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http://dx.doi.org/10.5012/jkcs.2012.56.1.078

New Synthesis of Perhydrotriazolotriazoles Catalyzed by TiCl4 under Ambient Conditions  

Safari, J. (Laboratory of Organic Compound Research, Department of Organic Chemistry, Faculty of Chemistry, University of Kashan)
Gandomi-Ravandi, S. (Laboratory of Organic Compound Research, Department of Organic Chemistry, Faculty of Chemistry, University of Kashan)
Ghotbinejad, M. (Laboratory of Organic Compound Research, Department of Organic Chemistry, Faculty of Chemistry, University of Kashan)
Publication Information
Journal of the Korean Chemical Society / v.56, no.1, 2012 , pp. 78-81 More about this Journal
Abstract
Aromatic 2,3-diazabuta-1,3-dienes in glacial acetic acid with isothiocyanate in the presence of catalyst $TiCl_4$ at room temperature produced via criss-cross cycloaddition reactions the corresponding perhydro[1,2,4]triazolo[1,2-a][1,2,4] triazole-1,5-dithiones in relatively high yields and short reaction time.
Keywords
Criss cross cycloaddition; Azine; Catalyst; Perhydrotriazolotriazole;
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