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http://dx.doi.org/10.5012/bkcs.2014.35.1.204

Simultaneous Electrochemical Determination of Hydroquinone, Catechol and Resorcinol at Nitrogen Doped Porous Carbon Nanopolyhedrons-multiwall Carbon Nanotubes Hybrid Materials Modified Glassy Carbon Electrode  

Liu, Wei (State Key Laboratory of Chemo/Biosensing and Chemometrics, College of Chemistry and Chemical Engineering, Hunan University)
Wu, Liang (State Key Laboratory of Chemo/Biosensing and Chemometrics, College of Chemistry and Chemical Engineering, Hunan University)
Zhang, Xiaohua (State Key Laboratory of Chemo/Biosensing and Chemometrics, College of Chemistry and Chemical Engineering, Hunan University)
Chen, Jinhua (State Key Laboratory of Chemo/Biosensing and Chemometrics, College of Chemistry and Chemical Engineering, Hunan University)
Publication Information
Bulletin of the Korean Chemical Society / v.35, no.1, 2014 , pp. 204-210 More about this Journal
Abstract
The nitrogen doped porous carbon nanopolyhedrons (N-PCNPs)-multi-walled carbon nanotubes (MWCNTs) hybrid materials were prepared for the first time. Combining the excellent catalytic activities, good electrical conductivities and high surface areas of N-PCNPs and MWCNTs, the simultaneous determination of hydroquinone (HQ), catechol (CC) and resorcinol (RE) with good analytical performance was achieved at the N-PCNPs-MWCNTs modified electrode. The linear response ranges for HQ, CC and RE are 0.2-455 ${\mu}M$, 0.7-440 ${\mu}M$ and 3.0-365 ${\mu}M$, respectively, and the detection limits (S/N = 3) are $0.03{\mu}M$, $0.11{\mu}M$ and $0.38{\mu}M$, respectively. These results are much better than that obtained on some graphene or CNTs-based materials modified electrodes. Furthermore, the developed sensor was successfully applied to simultaneously detect HQ, CC and RE in the local river water samples.
Keywords
Multi-walled carbon nanotubes; Nitrogen doped porous carbon nanopolyhedrons; Simultaneous detection; Dihydroxybenzene isomers;
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