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http://dx.doi.org/10.4191/KCERS.2004.41.8.582

Microstructure Evolution of Solid State Reacted HAp/β-TCP Composite Powders by Post-Treatment Processing  

박영민 (부산대학교 재료공학부)
양태영 (부산대학교 재료공학)
박상희 (가야대학교 세라믹공학)
윤석영 (부산대학교 재료공학)
박홍채 (부산대학교 재료공학부)
Publication Information
Abstract
Biphasic Calcium Phosphate (BCP) consisted of hydroxyapatite (HAp) and $\beta$-tricalcium phosphate (P-TCP) has been prepared by solid state reaction. The size reduction of the resultant BCP agglomerate was carried out by reaction with hot water under atmospheric condition uld also under high pressure using an autoclave. The influence of processing conditions on the change of crystalline phase and composition, relative amount of constituent, specific surface area, and microstructure was investigated by means of XRD, FT-IR, BET method using a nitrogen adsorption and SEM.
Keywords
Solid state reaction; BCP; HAp; $\beta$-TCP; Size reduction;
Citations & Related Records
Times Cited By KSCI : 3  (Citation Analysis)
연도 인용수 순위
1 Hydroxyapatite and Tricalcium Phosphate Bone Graft Substitutes /
[ R. W. Bucholz;A. Carlton;R. E. Holmes ] / Orthop. Clic. North Am.
2 Bone Formation Following Implantation of Fibrous Compounds (<TEX>${\beta}-Ca(PO_3)_2$</TEX>, CaCO<TEX>$_3$</TEX> (Aragonite)) into Bone Marrow /
[ Y. Ota;T. Iwashita;T. Kasuga;Y. Abe;A. Seki ] / J. Mater Sci.: Mater in Med.   DOI   ScienceOn
3 Microstructural Development in Synthetic Hydroxyapatite /
[ J. H. Kim;Y. M. Park;Y. Y. Yang;S. Y. Yoon;H. C. Park ] / J. Kor Ceram. Soc.   DOI   ScienceOn
4 The Preparation of Biphasic Porous Calcium Phosphate by the Mixture of Ca(H<TEX>$_2PO_4)_2$</TEX> H<TEX>$_2$</TEX> O and CaCO<TEX>$_3$</TEX> /
[ C. K. Hsu ] / Mater Chem. & Phys.
5 Synthesis of Calcium Hydroxyapatite-Tricalcium Phosphate (HA-TCP) Composite Bioceramic Powders and their Sintering Behavior /
[ N. Kivrak;A. C. Tas ] / J. Am. Ceram. Soc.   DOI   ScienceOn
6 Processing and Properties of Hydroxyapatite-Based Biomaterials for Use as Hard Tissue Replacement Implants /
[ W. Suchanek;M. Yoshimura ] / J. Mater Res.   DOI   ScienceOn
7 Biodegradation and Bioresorption of Calcium Phosphate Ceramics /
[ R. Z. Legeros ] / Clin. Mater.   DOI   ScienceOn
8 Surface Dissolution of Hydroxyapatite Biomaterials with Ca/P Ratio /
[ D. S. Seo;H. Kim;J. K. Lee ] / J. Kor. Ceram. Soc.   DOI   ScienceOn
9 Joint Committee on Powder Diffraction Standard /
[] / JCPDS File No. 9-432(HA)
10 Joint Committee on Powder Diffraction Standard /
[] / JCPDS File No. 9-169(TCP)
11 Crystallographic Structure and Surface Morphology of Sintering Carbonated Apatites /
[ L. G. Ellies;D. G. A. Nelson;J. D. B. Featherstone ] / J. Biomed. Mater. Res.   DOI   ScienceOn
12 Fabrication of Hydroxyapatite Whiskers by Hydrolysis of <TEX>${\alpha}$</TEX>-TCP /
[ D. J. Baek;T. Y. Yang;Y. B. Lee;S. Y. Yoon;H. C. Park ] / J. Kor Ceram. Soc.   DOI   ScienceOn
13 Synthesis and Dissolution Behavior of <TEX>${\beta}$</TEX>-TCP and HA/<TEX>${\beta}$</TEX>-TCP Composite Powders /
[ S. H. Kwon;Y. K. Jun;S. H. Hong;H. E. Kim ] / J. Eur. Ceram. Soc.   DOI   ScienceOn
14 In-Situ Synthesis of Biphasic Calcium Phosphate Ceramics Using Microwave Irradiation /
[ I. Manjubala;M. Sivakumar ] / Mater Chem. & Phys.   DOI   ScienceOn
15 Solid-State Transformation of a Non-Stoichiometric Calcium Deficient Apatite into the Biphasic Calcium Phosphate /
[ S. V. Dorozhkin ] / Key Eng.   DOI
16 Preparation of <TEX>${\beta}$</TEX>-TCP with High Thermal Stability by Solid Reaction Route /
[ Y. Pan;J. A. Huang;C. Y. Shao ] / J. Mater. Sci.   DOI   ScienceOn
17 /
[ W. Van Raemdonck;P. Ducheyne;P. De Meedter ] / Metal and Ceramic Biomaterials