Browse > Article
http://dx.doi.org/10.4191/KCERS.2006.43.8.492

Mechanical Properties of Chemical Vapor Deposited SiC Coating Layer  

Lee, Hyeon-Keun (Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology (KAIST))
Kim, Jong-Ho (Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology (KAIST))
Kim, Do-Kyung (Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology (KAIST))
Publication Information
Abstract
SiC coating has been introduced as protective layer in TRISO nuclear fuel particle of High Temperature Gas cooled Reactor (HTGR) due to excellent mechanical stability at high temperature. In order to inhibit the failure of the TRISO particles, it is important to evaluate the fracture strength of the SiC coating layer. ]n present work, thin silicon carbide coating was fabricated using chemical vapor deposition process with different microstructures and thicknesses. Processing condition and surface status of substrate.affect on the microstructure of SiC coating layer. Sphere indentation method on trilayer configuration was conducted to measure the fracture strength of the SiC film. The fracture strength of SiC film with different microstructure and thickness were characterized by trilayer strength measurement method nanoindentation technique was also used to characterize the elastic modulus and th ε hardness of the SiC film. Relationships between microstructure and mechanical properties of CVD SiC thin film were discussed.
Keywords
Silicon carbide coating; Fracture strength; Microstructure; Trilayer strength measurement method;
Citations & Related Records
연도 인용수 순위
  • Reference
1 D. W. Shaw, 'Kinetics of Transport and Epitaxial Growth of GaAs with a $Ga-AsCl_3$ System,' J. Cry. Growth, 8 [1] 117- 28 (1971)   DOI   ScienceOn
2 D. J. Kim, D. J. Choi, and Y. W. Kim, 'Effect of Reactant Depletion on the Microstructure and Preferred Orientation of Polycrystalline SiC Films by Chemical Vapor Deposition,' Thin Solid Films, 266 192-97 (1995)   DOI   ScienceOn
3 K. Niihara, 'High Temperature Hardness and Strength Correlation in $Si_3N_4$,' J. Less-Common Metals, 92 [2] L15-L20 (1983)   DOI   ScienceOn
4 W. A. Bryant, 'Funamentals of Chemical Vapour Deposition,' J. Mat. Sci., 12 [7] 1285-306 (1977)   DOI
5 J. H. Kim, H. K. Lee, and D. K. Kim, 'Strength Measurement of a Brittle Coating with a Trilayer Structure Using Instrumented Indentation and In Situ Observation Techniques,' Phil. Mag., In Press
6 H. S. Kim and D. J. Choi, 'Effect of Diluent Gases on Growth Behavior and Characteristics of Chemically Vapor Deposited Silicon Carbide Films,' J. Am. Ceram. Soc., 82 [2] 331-37 (1999)   DOI   ScienceOn
7 B. R. Lawn, Y. Deng, P. Miranda, A. Pajares, H. Chai, and D. K. Kim, 'Overview: Damage in Brittle Layer Structures from Concentrated Loads,' J. Mater. Res., 17 [12] 3019-36 (2002)   DOI   ScienceOn
8 D. J. Choi, J. G. Lee, J. S. Soo, Y. W. Kim, and D. J. Kim, 'Low Pressure Chemical Vapor Deposition of Silicon Carbide( in Korean),' J. Kor. Ceram. Soc., 31 [3] 257-64 (1994)   과학기술학회마을
9 H. K. Lee, 'Characterization of CVD Silicon Carbide Coating Layer Application for Nuclear Fuel Particle(in Korean),' MS Thesis, KAIST, Daejeon, 2006
10 S. Motojima, H. Yagi, and N. Iwamori, 'Chemical Vapor Deposition of SiC and Some of Its Properties,' J. Mater. Sci. Lett., 5 13-5 (1986)   DOI
11 M. K. So, 'A Study on Deposition Mechanism and Mechanical Property of Silicon Carbide Layer by Chemical Vapor Deposition(in Korean),' Ph. D. Thesis, KAIST, Daejeon, 1987
12 S. Y. Yoon, J. Y. Seo, C. Y. Kim, K. Niihara, and K. H. Kim, 'Deposition of 3C-SiC Films by Plasma-Enhanced Chemical Vapor Deposition (II) : Mechanical Properties of SiC Films by Nanoindentation Technique(in Korean),' J. Kor. Ceram. Soc., 38 [4] 365-69 (2001)
13 J. Chin and T. Ohkawa, 'In Situ Regeneration of Fusion Reactor First Walls,' Nuclear Technology, 32 [3] 115-24 (1977)   DOI
14 J. W. Oh, B. J. Oh, and D. J. Choi, 'The Effect of Input Gas Ratio on the Growth Behavior of Chemical Vapor Deposited SiC Films,' J. Mater. Sci., 35 [2] 1695-700 (2001)
15 M. Hrovat, H. Huschka, A.-W. Mehner, and W. Warzawa, 'Spherical Fuel Elements for Small and Medium Sized HTR,' Nucl. Eng. Des., 109 [1] 253-56 (1988)   DOI   ScienceOn