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http://dx.doi.org/10.4191/KCERS.2003.40.12.1197

Properties of Nano-sized Au Particle Doped ZrO2 Thin Film Prepared by the Sol-gel Method  

이승민 (경남대학교 신소재공학부)
문종수 (경남대학교 신소재공학부)
Publication Information
Abstract
Thin film on SiO$_2$ glass was synthesized by a dip-coating method from the ZrO$_2$ sol which had dispersed nanosize Au particle under ambient atmosphere. After heat treatment of the prepared thin film, the characteristics were investigated by X-ray diffraction, UV-VIS spectrometer, Atomic Force Microscopy (AFM), Scanning Electron Microscopy (SEM) and Transmission Electron Microscopy (TEM). It was found that ZrO$_2$ thin film with 100 nm thickness was crystallized to tetragonal phase at 50$0^{\circ}C$. The size of dispersed Au particle was 15∼40nm and the film had a smooth surface with a roughness of 0.84 nm. The film showed nonlinearity characteristics with absorption peaks at 630∼670nm visible region because of the plasma resonance of Au metallic particles.
Keywords
Sol-gel; Chelating agent; Heat treatment; Thin film;
Citations & Related Records
Times Cited By KSCI : 9  (Citation Analysis)
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1 Control of Pore Size Distribution of Silica Gel through Sol-gel Process Using Inorganic Salts and Surfactant as Additives /
[ T.Murakata;S.Sato ] / J. Mater. Sci.   DOI
2 Preparation of Crystalline LiNbO₃Films with Preffered Orientation by Hydrolysis of Metal Alkoxides /
[ S.I.Hirano;K.Kato ] / Adv. Ceram. Mater.
3 /
[ A.Stamper;D.W.Greve;D.Wong;T.E.Schlesinger ] / Appl. Phys. Lett.   DOI
4 Preparation of Gold Microcrystal-doped Oxide Optical Coatings Through Adsorption of Tetrachloroaurate Ions on Gel Films /
[ J.Matsuoka;R.Naruse;H.Nasu;K.Kamiya ] / J. Non-cryst. Solids   DOI   ScienceOn
5 /
[ H.Kozuka;S.Sakka ] / Chem. Mater.   DOI
6 /
[ C.S.Mun ] / Science of Sol-gel
7 Zirconia Coating on Stainless Steel Sheets from Organozirconium Compounds /
[ K.Izumi;M.Murakami;T.Deguchi;A.Morita ] / J. Am. Ceram. Soc.   DOI   ScienceOn
8 Semiconductor Nonlinear Materials in Nonlinear Photonics /
[ N.Peyghambarian;S.W.Koch ] / Springer Series in Electronics and Photonics   DOI
9 Synthesis of YSZ Thin Films by PECVD /
[ K.D.Kim;D.G.Shin;Y.A.Cho;J.S.Jeon;D.S.Choi;J.J.Park ] / J. Kor. Mater. Res.   과학기술학회마을
10 Synthesis and Properties of ZrO₂Films Dispersed with Au Nanoparticles /
[ W.Huang;J.Shi ] / J. Sol-gel Sci. and Tech.   DOI   ScienceOn
11 Synthesis of ZrO₂Gel Dispersed with Au Fine Particles by the Sol-gel Method /
[ C.S.Mun;S.M.Lee ] / J. Kor. Mater. Res.   과학기술학회마을   DOI   ScienceOn
12 Characterization of Oxygen Deficiency and Trivalent Zirconium in Sol-gel Derived Zirconia Films /
[ S.Jana;P.K.Biwawa ] / Mater. Lett.   DOI   ScienceOn
13 Properties of Te Fine Particle Doped SiO₂Gel by the Sol-gel Method /
[ C.S.Mun;B.R.Jo;B.S.Kang ] / J. Kor. Mater. Res.   과학기술학회마을   DOI   ScienceOn
14 Sol-gel Processing for Epitaxial Growth of ZrO₂Thin Films on Si(100) Wafers /
[ S.Y.Bae;H.S.Choi;S.Y.Choi;Y.J.Oh ] / Ceram. Int.   DOI   ScienceOn
15 Research on Nonlinear Optical Materials : An Assessement /
[ D.H.Auston(et al.) ] / Appl. Opt.
16 /
[ H.Kozuka ] / Sol-gel Optics Ⅳ
17 Preparation of Zirconia Coating by Hydrolysis of Zirconium Alkoxides with Hydrogen Peroxide /
[ C.Sakurai;T.Fukui ] / J. Am. Ceram. Soc.   DOI   ScienceOn
18 A Study on the Improvement of Oxidation and Corrosion Resistance of Stainless Steel by Sol-gel Ceramic Coating(Ⅱ) : Effect on Oxidation and Corrosion Resistance of CeO₂Stabilized Zirconia Thin Film /
[ K.Hong;I.K.Woo;B.H.Kim ] / J. Kor. Ceram. Soc.   과학기술학회마을
19 Fabrication of Zirconia Thin Films by Plasma Enhanced Metal-organic Chemical Vapor Deposition /
[ K.D.Kim;Y.A.Cho;D.G.Shin;J.S.Jeon;D.S.Choi;J.J.Park ] / J. Kor. Mater. Res.   과학기술학회마을
20 Preparation of Ferroelectric PZT Thin Film by Sol-gel Processing : (Ⅰ) Synthesis of Stable PZT Sol Using Chelating Agent and Preparation of its Thin Film /
[ B.H.Kim;K.Hong;H.Y.Cho ] / J. Kor. Ceram. Soc.   과학기술학회마을
21 Preparation and Properties of Zirconia Coatings form Aquo-organic Solutions of Zirconyl Chloride Octahydrate /
[ A.Atta;P.K.Biswas;D.Ganguli ] / Thin Solid Films   DOI   ScienceOn
22 Preparation of Ag/TiO₂Composite Films by the Sol-gel Method /
[ H.Kozuka;G.Zhao;S.Sakka ] / Bull. Inst. Chem. Res.
23 Fabrication of Sol-gel Derived Antireflective Thin Films of SiO₂-ZrO₂System /
[ B.H.Kim;K.Hong;J.Namkung ] / J. Kor. Ceram. Soc.   과학기술학회마을
24 Fabrication and Properties of Au Fine Particles Doped ZrO₂Thin Film by the Sol-gel Method /
[ C.S.Mun;S.M.Lee ] / J. Kor. Ceram. Soc.   과학기술학회마을   DOI   ScienceOn
25 Preparation of CdS Doped SiO₂Glass Coating Film by the Sol-gel Method /
[ K.M.Kim;H.S.Park;C.S.Mun ] / J. Kor. Ceram. Soc.   과학기술학회마을
26 The Nonlinear Optical Properties of Cds-doped SiO₂Glass Thin Film by the Sol-gel Method /
[ C.S.Mun;J.B.Kang;K.M.Kim ] / J. Kor. Ceram. Soc.