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http://dx.doi.org/10.4191/kcers.2016.53.1.87

Formation of Ti3SiC2 Interphase of SiC Fiber by Electrophoretic Deposition Method  

Lee, Hyeon-Geun (Nuclear Materials Development Division, Korea Atomic Energy Research Institute)
Kim, Daejong (Nuclear Materials Development Division, Korea Atomic Energy Research Institute)
Jeong, Yeon Su (Nuclear Materials Development Division, Korea Atomic Energy Research Institute)
Park, Ji Yeon (Nuclear Materials Development Division, Korea Atomic Energy Research Institute)
Kim, Weon-Ju (Nuclear Materials Development Division, Korea Atomic Energy Research Institute)
Publication Information
Abstract
Due to its stability at high temperature and its layered structure, $Ti_3SiC_2$ MAX phase was considered to the interphase of $SiC_f/SiC$ composite. In this study, $Ti_3SiC_2$ MAX phase powder was deposited on SiC fiber via the electrophoretic deposition (EPD) method. The Zeta potential of the $Ti_3SiC_2$ suspension with and without polyethyleneimine as a dispersant was measured to determine the conditions of the EPD experiments. Using a suspension with 0.03 wt.% ball milled $Ti_3SiC_2$ powder and 0.3 wt.% PEI, $Ti_3SiC_2$ MAX phase was successfully coated on SiC fiber with an EPD voltage of 10 V for 2 h. Most of the coated $Ti_3SiC_2$ powders are composed of spherical particles. Part of the $Ti_3SiC_2$ powders that are platelet shaped are oriented parallel to the SiC fiber surface. From these results we expect that $Ti_3SiC_2$ can be applied to the interphase of $SiC_f/SiC$ composites.
Keywords
Interphase; MAX phase; SiC fiber; EPD; $Ti_3SiC_2$;
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