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http://dx.doi.org/10.5805/SFTI.2021.23.6.844

Study of Simultaneous Analysis of Indicator Components of DTP(Digital Textile Printing) Textile Products Using HPLC-MS/MS - Focusing on Natural Dyes -  

Lee, Wonkyoung (Korea high tech textile research institute)
Sung, Eunji (Korea high tech textile research institute)
Moon, Joung Ryul (Korea high tech textile research institute)
Kim, Miji (Korea high tech textile research institute)
Kim, Jonghoon (Korea high tech textile research institute)
Publication Information
Fashion & Textile Research Journal / v.23, no.6, 2021 , pp. 844-851 More about this Journal
Abstract
Due to the increase in consumers' interest about well-being, interest in eco-friendly products has been increasing due to the harmful effects of various harmful substances contained in textile products and environmental issues. As a result, natural dyes of less potential risk than synthetic dyes and digital textile printing(DTP) textile products with less environmental pollution are drawing attention. However, due to the lack of evaluation criteria for DTP textile products with natural ink and the nature of many colors are stacked layer by layer for dying, the need for simultaneous analysis is emerging. To evaluate whether the natural dye is derived from natural ingredients, the biocarbon content is analyzed. However, in the case of ink made using natural dyes and DTP textile products using natural ink, it is difficult to analyze the biocarbon content due to the limitation of the presence of a small amount of dye contained therein. In this study, we were shown the possibility of natural derived verification by cross-checking the analytes of natural dyes (Persicaria tinctoria, an indigo dye; Dactylopius coccus, a light red; and Curcum longa L., i.e., turmeric) and natural ink with HPLC-MS/MS. The coefficient of determination was 0.999 or higher, the limit of quantification was 0.647-3.664 ㎍/L and a %RSD of each indicator material was less than 10. Then, the extraction amount of natural dyes for five patterned fabrics was analyzed.
Keywords
digital textile printing; natural dyes; natural ink; high-performance liquid chromatography-quadrupole tandem mass spectrometry; biocarbon analysis;
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