Excluding molten fluoride salt from nuclear graphite by SiC/glassy carbon composite coating |
He, Zhao
(Key Laboratory of Carbon Materials, Institute of Coal Chemistry, Chinese Academy of Sciences)
Song, Jinliang (Key Laboratory of Nuclear Radiation and Nuclear Energy Technology, Shanghai Institute of Applied Physics, Chinese Academy of Sciences) Lian, Pengfei (Key Laboratory of Carbon Materials, Institute of Coal Chemistry, Chinese Academy of Sciences) Zhang, Dongqing (Key Laboratory of Carbon Materials, Institute of Coal Chemistry, Chinese Academy of Sciences) Liu, Zhanjun (Key Laboratory of Carbon Materials, Institute of Coal Chemistry, Chinese Academy of Sciences) |
1 | E. Capelli, O. Bene-s, R.J.M. Konings, Thermodynamic assessment of the system, J. Nucl. Mater. 449 (1-3) (2014) 111-121. DOI |
2 | X.H. An, J.H. Cheng, H.Q. Yin, et al., Thermal conductivity of high temperature fluoride molten salt determined by laser flash technique, Int. J. Heat Mass Transf. 90 (2015) 872-877. DOI |
3 | R.B. Briggs, Molten-Salt Reactor Program Progress Report, Oak Ridge National Laboratory, USA, 1961. ORNL-3122. |
4 | M.W. Rosenthal, P.N. Haubenreich, R.B. Briggs, The Development Status of Molten-Salt Breeder Reactors, Oak Ridge National Laboratory, USA, 1972. ORNL-4812. |
5 | R.B. Briggs, Molten-salt Reactor Program Semi Annual Progress Report, Oak Ridge National Laboratory, USA, 1964. ORNL-3708. |
6 | H. Mccoy, R. Beatty, W. Cook, et al., New developments in materials for molten salt reactors, Nucl. Appl. Technol. 8 (2) (1970) 156-169. DOI |
7 | X.J. He, J.L. Song, L. Xu, et al., Protection of nuclear graphite toward liquid fluoride salt by isotropic pyrolytic carbon coating, J. Nucl. Mater. 442 (1-3) (2013) 306-308. DOI |
8 | X.J. He, J.L. Song, J. Tan, et al., SiC coating: an alternative for the protection of nuclear graphite from liquid fluoride salt, J. Nucl. Mater. 448 (1-3) (2014) 1-3. DOI |
9 | R.B. Briggs, M.W. Rosenthal, P.N. Haubenreich, Molten Salt Reactor Program Semiannual Progress Report, Oak Ridge National Laboratory, USA, 1971. ORNL-4728. |
10 | R.B. Briggs, P.R. Kasten, Molten-salt Reactor Program Semiannual Progress Report, Oak Ridge National Laboratory, USA, 1963. ORNL-3419. |
11 | S. Dutta, Effects of various consolidation techniques on microstructure, strength, and reliability of alpha-SiC, Ceram. Trans. 2 (1989) 215-226. Silicon Carbide '287, printed in United States. |
12 | X. Yang, Q. Huang, Z. Su, et al., Resistance to oxidation and ablation of SiC coating on graphite prepared by chemical vapor reaction, Corros. Sci. 75 (2013) 16-27. DOI |
13 | Y. Kim, C. Jang, E.-S. Kim, SiC coating on various nuclear-grade graphite substrates by chemical vapor reaction, J. Ceram. Process. Res. 15 (5) (2014) 294-297. DOI |
14 | Pimenta MA, G. Dresselhaus, M.S. Dresselhaus, et al., Studying disorder in graphite-based systems by Raman spectroscopy, Phys. Chem. Chem. Phys. 9 (11) (2007) 1276-1291. DOI |
15 | K.S. Xiao, Q.G. Guo, Z.J. Liu, et al., Influence of fiber coating thickness on microstructure and mechanical properties of carbon fiber-reinforced zirconium diboride based composites, Ceram. Int. 40 (1) (2014) 1539-1544. DOI |
16 | ASTM C695-91, Standard Test Method for Compressive Strength of Carbon and Graphite, 2010. |
17 | F. Tuinstra, J.L. Koenig, Raman spectrum of graphite, J. Chem. Phys. 53 (3) (1970) 1126-1130. DOI |
18 | L. Nikiel, P.W. Jagodzinski, Raman-spectroscopic characterization of graphitesa reevaluation of spectra/structure correlation, Carbon 31 (8) (1993) 1313-1317. DOI |
19 | T. Jawhari, A. Roid, J. Casado, Raman spectroscopic characterization of some commercially available carbon black materials, Carbon 33 (11) (1995) 1561-1565. DOI |
20 | S. Chakraborty, D. Debnath, A.R. Mallick, et al., Microscopic, mechanical and thermal properties of spark plasma sintered based composite containing polycarbosilane derived SiC, Int. J. Refract. Metals Hard Mater. 52 (2015) 176-182. DOI |
21 | B. Vriesema, Aspects of Molten Fluorides as Heat Transfer Agents for Power Generation, University of Technology the Netherlands, Department of Mechanical Engineering, 1979. |
22 | GB/T 21650.1-2008/ISO15901-1, Pore Size Distribution and Porosity of Solid Materials by Mercury Porosimetry and Gas Adsorption-Part 1: Mercury Porosimetry, 2005, p. 1. |
23 | Z.T. He, L.N. Gao, X. Wang, et al., Improvement of stacking order in graphite by molten fluoride salt infiltration, Carbon 72 (2014) 304-311. DOI |
24 | M.C. Huang, HsishengTeng, Urea impregnation to enhance porosity development of carbons prepared from phenol-formaldehyde resins, Carbon 40 (6) (2002) 955-958. DOI |
25 | Z. He, P.F. Lian, Y. Song, et al., Improving molten fluoride salt and barrier property of nuclear graphite by phenolic resin impregnation process, J. Nucl. Mater. 499 (2018) 79-87. DOI |
26 | S.S. Tzeng, J.H. Pan, Densification of two-dimensional carbon/carbon composites by pitch impregnation, Mater. Sci. Eng. 316 (2001) 127-134. DOI |
27 | J.L. Song, Y.L. Zhao, J.P. Zhang, et al., Preparation of binderless nanopore-isotropic graphite for inhibiting the liquid fluoride salt and penetration for molten salt nuclear reactor, Carbon 79 (2014) 36-45. DOI |
28 | J.J. Biernacki, G.P. Wotzak, Stoichiometry of the reaction, J. Am. Ceram. Soc. 72 (1) (1989) 122-129. DOI |
29 | P.F. Lian, J.L. Song, Z.J. Liu, et al., Preparation of ultrafine-grain graphite by liquid dispersion technique for inhibiting the liquid fluoride salt infiltration, Carbon 102 (2016) 208-215. DOI |
30 | J.L. Song, Q.G. Guo, X.Q. Gao, et al., intermediate layers for the wetting and infiltration of graphite foams by liquid copper, Carbon 49 (10) (2011) 3165-3170. DOI |
31 | X.M. Yang, M. Liu, Y.T. Gao, et al., Effect of oxygen on the corrosion of SiC in LiF-NaF-KF molten salt, Corros. Sci. 103 (2016) 165-172. DOI |
32 | W.T. Zhang, B.L. Zhang, J.L. Song, et al., Microstructure and molten salt impregnation characteristics of a micro-fine grain graphite for use in molten salt reactors, N. Carbon Mater. 31 (6) (2016) 585-593. DOI |
33 | T. Abram, S. Ion, Generation-IV nuclear power: a review of the state of the science, Energy Policy 36 (12) (2008) 4323-4330. DOI |
34 | M.S. Sohal, M.A. Ebner, P. Sabharwall, et al., Engineering Database of Liquid Salt Thermophysical and Thermochemical Properties, 2010. Technical Report INL/EXT-10-18297. |
35 | D.E. Holcomb, S.M. Cetiner, An Overview of Liquid-Fluoride-Salt Heat Transport Systems, Oak Ridge National Laboratory, USA, 2010. ORNL/TM-2010/156. |
36 | J.L. Song, Y.L. Zhao, X.J. He, et al., Preparation of pyrolytic carbon coating on graphite for inhibiting liquid fluoride salt and penetration for molten salt breeder reactor, J. Nucl. Mater. 456 (2015) 33-40. DOI |
37 | Z. He, P.F. Lian, Y. Song, et al., Protecting nuclear graphite from liquid fluoride salt and oxidation by SiC coating derived from polycarbosilane, J. Eur. Ceram. Soc. 38 (2) (2018) 453-462. DOI |
38 | V. Bernardet, S. Gomes, S. Delpeux, et al., Protection of nuclear graphite toward fluoride molten salt by glassy carbon deposit, J. Nucl. Mater. 384 (3) (2009) 292-302. DOI |
39 | S. Ueta, J. Sumita, T. Shibata, et al., R&D plan for development of oxidation-resistant graphite and investigation of oxidation behavior of SiC coated fuel particle to enhance safety of HTGR, Nucl. Eng. Des. 271 (2014) 309-313. DOI |
40 | Y.F. Gu, J.X. Liu, Y. Wang, et al., Corrosion behavior of TiC-SiC composite ceramics in molten FLiNaK salt, J. Eur. Ceram. Soc. 37 (7) (2017) 2575-2582. DOI |
41 | Y.H. Yun, Y.H. Park, M.Y. Ahn, et al., CVR-SiC coating of graphite pebbles for fusion blanket application, Ceram. Int. 40 (1) (2014) 879-885. DOI |
42 | Y. Lee, Y.H. Yun, Y.H. Park, et al., Surface coating of graphite pebbles for Korean HCCR TBM, Fusion Eng. Des. 89 (7-8) (2014) 1734-1738. DOI |
43 | T. Iseki, M. Ishida, H. Suzuki, Thermal shock behavior of SiC coatings for fusion reactor applications, J. Nucl. Sci. Technol. 19 (7) (1982) 587-592. DOI |