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Analysis of 236 Pesticides in Apple for Validation of Multiresidue Method using QuEChERS Sample Preparation and PTV-GC/TOFMS Analysis  

Ju, Ok-Jung (Department of Agro-food Safety, National Academy of Agriculture Science, Rural Development Administration)
Kwon, Hye-Young (Department of Agro-food Safety, National Academy of Agriculture Science, Rural Development Administration)
Park, Byeong-Jun (Department of Agro-food Safety, National Academy of Agriculture Science, Rural Development Administration)
Kim, Chan-Seob (Department of Agro-food Safety, National Academy of Agriculture Science, Rural Development Administration)
Jin, Yong-Duk (Department of Agro-food Safety, National Academy of Agriculture Science, Rural Development Administration)
Lee, Je-Bong (Department of Agro-food Safety, National Academy of Agriculture Science, Rural Development Administration)
Yun, Seo-Hee (Department of Agro-food Safety, National Academy of Agriculture Science, Rural Development Administration)
Son, Kyung-Ae (Department of Agro-food Safety, National Academy of Agriculture Science, Rural Development Administration)
Hong, Su-Myeong (Department of Agro-food Safety, National Academy of Agriculture Science, Rural Development Administration)
Im, Geon-Jae (Department of Agro-food Safety, National Academy of Agriculture Science, Rural Development Administration)
Publication Information
The Korean Journal of Pesticide Science / v.15, no.4, 2011 , pp. 401-416 More about this Journal
Abstract
The recent trend for pesticide residue analysis in food involves fast cleanup and use of mass spectrometry to achieve quantitative and qualitative analysis at the same time. Recently, the QuEChERS (quick, easy, cheap, effective, rugged and safe) multi-reside method has received much attention as a fast extraction and cleanup method of pesticide residue analysis. Therefore, multi-residue analysis of 236 pesticides was tested with the QuEChERS method by concurrent use of PTV-GC/TOFMS (gas chromatography/ time-of-flight mass spectrometry with programmable temperature vaporizer). PTV condition was optimized and when the method was applied to apples, pesticide recovery rates (spiked at 400 ng/g) ranged from 80% to 120%, and RSD values were under 10% for most compounds. The results showed that the QuEChERS sample preparation and PTV-GC/TOFMS analysis can be applied to multi-residue analysis of pesticides in fruits and vegetables.
Keywords
Pesticide; Multiresidue analysis; QuEChERS; PTV-GC/TOFMS;
Citations & Related Records
Times Cited By KSCI : 3  (Citation Analysis)
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