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http://dx.doi.org/10.5012/bkcs.2014.35.7.1999

Hydrothermal Synthesis of Indium Tin Oxide Nanoparticles without Chlorine Contamination  

Wang, Hai Wen (Department of Chemistry, East China University of Science and Technology)
Xu, Guo Dong (Department of Chemistry, East China University of Science and Technology)
Zhang, Jian Rong (Ningbo Jinxin Advanced Materials Ltd.)
Yin, Xin (Department of Chemistry, East China University of Science and Technology)
Publication Information
Bulletin of the Korean Chemical Society / v.35, no.7, 2014 , pp. 1999-2003 More about this Journal
Abstract
Indium tin oxide ($In_2Sn_{1-x}O_{5-y}$) nanoparticles were synthesized by hydrothermal method from stable indium tin acetylacetone complexes and postannealing at $600^{\circ}C$. The absence of chlorine ions shortened the synthesis process, decreased the particle agglomeration and improved the particle purity. The introduced complexing ligand acetylacetone decreased the obtained nanoparticle size. The improved powder properties accelerated the sintering of the $In_2Sn_{1-x}O_{5-y}$ nanoparticles and reached a relative density of 96.4% when pressureless sintered at $1400^{\circ}C$.
Keywords
Indium tin oxide; Synthesis; Nanoparticle; Sintering;
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