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http://dx.doi.org/10.22807/KJMP.2022.35.1.65

Pressure-load Calibration of Multi-anvil Press at Ambient Temperature through Structural Change in Cold Compressed Amorphous Pyrope  

Lhee, Juho (School of Earth and Environmental Sciences, Seoul National University)
Kim, Yong-Hyun (School of Earth and Environmental Sciences, Seoul National University)
Lee, A Chim (School of Earth and Environmental Sciences, Seoul National University)
Kim, Eun Jeong (School of Earth and Environmental Sciences, Seoul National University)
Lee, Seoyoung (School of Earth and Environmental Sciences, Seoul National University)
Lee, Sung Keun (School of Earth and Environmental Sciences, Seoul National University)
Publication Information
Korean Journal of Mineralogy and Petrology / v.35, no.1, 2022 , pp. 65-73 More about this Journal
Abstract
The proper estimation of physical and chemical properties of Earth materials and their structures at high pressure and high temperature conditions is key to the full understanding of diverse geological processes in Earth and planetary interiors. Multi-anvil press - high-pressure generating device - provides unique information of Earth materials under compression, mainly relevant to Earth's upper mantle. The quantitative estimation of the relationship between the oil load within press and the actual pressure conditions within the sample needs to be established to infer the planetary processes. Such pressure-load calibration has often been based on the phase transitions of crystalline earth materials with known pressure conditions; however, unlike at high temperature conditions, phase transitions at low (or room) temperatures can be sluggish, making the calibration at such conditions challenging. In this study, we explored the changes in Al coordination environments of permanently densified pyrope glasses upon the cold compression using the high-resolution 27Al MAS and 3QMAS NMR. The fractions of highly coordinated Al in the cold compressed pyrope glasses increase with increasing oil load and thus, the peak pressure condition. Based on known relationship between the peak pressure and the Al coordination environment in the compressed pyrope glasses at room temperature, we established a room temperature pressure-load calibration of the 14/8 HT assembly in 1,100-ton multi-anvil press. The current results highlight the first pressure-load calibration of any high pressure device using high-resolution NMR. Irreversible structural densification upon cold compression observed for the pyrope glasses provides insights into the deformation and densification mechanisms of amorphous earth materials at low temperature and high pressure conditions within the subducting slabs.
Keywords
Pyrope glass; $^{27}Al$ MAS & 3QMAS NMR; Al coordination environment; Multi-anvil press; Room temperature pressure-load calibration;
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1 Lee, S.K., Cody, G.D., Fei, Y. and Mysen, B.O., 2004, Nature of polymerization and properties of silicate melts and glasses at high pressure. Geochimica et Cosmochimica Acta, 68, 4189-4200.   DOI
2 Lee, S.K., Mosenfelder, J.L., Park, S.Y., Lee, A.C. and Asimow, P., 2020a, Configurational entropy of basaltic melts in Earth's mantle. Proceedings of the National Academy of Sciences, 117, 21938-21944.   DOI
3 Yamazaki, D., Ito, E., Yoshino, T., Tsujino, N., Yoneda, A., Gomi, H., Vazhakuttiyakam, J., Sakurai, M., Zhang, Y., Higo, Y. and Tange, Y., 2019, High-pressure generation in the Kawai-type multianvil apparatus equipped with tungsten-carbide anvils and sintered-diamond anvils, and X-ray observation on CaSnO3 and (Mg,Fe)SiO3. Comptes Rendus Geoscience, 351, 253-259.   DOI
4 Lee, S.K., Lee, S.B., Park, S.Y., Yi, Y.S. and Ahn, C.W., 2009, Structure of amorphous aluminum oxide. Physical Review Letters, 103, 095501.   DOI
5 Leinenweber, K.D., Tyburczy, J.A., Sharp, T.G., Soignard, E., Diedrich, T., Petuskey, W.B., Wang, Y. and Mosenfelder, J.L., 2012, Cell assemblies for reproducible multianvil experiments (the COMPRES assemblies). American Mineralogist, 97, 353-368.   DOI
6 Liebermann, R.C., 2011, Multi-anvil, high pressure apparatus: a half-century of development and progress. High Pressure Research, 31, 493-532.   DOI
7 Mosenfelder, J.L., Deligne, N.I., Asimow, P.D. and Rossman, G.R., 2006, Hydrogen incorporation in olivine from 2-12 GPa. American Mineralogist, 91, 285-294.   DOI
8 Park, S.Y. and Lee, S.K., 2018, Probing the structure of Fe-free model basaltic glasses: A view from a solid-state 27Al and 17O NMR study of Na-Mg silicate glasses, Na2O-MgOAl2O3-SiO2 glasses, and synthetic Fe-free KLB-1 basaltic glasses. Geochimica Et Cosmochimica Acta, 238, 563-579.   DOI
9 Allwardt, J.R., 2005, Aluminum coordination and the densification of high-pressure aluminosilicate glasses. American Mineralogist, 90, 1218-1222.   DOI
10 Allwardt, J.R., Stebbins, J.F., Terasaki, H., Du, L.-S., Frost, D.J., Withers, A.C., Hirschmann, M.M., Suzuki, A. and Ohtani, E., 2007, Effect of structural transitions on properties of high-pressure silicate melts: 27Al NMR, glass densities, and melt viscosities. American Mineralogist, 92, 1093-1104.   DOI
11 Bertka, C.M. and Fei, Y., 1997, Mineralogy of the Martian interior up to core-mantle boundary pressures. Journal of Geophysical Research: Solid Earth, 102, 5251-5264.   DOI
12 Bista, S., Stebbins, J.F., Hankins, W.B. and Sisson, T.W., 2015, Aluminosilicate melts and glasses at 1 to 3 GPa: Temperature and pressure effects on recovered structural and density changes. American Mineralogist, 100, 2298-2307.   DOI
13 Stebbins, J.F., Kroeker, S., Keun Lee, S. and Kiczenski, T.J., 2000, Quantification of five- and six-coordinated aluminum ions in aluminosilicate and fluoride-containing glasses by high-field, high-resolution 27Al NMR. Journal of NonCrystalline Solids, 275, 1-6.   DOI
14 Stoyanov, E., Haussermann, U. and Leinenweber, K., 2010, Large-volume multianvil cells designed for chemical synthesis at high pressures. High Pressure Research, 30, 175-189.   DOI
15 Yarger, J.L., Smith, K.H., Nieman, R.A., Diefenbacher, J., Wolf, G.H., Poe, B.T. and McMillan, P.F., 1995, Al coordination changes in high-pressure aluminosilicate liquids. Science, 270, 1964-1967.   DOI
16 Kim, E.J., Kim, Y.-H. and Lee, S.K., 2019, Pressure-induced structural transitions in Na-Li silicate glasses under compression. Journal of Physical Chemistry C, 123, 26608-26622.   DOI
17 Bridgman, P.W. and Simon, I., 1953, Effects of very high pressures on glass. Journal of Applied Physics, 24, 405-413.   DOI
18 Della Valle, R.G. and Venuti, E., 1996, High-pressure densification of silica glass: A molecular-dynamics simulation. Physical Review B, 54, 3809-3816.   DOI
19 Kelsey, K.E., Stebbins, J.F., Singer, D.M., Brown, G.E., Mosenfelder, J.L. and Asimow, P.D., 2009, Cation field strength effects on high pressure aluminosilicate glass structure: Multinuclear NMR and La XAFS results. Geochimica et Cosmochimica Acta, 73, 3914-3933.   DOI
20 Frost, D.J., Poe, B.T., Tronnes, R.G., Liebske, C., Duba, A. and Rubie, D.C., 2004, A new large-volume multianvil system. Physics of the Earth and Planetary Interiors, 143-144, 507-514.   DOI
21 Ji, H., Keryvin, V., Rouxel, T. and Hammouda, T., 2006, Densification of window glass under very high pressure and its relevance to Vickers indentation. Scripta Materialia, 55, 1159-1162.   DOI
22 Keryvin, V., Meng, J.X., Gicquel, S., Guin, J.P., Charleux, L., Sangleboeuf, J.C., Pilvin, P., Rouxel, T. and Le Quilliec, G., 2014, Constitutive modeling of the densification process in silica glass under hydrostatic compression. Acta Materialia, 62, 250-257.   DOI
23 Lee, S.K., Kim, H.-I., Kim, E.J., Mun, K.Y. and Ryu, S., 2016, Extent of disorder in magnesium aluminosilicate glasses: Insights from 27Al and 17O NMR. Journal of Physical Chemistry C, 120, 737-749.   DOI
24 Lee, S.K., 2010, Effect of pressure on structure of oxide glasses at high pressure: Insights from solid-state NMR of quadrupolar nuclides. Solid State Nuclear Magnetic Resonance, 38, 45-57.   DOI
25 Lee, S.K. and Ahn, C.W., 2014, Probing of 2 dimensional confinement-induced structural transitions in amorphous oxide thin film. Scientific Reports, 4.
26 Lee, S.K., Cody, G.D. and Mysen, B.O., 2005, Structure and the extent of disorder in quaternary (Ca-Mg and Ca-Na) aluminosilicate glasses and melts. American Mineralogist, 90, 1393-1401.   DOI
27 Lee, S.K., Lee, A.C. and Kweon, J.J., 2021, Probing medium-range order in oxide glasses at high pressure. The Journal of Physical Chemistry Letters, 12, 1330-1338.   DOI
28 Lee, S.K., 2004, Structure of silicate glasses and melts at high pressure: Quantum chemical calculations and solid-state NMR. The Journal of Physical Chemistry B, 108, 5889-5900.   DOI
29 Kim, E.J., Fei, Y. and Lee, S.K., 2018, Effect of pressure on the short-range structure and speciation of carbon in alkali silicate and aluminosilicate glasses and melts at high pressure up to 8 GPa: 13C, 27Al, 17O and 29Si solid-state NMR study. Geochimica et Cosmochimica Acta, 224, 327-343.   DOI
30 Kim, E.J. and Lee, S.K., 2018, Pressure-load calibration of multi-anvil press and the thermal gradient within the sample chamber. Journal of the Mineralogical Society of Korea, 31, 161-172.   DOI
31 Molnar, G., Ganster, P. and Tanguy, A., 2017, Effect of composition and pressure on the shear strength of sodium silicate glasses: An atomic scale simulation study. Physical Review E, 95, 043001.   DOI
32 Rouxel, T., Ji, H., Guin, J.P., Augereau, F. and Ruffle, B., 2010, Indentation deformation mechanism in glass: Densification versus shear flow. Journal of Applied Physics, 107, 094903.   DOI
33 Ito, E., 2015, Multi-anvil cells and high pressure experimental methods, Treatise on Geophysics (Second Edition). Elsevier, Oxford, 233-261.
34 Vandembroucq, D., Deschamps, T., Coussa, C., Perriot, A., Barthel, E., Champagnon, B. and Martinet, C., 2008, Density hardening plasticity and mechanical ageing of silica glass under pressure: a Raman spectroscopic study. Journal of Physics: Condensed Matter, 20, 485221.   DOI
35 Guerette, M., Poltorak, A., Fei, Y. and Strobel, T.A., 2019, Permanent densification of silica glass for pressure calibration between 9 and 20 GPa at ambient temperature. High Pressure Research, 39, 117-130.   DOI
36 Lee, S.K., Mun, K.Y., Kim, Y.-H., Lhee, J., Okuchi, T. and Lin, J.F., 2020b, Degree of permanent densification in oxide glasses upon extreme compression up to 24 GPa at room temperature. Journal of Physical Chemistry Letters, 11, 2917-2924.   DOI
37 Lee, S.K. and Ryu, S., 2018, Probing of triply coordinated oxygen in amorphous Al2O3. Journal of Physical Chemistry Letters, 9, 150-156.   DOI