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http://dx.doi.org/10.5012/bkcs.2014.35.5.1495

Syntheses, Structures, and Characterization of Two Novel Copper(II) and Cadmium(II) Compounds Based on Pyridyl Conjugated 1,2,3-Triazole  

Hong, Jin-Long (School of Chemistry and Chemical Engineering, Southeast University)
Qu, Zhi-Rong (Key Laboratory of Organosilicon Chemistry and Material Technology of Ministry of Education, Hangzhou Normal University)
Ma, Hua-Jun (Key Laboratory of Organosilicon Chemistry and Material Technology of Ministry of Education, Hangzhou Normal University)
Wang, Gai-Gai (School of Chemistry and Chemical Engineering, Southeast University)
Zhao, Hong (School of Chemistry and Chemical Engineering, Southeast University)
Publication Information
Bulletin of the Korean Chemical Society / v.35, no.5, 2014 , pp. 1495-1500 More about this Journal
Abstract
Two new complexes with 5-methyl-1-(pyridine-3-yl)-1H-1,2,3-triazole-4-carboxylic acid (Hmptc) ligand: [$Cd(mptc)_2(H_2O)_4$] (1) and $[Cu(mptc)_4{\cdot}2H_2O]_n$ (2) were prepared and their crystal structures were determined by single crystal X-ray diffraction analyses. In complex 1, the Cd(II) ions coordinates with the pyridyl nitogen atom from the Hmptc ligand, forming a mononuclear Cd(II) compound. Complex 2 exhibits a novel two-dimensional (2D) polymer in which four Hmptc ligands stabilize the Cu(II) atom. And the coordination involves one nitrogen atom of the triazole, one oxygen atom of the carboxylic acid and the pyridyl nitrogen atom. In addition, FT-IR and solid-state fluorescent emission spectroscopy of two compounds have been determined.
Keywords
Triazole; Copper(II) complex; Cadmium(II) complex; Crystal structure;
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