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http://dx.doi.org/10.6564/JKMRS.2011.15.1.014

Liquid Chromatography-Solid Phase Extraction-NMR (LC-SPE-NMR) Analysis of Liquid Crystalline Mixtures  

Park, Gregory Hyung-Jin (LCD R&D Center, LCD Business, Samsung Electronic Co., Ltd.)
Park, Ae-Na (LCD R&D Center, LCD Business, Samsung Electronic Co., Ltd.)
Rho, Kyung-Rae (LCD R&D Center, LCD Business, Samsung Electronic Co., Ltd.)
Shin, Jong-Ho (LCD R&D Center, LCD Business, Samsung Electronic Co., Ltd.)
Kim, Yeong-Jeon (LCD R&D Center, LCD Business, Samsung Electronic Co., Ltd.)
Jo, Sung-Chan (LCD R&D Center, LCD Business, Samsung Electronic Co., Ltd.)
Oh, Weon-Sik (LCD R&D Center, LCD Business, Samsung Electronic Co., Ltd.)
Publication Information
Journal of the Korean Magnetic Resonance Society / v.15, no.1, 2011 , pp. 14-24 More about this Journal
Abstract
We have performed Liquid Chromatography-Solid Phase Extraction-NMR (LC-SPE-NMR) analysis for liquid crystalline mixture and elucidated the structures of selected components by NMR spectra. Combining the results of one-dimensional 1H experiments as well as homonuclear and heteronuclear two-dimensional experiments, we could analyze the molecular structure of the liquid crystal singles whose structure had not been interpretable by mass spectrometry alone.
Keywords
Liquid crystal; NMR; LC-SPE-NMR; tetrahydropyran;
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