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http://dx.doi.org/10.12989/anr.2021.10.3.295

Ionic liquid coated magnetic core/shell CoFe2O4@SiO2 nanoparticles for the separation/analysis of trace gold in water sample  

Zeng, Yanxia (Department of Chemical Engineering, Yangzhou University)
Zhu, Xiashi (Department of Chemical Engineering, Yangzhou University)
Xie, Jiliang (Institute of Marine Resource Development, Jiangsu Ocean University)
Chen, Li (Institute of Marine Resource Development, Jiangsu Ocean University)
Publication Information
Advances in nano research / v.10, no.3, 2021 , pp. 295-312 More about this Journal
Abstract
A new ionic liquid functionalized magnetic silica nanoparticle was synthesized and characterized and tested as an adsorbent. The adsorbent was used for magnetic solid phase extraction on ICP-MS method. Simultaneous determination of precious metal Au has been addressed. The method is simple and fast and has been applied to standard water and surface water analysis. A new method for separation/analysis of trace precious metal Au by Magnetron Solid Phase Extraction (MSPE) combined with ICP-MS. The element to be tested is rapidly adsorbed on CoFe2O4@SiO2@[BMIM]PF6 composite nano-adsorbent and eluted with thiourea. The method has a preconcentration factor of 9.5-fold. This method has been successfully applied to the determination of gold in actual water samples. Hydrophobic Ionic Liquids (ILs) 1-butyl-3-methylimidazole hexafluorophosphate ([BMIM]PF6) coated CoFe2O4@SiO2 nanoparticles with core-shell structure to prepare magnetic solid phase extraction agent (CoFe2O4@SiO2@ILs) and establish a new method of MSPE coupled with inductively coupled plasma mass spectrometry for separation/analysis of trace gold. The results showed that trace gold was adsorbed rapidly by CoFe2O4@SiO2@[BMIM]PF6 and eluanted by thiourea. Under the optimal conditions, preconcentration factor of the proposed method was 9.5-fold. The linear range, detection limit, correlation coefficient (R) and relative standard deviation (RSD) were found to be 0.01~1000.00 ng·mL-1, 0.001 ng·mL-1, 0.9990 and 3.4% (n = 11, c = 4.5 ng·mL-1). The CoFe2O4@SiO2 nanoparticles could be used repeatedly for 8 times. This proposed method has been successfully applied to the determination of trace gold in water samples.
Keywords
gold; magnetic silica nanoparticles; magnetic solid phase extraction; [BMIM] $PF_6$; loaded;
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192 Zhang, J. and Liu, B. (2019), "A review on the recent developments of sequence-based protein feature extraction methods", Curr. Bioinform., 14(3), 190-199. https://doi.org/10.2174/1574893614666181212102749.   DOI
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194 Jia, Q., Huang, S., Hu, M., Song, Y., Wang, M., Zhang, Z. and He, L. (2020b), "Polyoxometalate-derived MoS2 nanosheets embedded around iron-hydroxide nanorods as the platform for sensitively determining miRNA-21", Sens. Actuators B Chem., 323, 128647. https://doi.org/10.1016/j.snb.2020.128647.   DOI
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201 Xu, P., Lu, W., Zhang, J. and Zhang, L. (2020b), "Efficient hydrolysis of ammonia borane for hydrogen evolution catalyzed by plasmonic Ag@ Pd core-shell nanocubes", ACS Sustain. Chem. Eng., 8(33), 12366-12377. https://doi.org/10.1021/acssuschemeng.0c02276.   DOI
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215 Gao, N., Tang, L., Deng, J., Lu, K., Hou, H. and Chen, K. (2021), "Design, fabrication and sound absorption test of composite porous metamaterial with embedding i-plates into porous polyurethane sponge", Appl. Acoust., 175, 107845. https://doi.org/10.1016/j.apacoust.2020.107845.   DOI