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http://dx.doi.org/10.17702/jai.2011.12.4.133

Preparation and Characterization of Graphene/Zn-Al Layered Double Hydroxide Composites  

Lee, Jong-Hee (Department of Polymer Science and Engineering, Chungju National University)
Ko, Yl-Woong (Department of Polymer Science and Engineering, Chungju National University)
Kim, Ki-Young (Department of Textile Convergence of Biotechnology & Nanotechnology, Korea Institute of Industrial Technology)
Lim, Jung-Hyurk (Department of Polymer Science and Engineering, Chungju National University)
Kim, Kyung-Min (Department of Polymer Science and Engineering, Chungju National University)
Publication Information
Journal of Adhesion and Interface / v.12, no.4, 2011 , pp. 133-137 More about this Journal
Abstract
Exfoliated graphite oxide (EGO) was prepared by graphite oxide in an aqueous solution of TMAOH. The hybrid graphene/Zn-Al LDH material was fabricated by the hydrothermal reduction of the solution of EGO, $Zn(NO_3)_2{\cdot}6H_2O$, $Al(NO_3)_3{\cdot}9H_2O$, urea, and trisodium citrate. That is, metal ions were absorbed on the surface of EGO, and Zn-Al LDH material was randomly dispersed on the surface of graphene along with a reduction process of EGO to graphene by hydrothermal treatment. The composition, morphology, and thermal property of the obtained graphene-based hybrid material were studied by FE-SEM, EDX, TEM, FT-IR, XRD, TGA, and DSC.
Keywords
graphite oxide; graphene; layered double hydroxide; hydrothermal reduction;
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