Browse > Article
http://dx.doi.org/10.12654/JCS.2012.28.2.113

The Analysis on VOCs That Occurs in Leather Cultural Heritage with SPME  

Chung, Yong-Jae (Department of Conservation Science, The Korean National University of Cultural Heritage)
Publication Information
Journal of Conservation Science / v.28, no.2, 2012 , pp. 113-118 More about this Journal
Abstract
Cultural heritages emit volatile organic compounds(VOCs) during degradation as chemical, biological factors. These VOCs in the atmosphere are degradation factors for another materials. But non-destructive organic analysis methods are uncommon, and have difficulties for field application. In this study, solid phase micro-extraction(SPME) and gas chromatography( GC) are carried out for analysis of VOCs which are emitted from leather, and prove SPME field holder's efficiency. I analize leather archival objects at The National Archives of Korea by cross-checking GC and SPME methods. It could be confirmed that the compounds are (E)-2-nonenal, butyl hydroxy toluene emitted itself from leather.
Keywords
Solid-phase microextraction(SPME); Non-destructive analysis method; Volatile organic compound(VOCs); Archival objects; Leather; Gas chromatography(GC);
Citations & Related Records
연도 인용수 순위
  • Reference
1 Stolow Nathan, "Conservation standards for works of art in trasit and on exhibition". UNESCO, (1979).
2 Baer, N.S & P.N.Banks, "Indoor air pollution: effects on cultural and historic material", International Journal of Museum Managemant and curatorship, 4, p9-20, (1985).
3 L.Muller, T.Gorecki, J.Pawliszyn, "Optimization of the SPME device design for field application.", Anal Chem, 24, p610-616, (1999).
4 Koziel, J.A, P.A.martos, J.Pawliszyn, "System for the generation of standard gas mixtures of volitale and semi-volitale organic compounds for calibrations of solid-phase microextraction and other sampling device", Journal of Chromatography A, 30, p3-9, (2004).
5 Agnes Lattuati-Derieux, "Characterisation of volatile organic compounds emitted by a naturally aged book using SPME-GC/MS", Centre de recherches sur la conservation des doucments graphiques, p.9-18, (2004).
6 Butterworth-Heinemann, "The National Trust Manual of Housekeeping", ELSEVIER, p393-403, (2008).
7 Marion Kite.Roy Thomson, "Conservation of leather and related materials", ELSEVIER, p127-150, (2006).
8 김명웅, "가죽공업화학 ", 선진문화사, p44, (2008).
9 이현경, "흡착/열탈착/GC/MSD를 이용한 제품에서의 VOC분석", 국민대학교 대학원 석사학위논문, p13-20, (2004).
10 임문순, 송희남, 김기현, "SPME 분석기법을 응용한 VOC 및 주요 악취물질들의 검량특성에 대한 연구", 한국대기환경학회, 10, p62-65, (2006).
11 허귀석, 유혜경, 홍진희, 신호상, "SPME를 이용한 대기중 미량 악취성 Aldehyde 화합물의 분석", 한국대기환경학회 학술대회 논문집 2, p350-351, (2000).