Development of Analytical Method for Ergot Alkaloids in Foods Using Liquid Chromatoraphy-Tandem Mass Spectrometry |
Chun, So Young
(Food Contaminants Division, National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety)
Chong, Euna (Food Contaminants Division, National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety) Lee, Bomnae (Food Contaminants Division, National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety) Kwon, Jin-Wook (Food Contaminants Division, National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety) Park, Hye Young (Herbal Medicine Research Division, National Institute of Food and Drug Safety Evaluation, Ministry of Food Drug Safety) Kim, Sheenhee (Food Contaminants Division, National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety) Gang, Giljin (Food Contaminants Division, National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety) |
1 | Audenaert K., Vanheule A., Hofte M., Haesaert G.: Deoxynivalenol: A major player in the multifaceted response of fusarium to its environment., Toxins., 6, 1-19 (2013). DOI |
2 | Rasmussen T.B.: Identity and effects of quorum-sensing inhibitors produced by Penicillium species., Microbiology. 151, 1325-1340 (2005). DOI |
3 | Sanzani S., Reverberi M., Punelli M., Ippolito A., Fanelli C.: Study on the role of patulin on pathogenicity and virulence of Penicillium expansum. Int. J. Food Microgiol. 153, 323-331 (2012). DOI |
4 | Meri K., Marika J.: Determination of erogot alkaloids from grains with UPLC-MS/MS, J.Sep. Sci., 33, 2322-2327 (2010). DOI |
5 | Muller C., Klaffke H.S., Krauthause W., Wittkowski R.: Determination of ergot alkaloids in rye and rye flour, Mycotoxin Research, 22, 197-200 (2006). DOI |
6 | Storm I.D., Haverasmussen P., Stobel B.W., Hansen H.C.B.: Ergot alkaloids in rye flour determined by solid-phase cation-exchange and high-pressure liquid chromatography with flourescence dtection, Food Additive and Contaminants, 25, 338-346 (2008). DOI |
7 | Muller C., Sabine K., Klaffke.H, Krauthause W., Weigert A.P., Wittkowski R.: A basic tool for risk assessment: A new method for the analysis of ergot alkaloids in rye and selected rye products, Mol. Nurt. Food Res. 53, 500-507 (2009). DOI |
8 | Komarova E.L., Tolkachev O.N.: The chemistry of peptide ergot alkaloids. Part 1. Classification and chemistry of ergot peptides, Pharmceutical Chemistry Journal 35, 504-513 (2001). DOI |
9 | Floss, H.G., Anderson, J.A.: Biosynthesis of ergot toxins: In Steyn PS (ed) The biosynthesis of mycotoxins a study in secondary metabolism academic press New York. pp. 17-67 (1980). |
10 | Janssen G.B., Beems R.B., Speijers G.J. Egmond H.P.: Subacute toxicity of alpha ergocryptine in Sprague-Dawley rats. 1: general toxicological effects. Food. Chem. Toxicology, 38, 679-688 (2000). DOI |
11 | Bennett, J.W. Klich, M.: Mycotoxins, Clinical Microbiology Reviews. 16, 497-516 (2003). DOI |
12 | Hussein, S.H., Brasel, J.M.: Toxicity, metabolism, and impact of mycotoxins on humans and animals. Toxicology, 167, 101-134. (2001). DOI |
13 | Codex Alimentarius Commission Code of Practice for the prevention and reduction of mycotoxin contamination in cereals (CAC/RCP 51-2003, revised 2014). |
14 | Mulder P.P.J., Fauw D.P.K.H.P., Hoogenboom R.L.A.P., Stoppelaar J., Nijs M.: Tropane and alkaloids in train-based products for infants and young children in the Netherlands in 2011-2014, Food Additive & Contminats : Part B, 8, 284-290 (2015). |
15 | Josep R., Zbynek D., Marta V., Milena Z., Carla S., Jana H.: Anaylsis of mycotoxins in Barley using ultra high liquid chromatography ghig resolution mass spectrometry : comparison of effiency and efficacy of different extraciotn procedure, Talanta, 99, 712-719 (2012). DOI |
16 | Reinhard H., Rupp H., Zoller O.: Ergot alkaloids : quantitation and recognition challenges., Mycotoxin Research, 24, 7-13 (2008). DOI |
17 | Sheryl A.T., Daninna D., Mike R., Twylla M.: Occurrence of ergot and ergot alkaloids in wstern canadian wheat and other cereals., J. Agri. Food Chem, 63, 6644-6650 (2015). DOI |
18 | Burk G., Hobel W., Richt A.: Ergot alkaloid in cereal products, Mol. Nutr. Food Res, 50, 437-442 (2006). DOI |
19 | Krska R., Stubbings G., Macarthur R. Crews C.: Simultaneous determination of six major ergot alkaloids and their epimers in cereals and foodstuffs by LC-MS-MS, Anal. Bioanal Chem, 391, 563-576 (2008). DOI |
20 | Mohameda R., Gremauda E., Payot J.R., Tabet J.C., Guy P.A.: Quantitaive determination of five ergot alkaloids in rye flour by liquid chromatography-electrospray ionisation tandem mass spectrometry, J. of Chrom., 1114, 62-72 (2006). DOI |
21 | Mavungu J.D.M., Malysheva S.V., Snders M., Larionova D., Robbens J., Dugruel P., Peteghem C.V., Saeger S.D.: Development and validation of a new LC-MS/MS method for the simutaneous determination of six major ergot alkaloids and their correspoding epimers. Application to some food and feed commodities, Food Chem., 135, 292-303 (2012). DOI |
22 | Guo Q., Shao B., Du Z., Zhang J.: Simultaneous Determination of 25 Ergot Alkaloids in Cereal Samples by Ultraperformance Liquid Chromatography- Tandem Mass Spectrometry, J. Agri. Food Chem. 64, 7033-7039 (2016). DOI |
23 | Krska R., Crews C.: Significance, chemistry and determination of ergot alkaloids: A review, Food Additive & Contminats : Part A, 25, 722-731 (2008). DOI |
24 | AOAC guidelines for single laboratory validation of chemical methods for dietary supplements and botanicals. Gaithersburg, MD, USA: AOAC International pp. 18-25, (2002). |
25 | The International Council for Harmonisation of Technical Requirements for Pharmaceuticals for Human Use (ICH) validation of analytical procedures: text and methodology, ICH Harmonised Tripartite Guideline p11-13) (2005). |