[KSCI] Korea Science Citation Index Service

http://dx.doi.org/10.5764/TCF.2014.26.2.143

Structural Analysis for the Single Crystal of 2-(4-(9H-carbazol-9-yl)benzylidene) based Dye Compound

Hwang, Jiyong (BK21, Department of Advanced Organic Materials Engineering, Chungnam National University)
Son, Young-A (BK21, Department of Advanced Organic Materials Engineering, Chungnam National University)

Publication Information

Textile Coloration and Finishing / v.26, no.2, 2014 , pp. 143-149 More about this Journal

Abstract

The designed dye material, namely 2-(4-(9H-carbazol-9-yl)benzylidene) compound, was synthesized. After the reaction, the solid was filtered and purified by recrystalization with acetone/water. To confirm and analyze its synthesis and structural formation, the single crystal was prepared and its measurement was carried out. A yellow needle crystal of $C_{22}H_{13}N_3$ were made on a Rigaku R-AXIS RAPID diffractometer using graphite monochromated CuK ${\alpha}$ radiation. All details were suggested and introduced to support and communicate this study.

Keywords

carbazol; benzylidene; malononitrile; $C_{22}H_{13}N_3$ ; orthorhombic; single crystal;

Citations & Related Records

Reference

1	M. Murakami, M. Fukuyama, M. Suzuki, and M. Hashimoto, Electroluminescent Device Containing Anthraquinone Derivative or Indandione Derivative, Japanese Kokai Tokkyo Koho, JP 08097465, 1996.
2	X. Li, S. H. Kim, and Y. A. Son, Optical Properties of Donor- $\pi$ -(accepter)n Merocyanine Dyes with Dicyanovinylindane as Acepter Group and Triphenylamine as Donor Unit, Dyes and Pigments, 82, 293(2009). DOI ScienceOn
3	S. Horie, M. Nagata, and J. Nakano, Electrophorographic Light-sensitive Materials, United States Patent, US 4469678, 1984.
4	E. Kato, Cellulose Acylate Films, their Manufacture, Optical Films, Liquid-crystal Displays, and Silver Halide Photographic Materials, Japanese Kokai Tokkyo Koho, JP 2004042381, 2004.
5	Crystal Structure 4.0, "Crystal Structure Analysis Package", Rigaku Corporation, Tokyo, pp.196-8666, 2000-2010.
6	M. C. Burla, R. Caliandro, M. Camalli, B. Carrozzini, G. L. Cascarano, L. D. Caro, C. Giacovazzo, G. Polidori, and R. Spagna, An Improved Tool for Crystal Structure Determination and Refinement, J. of Applied Crystallography, 38, 381(2005). DOI ScienceOn
7	G. M. Sheldrick, A Short History of SHELX, Acta Crystallographica Section A, 64, 112(2008).
8	Crystal Structure 3.8, "Crystal Structure Analysis Package", Rigaku and Rigaku/MSC, The Woodlands, TX(USA), 1998-2007.
9	A. Altomare, G. Cascarano, C. Giacovazzo, A. Guagliardi, M. Burla, G. Polidori, and M. Camalli, A Program for Automatic Solution of Crystal Structures by Direct Methods Optimized for Powder Data, J. of Applied Crystallography, 27, 435(1994).
10	V. V. Nesterov, M. Y. Antipin, V. N. Nesterov, and T. V. Timofeeva, Search for New Potential NLO Crystalline Materials: Chiral Derivatives of (2S)-2- (methoxymethyl)pyrrolidine, J. of Molecular Structure, 831, 18(2007). DOI ScienceOn