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http://dx.doi.org/10.4191/KCERS.2005.42.5.314

The Effect of Reaction Parameters in the Characteristic of PZT Powders Synthesized by SHS  

Kim, Byeong-Beom (Engineering Research Center for Rapidly Solidified Materials, Chungnam National University)
Yang, Beom-Seok (Engineering Research Center for Rapidly Solidified Materials, Chungnam National University)
Yun, Ki-Seok (Engineering Research Center for Rapidly Solidified Materials, Chungnam National University)
Won, Chang-Whan (Engineering Research Center for Rapidly Solidified Materials, Chungnam National University)
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Abstract
The effect of reaction parameters in the characteristic of $Pb(Zr_{0.52}Ti_{0.48})O_3$ (below nominal PZT) powders by SHS was investigated in this study. In the preparation of PZT, the effect of starting material contents, pressure, additive on phase fraction and morphology was investigated respectively. The optimum condition of PZT powders were prepared by SHS is $0.37Pb_3O_4+0.52ZrO_2+0.48TiO_2+0.35KClO_3+0.5C,\;(P_{Ar}= 50 atm)$. The PZT powder synthesized in this condition had an spherical shape and the particle size of 0.8$\mu$m.
Keywords
SHS; Characteristic;
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