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http://dx.doi.org/10.5012/jkcs.2002.46.3.194

Synthesis and Characterization of Mn(Ⅲ) Chloro Complexes with Salen-Type Ligands  

Byeon, Jong Cheol (Department of Chemistry, Cheju National University)
Han, Chung Hun (Department of Chemistry, Cheju National University)
Park, Yu Cheol (Department of Chemistry, Kyungpook National University)
Lee, Nam Ho (Department of Chemistry, Cheju National University)
Baek, Jong Seok (Department of Chemistry, Cheju National University)
Publication Information
Journal of the Korean Chemical Society / v.46, no.3, 2002 , pp. 194-204 More about this Journal
Abstract
Aseries of novel salen-type complexes {[Mn(III)($L_{acn}$)CI]: n=1~11} containing CI- ion were obtained by reactions of the Mn(CH$_3$COO)$_2$· 4H$_2$O with the potentially tetradentate compartmental ligand {$H$_2$L_{acn}$} prepared by condensation the of one mole of diamine {ethylenediamine, 1,3-propnediamine, o-phenylenediamine and 2,2-dimethyl-1,3-propanediamine} with two moles of aldehyde {alicylaldehyde, 5-chloro-salicylaldehyde, 3,5-dichlorosalicylaldethyde, and 3,5-di-tert-butyl-2-hydroxy-benzaldehyde} in a methanol solution. The resulting salen-type lignds and their Mn(III) complexes were identified and characterized by elemental analysis, conductivity, themogravimetry and UV-VIS, IR and NMR spectroscopy.
Keywords
Salen-Type Complexes; [Mn(Ⅲ)($L_acn$)CI];
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