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The Fingerprinting of Huangjinju Powder for Injection on Chinese Patent Medicine by XRD Fourier  

Pan, Yan-Li (Beijing University of Chinese Medicine)
Zhang, Gui-Jun (Beijing University of Chinese Medicine)
Gong, Ning-Bo (Institute of Materia Medica of Chinese Academy of Medical Sciences)
Wu, Yun-Shan (Institute of Materia Medica of Chinese Academy of Medical Sciences)
Lu, Yang (Institute of Materia Medica of Chinese Academy of Medical Sciences)
Luo, Rong (Beijing University of Chinese Medicine)
Choi, Ho-Young (Kyung Hee University)
Publication Information
Korean Journal of Medicinal Crop Science / v.14, no.2, 2006 , pp. 117-123 More about this Journal
Abstract
The purpose is to study the identification method of Huangjinju powder for injection and the medicinal materials by the fingerprint off-ray Diffraction Fourier (XRDF). We used the same method on both the studying of Huangjinju and the medicinal materials. Then we selected a few components alignment to compare. We analyzed the data by setting up the deviation $d({\AA})$ as ${\pm}0.05$ to calculate the rate of special mark on the sample (Px) and on the patent (P). The special XRDF of Huangjinju$[d({\AA})/(I/I_0)]$ have 5 peaks that have not expressed in medicinal materials. Therefore Px is 22.73%. Flos Trollii Chinensis has 3 special marks and Px is 17.65%. Flos Chrysanthemi Indici has 1 special mark and Px is 3.57%. Its coincided interplanar spacing with the patent is $2.907{\AA}$. Flos Lonicerae Japonicae has 6 special marks and Px is 23.08%. Its special mark in the patent are 4.95/14 and 4.50/15, respectively. The P is 9.09%. Its coincided interplanar spacing with the patent is $2.910{\AA}\;and\;3.05{\AA}$, respectively. The number of special XRDF mark peaks of baicalin is 9 and Px is 18.37%. Its coincided interplanar spacing with the patent is $2.910{\AA}$. It has visible mark and specificity adopting XRDF fingerprint to identify Huangjinju and medicinal materials. Establishing the quality standard is a synthetic index that depends both on special marks in the medicinal materials of the patent and on the coincidence peak data.
Keywords
Huangjinju powder; XRDF Fingerprinting; Special mark; Evaluating quality;
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