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http://dx.doi.org/10.4191/KCERS.2002.39.10.903

Synthesis and Characterization of Nanosized MnxFe2O4 Powders by Glycothermal Process  

Bae, Dong-Sik (Division of Ceramics, Korea Institute of Science and Technology)
Kim, Eun-Jung (Division of Ceramics, Korea Institute of Science and Technology)
Lee, Hae-Won (Division of Ceramics, Korea Institute of Science and Technology)
Han, Kyong-Sop (Division of Ceramics, Korea Institute of Science and Technology)
Publication Information
Abstract
Nanosized $Mn_xFe_2O_4$ powders were prepared in ethylene glycol solution under mild temperature and pressure conditions by precipitation from metal nitrates with aqueous potassium hydroxide. The average size and distribution of the synthesized $Mn_xFe_2O_4$ powders was about 20 nm and broad, respectively. The phase of synthesized particles was crystalline reacted at 200${\circ}C$ for 6h. The magnetic properties of the synthesized $Mn_xFe_2O_4$ powders were about 35-60 (emu/g) with superparamagnetic character.
Keywords
$Mn_xFe_2O_4$ powders; Glycothermal process; Superparamagnetic character; Nanosize; VSM;
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