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http://dx.doi.org/10.4313/JKEM.2020.33.6.515

Process Parameter Control of Arc Melting Process for Ti3SiC2 MAX Phase Synthesis  

Nou, Chang Wan (School of Energy, Materials and Chemical Engineering, Korea University of Technology and Education)
Kim, Byeong Guen (Vehicle Engineering Team, Research Development Division, Gyeongbuk Institute of IT Convergence Industry Technology)
Bae, Sang Hyun (School of Energy, Materials and Chemical Engineering, Korea University of Technology and Education)
Choi, Soon-Mok (School of Energy, Materials and Chemical Engineering, Korea University of Technology and Education)
Publication Information
Journal of the Korean Institute of Electrical and Electronic Material Engineers / v.33, no.6, 2020 , pp. 515-520 More about this Journal
Abstract
The Ti3SiC2 MAX phase was synthesized by arc-melting process under three different processing times. We confirmed that the reaction between the TiCX phase and Ti-Si liquid phase is important for the synthesis of the Ti3SiC2 MAX phase. Results suggest that the Ti3SiC2 MAX phase decomposed when the arc-melting time was greater than 80s. Herein, we aim to determine the detailed parameters for the reported arc-melting process, which can provide useful insights on the synthesis of the Ti3SiC2 MAX phase by arc-melting process. Furthermore, we compared the electrical characteristics and densities of the three samples.
Keywords
MAX phase; $Ti_3SiC_2$; Arc melting; Electrical characteristics;
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