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http://dx.doi.org/10.4191/kcers.2013.50.6.396

Fabrication of Large-Size Alumina by Pressure-Vacuum Hybrid Slip Casting  

Cho, Kyeong-Sik (School of Advanced Materials and System Engineering, Kumoh National Institute of Technology)
Lee, Seung Yeul (Dicera Co. Ltd.)
Publication Information
Abstract
The size of various alumina ceramics used in the semiconductor and display industries must be increased to increase the size of wafers and panels. In this research, large alumina ceramics were fabricated by pressure-vacuum hybrid slip casting (PVHSC) employing a commercial powder, followed by sintering in a furnace. In the framework of the PVHSC method, the consolidation occurs not only by compression of the slip in the casting room but also by suction of the dispersion medium from the casting room. When sintered at $1650^{\circ}C$ for 4 h, the fabricated large-size alumina ($1,550{\times}300{\times}30mm^3$) exhibited a dense microstructure corresponding to more than 99.2% of the theoretical density and a high purity of 99.79%. The flexural and compressive strengths of the alumina plate were greater than 340 MPa and 2,600 MPa, respectively.
Keywords
Alumina; Slip casting; Microstructure; Strength;
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Times Cited By KSCI : 3  (Citation Analysis)
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1 H. K. Lee, K.-S. Cho, M. H. Jang, C. W. Jang, S. M. Kim, and M. Y. Kim, "Characteristics of Large Green and Sintered Alumina Ceramics by Filter Pressing (in Korean)," J. Kor. Ceram. Soc., 46 [3] 306-12 (2009).   과학기술학회마을   DOI   ScienceOn
2 A. Kell and P. Blank, "The Influence of Shaping Method on the Grain Size Dependence of Strength in Dense Submicrometer Alumina," J. Eur. Ceram. Soc., 16 [11] 1189-200 (1996).   DOI   ScienceOn
3 W. E. Lee and W. M Rainforth, "Shape Forming," pp. 31-33 in Ceramic Microstructures, Property Control by Processing, Chapman & Hall, London, 1994.
4 R. Janssen, S. Scheppokat, and N. Claussen, "Tailor-made Ceramic-based Components-Advantages by Reactive Processing and Advanced Shaping Techniques," J. Eur. Ceram. Soc., 28 [7] 1369-79 (2008).   DOI   ScienceOn
5 F. M. Tiller and C.-D. Tsai, "Theory of Filtration of Ceramics: 1, Slip Casting," J. Am. Ceram. Soc., 69 [12] 882-87 (1986).   DOI   ScienceOn
6 G. Tari, S. M. Olhero, and J. M. F. Ferreira, "Influence of Temperature on the Colloidal Processing of Electrostatically Stabilized Alumina Suspensions," J. Mater. Process. Tech., 137 [1-3] 102-09 (2003).   DOI   ScienceOn
7 G. Tari and J. M. F. Ferreira, "Influence of Solid Loading on Drying Shrinkage Behaviour of Slip Cast Bodies," J. Eur. Ceram. Soc., 18 [5] 487-93 (1998).   DOI   ScienceOn
8 S. C. Danforth and M. Velazques, "Permeability of Colloidally Filtered (Slip Cast) Monosized Ceramic Powders," pp. 239-43 in Mater. Res. Soc. Symp. Proc. 24, Eds. by J. H. Crawford, Jr, Y. Chen, and W. A. Sibley, Elsevier, New York, 1984.
9 T. Tambas, Z. E. Erkmen, and S. Ozgen, "Improvement on the Slip Casting of Bayer-Processed Alumina," Am. Ceram. Soc. Bull., 86 [2] 9201-06 (2007).
10 F. F. Lange and K. T. Miller, "Pressure Filtration: Consolidation Kinetics and Mechanics," Am. Ceram. Soc. Bull., 66 [10] 1498-504 (1987).
11 A. Dietrich, A. Neubrand, and Y. Hirata, "Filtration Behavior of Nanoparticulate $CeO_2$ Slurries," J. Am. Ceram. Soc., 85 [11] 2719-24 (2002).
12 Y. Hirata, K. Onoue, and Y. Tanaka, "Effects of pH and Concentration of Aqueous Alumina Suspension on Pressure Filtration Rate and Green Microstructure of Consolidated Powder Cake," J. Ceram. Soc. Jpn., 111 [2] 93-99 (2003).   DOI
13 Y. Hirata, M. Nakamura, M. Miyamoto, Y. Tanaka, and X. H. Wang, "Colloidal Consolidation of Ceramic Nanoparticles by Pressure Filtration," J. Am. Ceram. Soc., 89 [6] 1883-89 (2006).   DOI   ScienceOn
14 S. Raha , K. C. Khilar, P. C. Kapur, and Pradip, "Regularities in Pressure Filtration of Fine and Colloidal Suspensions," Int. J. Miner. Process., 84 [1-4] 348-60 (2007).   DOI   ScienceOn
15 K.-S. Cho, H-K. Lee, and B.-J. Woo, "Effects of Step Pressure on the Shape Forming of Alumina by Pressure-Vacuum Hybrid Slip Casting (in Korean)," J. Kor. Ceram. Soc., 50 [2] 142-48 (2013).   DOI   ScienceOn
16 Y. Hirataw and Y. Tanaka, "Pressure Filtration Model of Ceramic Nanoparticles," J. Am. Ceram. Soc., 91 [3] 819-24 (2008).   DOI   ScienceOn
17 K.-S. Cho, J. Kim, S. Y. Lee, J. P. Oh, and S. I. Park, "Shape Forming of Alumina by Step Pressure-Vacuum Hybrid Slip Casting," Appl. Mech. Mater., 217-219 1899-902 (2012).   DOI
18 K.-S. Cho, I.-B. Song, and J. Kim, "Homogeneous Shape Forming of Alumina by Pressure-Vacuum Hybrid Slip Casting (in Korean)," J. Kor. Ceram. Soc., 49 [6] 592-600 (2012).   과학기술학회마을   DOI   ScienceOn
19 A. Aksay and C. H. Schilling, "Colloidal Filtration Route to Uniform Microstructure," pp. 483-91 in Ultrastructure Processing of Ceramics, Glasses, and Composites. Eds. by L. L. Hench, and D. R. Ulrich. Wiley, New York, 1984.
20 E. G. Blanchard, "Pressure Casting Improves Productivity," Am. Ceram. Soc. Bull., 67 [10] 1680-83(1988).
21 T. Uchikoshi, Y. Sakka, K. Ozawa, and K. Hiraga, "Pressure Filtration and Sintering of Fine Zirconia Powder," J. Eur. Ceram. Soc., 18 [6] 669-74 (1998).   DOI   ScienceOn
22 K. Kendall and M. R. Kosseva, "Nanoparticle Aggregation Influenced by Magnetic Fields," Colloids Surf., A, 286 [1-3] 112-16 (2006).   DOI   ScienceOn
23 K. Matsushima, Y. Hirata, N. Matsunaga, and S. Sameshima, "Pressure Filtration of Alumina Suspensions under Alternating Current Field," Colloids Surf., A, 364 [1-3] 138-44 (2010).   DOI   ScienceOn
24 G. W. Scherer, "Theory of Drying," J. Am. Ceram. Soc., 73 [1] 3-14 (1990).   DOI
25 ASTM C 773-88, "Standard Test Method for Compressive (Crushing) Strength of Fired Whiteware Materials," American Society for Testing and Materials, West Conshohocken, PA, 1999.
26 C.-W. Hong, "New Concept for Simulating Particle Packing in Colloidal Forming Processes," J. Am. Ceram. Soc., 80 [10] 2517-24 (1997).
27 J. D. Yates and S. J. Lombado, "Effect of Solid Loading and Dispersant Concentration on Strain Mismatch and Deformation of Slip-cast Green Bodies," J. Am. Ceram. Soc., 84 [10] 2274-80 (2001).
28 J. L. Amoros, E. Sanchez, V. Cantavella, and J. C. Jarque, "Evolution of the Mechanical Strength of Industrially Dried Ceramic Tiles during Storage," J. Eur. Ceram. Soc., 23 [6] 1839-45 (2003).   DOI   ScienceOn
29 J. D. Yates and S. J. Lombado, "The Effect of Plaster Composition and Binder Concentration on Strain Mismatch and Deformation of Slip-Cast Green Bodies," Mater. Sci. Eng., A, 337 [1-2] 297-305 (2002).   DOI   ScienceOn
30 L. Curkovic and M. F. Jelaca, "Dissolution of Alumina Ceramics in HCl Aqueous Solution," Ceram. Int., 35 [5] 2041-45 (2009).   DOI   ScienceOn
31 R. B. Heimann, "Oxide Ceramics: Structure, Technology, and Application," pp. 175-252 in Classic and Advanced Ceramics, Wiley-VCH Verlag GmbH & Co., Weinheim, 2010.
32 W. E. Lee and W. M Rainforth, "Structural Oxides 1:$Al_2O_3$ and Mullite," pp. 255-316 in Ceramic Microstructures Property Control by Processing, Chapman & Hall, London, 1994.