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http://dx.doi.org/10.5012/bkcs.2014.35.5.1417

Structural Diversity of Five New Lanthanide Coordination Polymers Tuned by Different Salt Anions  

Tao, Yinhua (School of Chemistry and Chemical Engineering, Southeast University)
Lou, Yongbing (School of Chemistry and Chemical Engineering, Southeast University)
Li, Yang (School of Chemistry and Chemical Engineering, Southeast University)
Chen, Jinxi (School of Chemistry and Chemical Engineering, Southeast University)
Publication Information
Bulletin of the Korean Chemical Society / v.35, no.5, 2014 , pp. 1417-1421 More about this Journal
Abstract
Five new lanthanide coordination polymers, $[Ln_2(1,4-NDC)_2(1,4-HNDC)_2(phen)_2]_n$ (Ln = Er (1), Yb (2)), and $[Ln_2(1,4-NDC)_3(phen)_2(H_2O)_2]_n$ (Ln = Nd (3), Gd (4), Er (5)) ($1,4-H_2NDC$ = 1,4-naphthalenedicarboxylic acid, phen = 1,10-phenanthroline), have been successfully prepared via the reaction of corresponding trivalent lanthanide salt, $1,4-H_2NDC$ and phen in the presence of NaOH and pyridine under hydrothermal condition. Pyridine plays a key role in the synthesis of these lanthanide coordination polymers. Single-crystal X-ray diffraction analyses indicate that compounds 1-5 all form a 2-D network while different salt anions result in the diversity of crystal structures. These lanthanide coordination polymers showed a considerable thermal stability in TGA analyses.
Keywords
Lanthanide coordination polymers; Pyridine; Structural diversity; Hydrothermal;
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