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http://dx.doi.org/10.4313/JKEM.2009.22.4.355

Dependence of Growth Temperature on MFI Zeolite Membrane Growth  

Kim, Duk-Eun (동의대학교 나노공학과)
Ko, Chang-Hyun (한국에너지기술연구원 화학공정연구센터)
Oh, Weon-Tae (동의대학교 나노공학과)
Publication Information
Journal of the Korean Institute of Electrical and Electronic Material Engineers / v.22, no.4, 2009 , pp. 355-359 More about this Journal
Abstract
Si wafer, which was treated with TMSP-TBA (N-trimethoxysilylpropyl-n,n,n-tri-n-butylammonium bromide), was used foF a substrate to grow a MFI membrane. Growth of membranes was conducted in various conditions such as temperature and gravity, and their structures were in detail studied with field emission scanning electron microscope and x-ray diffractometer. The structures of membranes grown on substrates were strongly dependent on growing temperature and gravity.
Keywords
MFI; Membrane; Growth; Self-assembly; Monolayer;
Citations & Related Records
Times Cited By KSCI : 1  (Citation Analysis)
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1 K.-K. Song and K. Ha, 'Preparation of oriented MFI zeolite membranes', Korean Chem. Eng. Res., Vol. 44, No. 3, p. 243, 2006
2 F. Gramm and C. Baerlocher, 'Complex zeolite structure solved by combining powder diffraction and electron microscopy', Nature, Vol. 444, p. 79, 2006   DOI   ScienceOn
3 G. Cao, 'Nanostructures and Nanomaterials', p. 51, p. 110, 2003
4 Lai, R. and Gavalas, G. R., 'Surface seeding in ZSM-5 membrane preparation', Ind. Eng. Chem. Res., Vol. 37, No. 11, p. 4275, 1998   DOI   ScienceOn
5 Valtchev, V., Mintova, S., and Konstantinov, L., 'Influence of metal substrate properties on the kinetics of zeolite film formation', Zeolites, Vol. 15, No. 8, p. 679, 1995   DOI   ScienceOn
6 Valtchev, V., Schoeman, B. J., Hedlund, J., Mintova, S., and Sterte, J., 'Preparation and characterization of hollow fibers of silicalite- 1', Zeolites, Vol. 17, No. 5-6, p. 408, 1996   DOI   ScienceOn
7 Valtchev, V., Hedlund, J., Schoeman, B. J., Sterte, J., and Mintova, S., 'Deposition of continuous silicalite-1 films on inorganic fibers', Microporous Materials, Vol. 8, No. 1-2, p. 93, 1997   DOI   ScienceOn
8 Bernal, M., Xomeritakis, G., and Tsapatsis, M., 'Tubular MFI zeolite membranes made by secondary (seeded) growth', Catal. Today, Vol. 67, No. 1-3, p. 101, 2001   DOI   ScienceOn
9 J. M. Lee, B.-J. Jung, J.-I. Lee, H. Y. Chu, L.-M. Do, and H.-K. Shim, 'Modification of an ITO anode with a hole-transporting SAM for improved OLED device characteristics', J. Mater. Chem., Vol. 12, p. 3494, 2002   DOI   ScienceOn
10 Larlus, O., Valtchev, V., Patarin, J., Faust, A.-C., and Maquin, B., 'Preparation of silicalite-1/glass fiber composites by one- and two-step hydrothermal syntheses', Microporous Mesoporous Mat., Vol. 56, No. 2, p. 175, 2002   DOI   ScienceOn
11 W. T. Oh and S. Nair, 'Concentration profiling of a molecular sieve membrane by step-scan photoacoustic spectroscopy', J. Phys. Chem. B, Vol. 108, No. 26, p. 8766, 2004   DOI   ScienceOn
12 Z. Lai., G. Bonilla., I. Diaz., and J. G. Nery, 'Microstructural optimization of a zeolite membrane for organic vapor separation', Science, Vol. 300, p. 456, 2003
13 P. A. Georgiev, A. Albinati, B. L. Mojet, and J. Ollivier, 'Observation of exceptionally strong binding of molecular hydrogen in a porous material: formation of an $\eta$2-H2 complex in a Cu-exchanged ZSM-5 zeolite', J. Am. Chem. Soc., Vol. 129, p. 8086, 2007   DOI   ScienceOn
14 K. Wang, X. Wang, and G. Li, 'A study on acid sites related to activity of nanoscale ZSM-5 in toluene disproportionation', Catal. Commun., Vol. 8, p. 324, 2007   DOI   ScienceOn
15 Lai, Z., Bonilla, G., Diaz, I., Nery, J. G., Sujaoti, K., Amat, M. A., Kokkoli, E., Terasaki, O., Thompson, R. W., Tsapatsis, M., and Vlachos, D. G., 'Microstructural optimization of a zeolite membrane for organic vapor separation', Science, Vol. 300, p. 456, 2003
16 Lai, Z., Tsapatsis, M., and Nicolich, J. P., 'Siliceous ZSM-5 membranes by secondary growth of b-oriented seed layers', Adv. Funct. Mater., Vol. 14, No. 7, p. 716, 2004   DOI   ScienceOn
17 Breck, D. W., 'Zeolite Molecular Sieve', Wiley, New York, p. 461, 1974
18 Zhang, F.-Z., Fuji, M., and Takahashi, M., 'In Situ growth of continuous b-oriented MFI zeolite membranes on porous $\alpha$-alumina substrates precoated with a mesoporous silica sublayer', Chem. Mater., Vol. 17, No. 5, p. 1167, 2005   DOI   ScienceOn
19 Kim, H. S., Lee, S. M., Ha, K., Jung, C., Lee, Y.-J., C. Hun, Y. S., Kim, D., Rhee, B. K., and Yoon, K. B., 'Aligned inclusion of hemicyanine dyes into silica zeolite films for second harmonic generation', J. Am. Chem. Soc., Vol. 126, No. 2, p. 673, 2004   DOI   ScienceOn
20 Chiou, Y. H., Taai, T. G., Sung, S. L., Shih, H. C., Wu, C. N., and Chao, K. J., 'Synthesis and characterization of zeolite (MFI) membrane on anodic alumina', J. Chem. Soc., Faraday Trans., Vol. 92, No. 6, p. 1061, 1996   DOI
21 P. Zhang, X. Guo, H. Guo, and X. Wang, 'Study of the performance of modified nano- scale ZSM-5 zeolite on olefins reduction in FCC gasoline', J. Mol. Catal. A, Chemical, Vol. 261, p. 139, 2007   DOI   ScienceOn
22 R. Rungsirisakun, T. Nanok, M. Probst, and J. Limtrakul, 'Adsorption and diffusion of benzene in the nanoporous catalysts FAU, ZSM-5 and MCM-22: A molecular dynamics study', J. Mol. Graphics Modell., Vol. 24, p. 373, 2006   DOI   ScienceOn