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Development of Rapid Analysis Method for Pesticide Residues by GC-MS/MS  

Choi, Yong-Hoon (Testing and Analysis Team, Gyeongin Regional Office, Korea Food and Drug Administration)
Nam, Hye-Seon (Testing and Analysis Team, Gyeongin Regional Office, Korea Food and Drug Administration)
Hong, Hye-Mi (Department of Food and Nutrition, Inha University)
Lee, Jin-Ha (Testing and Analysis Team, Gyeongin Regional Office, Korea Food and Drug Administration)
Chae, Kab-Ryong (Testing and Analysis Team, Busan Regional Office, Korea Food and Drug Administration)
Lee, Jong-Ok (Food Contaminants Team, Korea Food and Drug Administration)
Kim, Hee-Yun (Testing and Analysis Team, Gyeongin Regional Office, Korea Food and Drug Administration)
Yoon, Sang-Hyeon (Testing and Analysis Team, Gyeongin Regional Office, Korea Food and Drug Administration)
Publication Information
The Korean Journal of Pesticide Science / v.9, no.4, 2005 , pp. 292-302 More about this Journal
Abstract
Condition of Ion-Trap gas chromatography-mass spectrometry (GC-MS) for rapid screening of 206-pesticides residues in agricultural foodstuffs was optimized. As applying a wide-bore column (10 m${\times}$0.53 mm, DF 0.25 um) connected with a fused silica restrictor (0.6 m${\times}$0.1 mm), a significant retention time reduction was obtained. Additionally, the shape of peaks was sharper and higher than classical GC's and GC-MS's, which allowed lower detection limits. To easily manage many spectral data, both of Electron Ionization(EI) and Chemical Ionization(CI) techniques were adopted in screening procedure. At the following steps, MS-MS technique were used to confirm screened analytes in complicated matrices.
Keywords
GC-MS; Wide-bore column; Pesticide residues;
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