(SS41) and stainless steel(SUS316) used in this experimental study.

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Characteristics of Second Harmonic Generation in $LiB_3O_5 $ Crystals Grown by TSSG Method (TSSG 법으로 육성한 $LiB_3O_5 $ 단결정의 제2조화파 발생 특성)

  • 권택용;오학태;주정진;백현호;김정남;윤수인
    • Korean Journal of Optics and Photonics
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    • v.5 no.1
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    • pp.74-79
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    • 1994
  • The characteristics of the type I and type II SHG in LiB305 crystals grown by TSSG method have been investigated using 1064 nm beam from a Q-switched Nd:YAG laser. The measured phase matching angles and angular acceptance bandwidths were $\theta_m=90^{\circ}, \phi_m=11.6^{\circ}$, <$\delta\theta_{int}L_{1/2}=3.3^{\circ}-cm^{1/2}, \theta\phi_{int}L=0.27^{\circ}-cm^{1/2}$ for type I SHG and $\theta_m=20^{\circ}, \phi_m=90^{\circ}$, TEX>$\delta\theta_{int}L_=0.65^{\circ}-cm, \theta\phi_{int}L^{1/2}=3.5^{\circ}-cm^{1/2}$ for type II SHG, respectively. Thp. type I NCPM temperature of 1064 nm beam was found to be $149^{\circ}C$ with the temperature bandwidth $\DeltaTL$of $4.8^{\circ}C-cm$. An energy conversion efficiency of about 1.8% with 2.6 mm thick LBO crystal at an incident power of TEX>$171 MW/\textrm{cm}^2$ was demonstrated. The measured $d_{32} was 0.74\pm0.05 pm/V$..

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Detergent Screening for NMR-Based Structural Study of the Integral Membrane Protein, Emopamil Binding Protein (Human Sterol Δ8-Δ7 Isomerase)

  • Won, Hyung-Sik
    • Journal of the Korean Magnetic Resonance Society
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    • v.21 no.1
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    • pp.13-19
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    • 2017
  • Human sterol ${\Delta}8-{\Delta}7$ isomerase, commonly known as emopamil binding protein (EBP), is an essential protein in the cholesterol-synthetic pathway, and mutations of this protein are critically associated with human diseases such as Conradi-Hunermann-Happle or male EBP disorder with neurological defects syndrome. Due to such a clinical importance, EBP has been intensively investigated and some important features have been reported. EBP is a tetra-spanning membrane protein, of which $2^{nd}$, $3^{rd}$, and $4^{th}$ membrane-spanning ${\alpha}$ helices play an important role in its enzymatic function. However, detailed structural feature at atomic resolution has not yet been elucidated, due to characteristic difficulties in dealing with membrane protein. Here, we over-expressed EBP using Escherichia coli and performed detergent screening to find suitable membrane mimetics for structural studies of the protein by NMR. As results, DPC and LMPG could be evaluated as the most favorable detergents to acquire promising NMR spectra for structural study of EBP.

The mechanism of Bi$_{0.5}Pb_3Sr_2Ca_2CuO_{\delta}$ and (Ca,Sr)$_2$(BiPb)O$_4$ phase as a flux-pinning center in (Bi,Pb)$_2Sr_2Ca_2CuO_{10}$ superconductor ((Bi,Pb)$_2Sr_2Ca_2CuO_{10}$ 초전도체에l서 flux-pinning center로서 Bi$_{0.5}Pb_3Sr_2Ca_2CuO_{\delta}$ 및 (Ca,Sr)$_2$(BiPb)O$_4$ 상의도입 기구)

  • Chung, Jun-Ki;Kim, Cheol-Jin;Lee, Sang-Hee;Yoo, Jae-Moo;Kim, Hae-Doo;Koh, Jae-Woong
    • 한국초전도학회:학술대회논문집
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    • v.9
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    • pp.300-304
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    • 1999
  • To tap the feasibility of exploiting the 2$^{nd}$ phases as flux-pinning centers in the (Bi,Pb)$_2Sr_2Ca_2CuO_{10}$ superconductor, the size and the distribution of the precipitates have been controlled by changing reaction temperature and time, oxygen partial pressure Po$_2$ and annealing condition. Various annealing heat treatments were also conducted on the as-received 61 filament Bi-2223 tapes with Bi$_{1.8}Pb_{0.4}Sr_2Ca_{2.2}Cu_3O_8$ starting composition and annealed specimen were analyzed with XRD, SEM, EDS and TEM.. The grain size of (Ca,Sr)$_2$(BiPb)O$_4$ or Bi$_{0.5}Pb_3Sr_2Ca_2CuO_{\delta}$ was controllable by optimizing the heat treatment condition and critical current density (J$_c$) showed dependence on the size of the 2$^{nd}$ phases.

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Clinico-pathological studies on the experimental lead poisoning in goats I. Clinical observations(Clinical, hematological and urinary findings) (산양의 실험적 납중독에 관한 임상병리학적 관찰 I. 임상학적 관찰(증상, 혈액, 뇨))

  • Kwon, Oh-deog;Lee, Hyun-beom;Lee, Joo-mook;Chae, Joon-seok
    • Korean Journal of Veterinary Research
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    • v.32 no.1
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    • pp.127-134
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    • 1992
  • Present experiments were undertaken in order to clarify the clinico-pathological characteristics of lead poisoning in goats. Twenty goats were divided into three experimental groups(A, B and C) and a control(D). The three experimental groups received diets contaminated artificially with 10(A group), 200(B group) and 1,000(C group) ${\mu}g/$ of lead, for 70 days respectively. The control group received normal diets. Blood samples were collected 1 or 2 weeks interval and were examined for anemia(erythrocyte counts, hemoglobin concentrations and hematocrit values) and lead contents of erythrocyte and serum. Urine samples collected similarly with blood were examined for delta-aminolevulinic acid and lead content. Collected samples were analyzed for lead content by atomic absorption spectrophotometry. From these experiments following results were obtained : In group B and C, marked decreases in body weight and feed intake, and diarrhea were observed from the $30^{th}$ day of experimental periods. The B and C groups showed pronounced anemia(decrease in erythrocyte count, hemoglobin concentration and hematocrit value) from the $21^{st}$ or $42^{nd}$ day. In group B and C, the lead content of erythrocytes was increased significantly from the $28^{th}$ or $14^{th}$ day. The lead content of serum was increased significantly from the $42^{nd}$ or $14^{th}$ day in B and C groups. The lead content of urine was increased significantly from the first day in both B and C groups. The urinary delta-aminolevulinic acid content was increased significantly from $14^{th}$ day in both B and C groups.

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