Browse > Article
http://dx.doi.org/10.7747/JFES.2017.33.1.33

Effect of Spray-drying Condition and Surfactant Addition on Morphological Characteristics of Spray-dried Nanocellulose  

Park, Chan-Woo (Department of Forest Biomaterials & Engineering, College of Forest and Environmental Sciences, Kangwon National University)
Han, Song-Yi (Department of Forest Biomaterials & Engineering, College of Forest and Environmental Sciences, Kangwon National University)
Namgung, Hyun-Woo (Department of Forest Biomaterials & Engineering, College of Forest and Environmental Sciences, Kangwon National University)
Seo, Pureun-Narae (Department of Forest Biomaterials & Engineering, College of Forest and Environmental Sciences, Kangwon National University)
Lee, Seung-Hwan (Department of Forest Biomaterials & Engineering, College of Forest and Environmental Sciences, Kangwon National University)
Publication Information
Journal of Forest and Environmental Science / v.33, no.1, 2017 , pp. 33-38 More about this Journal
Abstract
In this study, spray-drying yield and morphological characterization of spray-dried cellulose nanofibril (CNF) and TEMPO-oxidized nanocellulose (TONC) depending on spray-drying condition and surfactant addition was investigated. As spray-drying temperature increased, the yield of spray-dried CNF was increased. The highest spray-drying yields in both nanocelluloses were found at didecyl dimethyl ammonium chloride (DDAC) addition of 2.5 phr at all investigated temperatures. The spray-dried CNF was the sphere-like particle, but the spray-dried TONC showed both rod and sphere-like morphology. The average diameter of spray-dried CNF was decreased with increasing DDAC addition amount, resulting in the increase of specific surface area.
Keywords
nanocellulose; TEMPO-oxidation; wet disk-milling; spray-drying; surfactant;
Citations & Related Records
연도 인용수 순위
  • Reference
1 Abe K, Iwamoto S, Yano H. 2007. Obtaining cellulose nanofibers with a uniform width of 15 nm from wood. Biomacromolecules 8: 3276-3278.   DOI
2 Henriksson M, Berglund LA, Isaksson P, Lindström T, Nishino T. 2008. Cellulose nanopaper structures of high toughness. Biomacromolecules 9: 1579-1585.   DOI
3 Iwamoto S, Abe K, Yano H. 2008. The effect of hemicelluloses on wood pulp nanofibrillation and nanofiber network characteristics. Biomacromolecules 9: 1022-1026.   DOI
4 Peng Y, Gardner DJ, Han Y. 2012a. Drying cellulose nanofibrils: in search of a suitable method. Cellulose 19: 91-102.   DOI
5 Peng Y, Han Y, Gardner DJ. 2012b. Spray-drying cellulose nanofibrils: effect of drying process parameters on particle morphology and size distriution. Wood and Fiber Science 44: 1-14.