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http://dx.doi.org/10.4191/KCERS.2009.46.6.592

A Simple Way to Prepare Nanosize NiO Powder by Mixing Acidic Ni Compound with Basic Ni Compound  

Cheong, Deock-Soo (Department of MATSE, Dankook University)
Yun, Dong-Hun (Division of MATSE, Korea Institute of Science and Technology)
Park, Sang-Hwan (Division of MATSE, Korea Institute of Science and Technology)
Kim, Chang-Sam (Battery Research Center, Korea Institute of Science and Technology)
Publication Information
Journal of the Korean Ceramic Society / v.46, no.6, 2009 , pp. 592-595 More about this Journal
Abstract
Nanosize NiO powder was prepared by mixing acidic nickel nitrate with basic nickel carbonate. The particle size and morphology of NiO were mainly governed by the mole ratio of the nitrate to the carbonate. The effects were studied by DSC, XRD, FTIR, and SEM. Heat treatment conditions influence the particle size distribution of produced NiO powder extensively for the case of 3N7C (3 moles of the nitrate and 7 moles of the carbonate) and 4N6C, but only slightly for 1N9C and 2N8C. Uniform pseudospherical NiO particles were obtained in $50{\sim}70$ nm for 1N9C and $30{\sim}60$ nm for 2N8C by calcination at $750{^{\circ}C}$ for 2 h.
Keywords
Nanosize NiO; Nickel nitrate; Basic nickel carbonate; Calcination effects; DSC;
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